IP Library Granted Patent US 9,005,669
Granted Patent B2
US 9,005,669 · App. 13/285,341 · Granted Apr 14, 2015

Synergy of strong acids and peroxy compounds

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Quick Facts
Patent No.
US 9,005,669
App. No.
13/285,341
Granted
Apr 14, 2015
Kind
B2
Abstract

Disclosed is a method for improving decontamination in meat, poultry, fish, fruit and vegetable processing using a combination of acid(s) and peroxy compound(s). The method comprises a “stacked” approach, sequentially adding the acid(s) and peroxy compound(s) to an aqueous stream to provide a point-of-use low-pH antimicrobial composition that is highly effective for decontamination of food products, as well as safer for use in a processing facility.

Claims (30)

1. A method of decontaminating food products comprising the steps of:

(a) establishing an aqueous flowing stream;

(b) introducing at least one strong acid into the aqueous flowing wherein the at least one strong acid is selected from a group consisting of hydrochloric acid, sulfuric acid and phosphoric acid;

(c) providing a peroxyacetic acid (PAA);

(d) admixing the peroxyacetic acid with the aqueous flowing stream separately from the at least one strong acid to provide an antimicrobial composition, wherein the concentration of said at least one strong acid ranges from about 5 to about 35 percent and the concentration of said peroxyacetic acid ranges from 1 ppm to about 1000 ppm of the antimicrobial composition, wherein the pH of the antimicrobial composition is from about 0.5 to about 3.5; and

(e) applying the antimicrobial composition directly to the food product selected from the group consisting of poultry, meat, fish, fruit, and vegetables.

2. The method of claim 1 , wherein the antimicrobial composition is directed to at least one endpoint selected from the group consisting of a mist, a spray, a dip, a deluge, a flume, an electrostatic application, and atomization, for application of the antimicrobial composition to the food product.

3. The method of claim 1 , wherein the at least one strong acid comprises at least one buffered acid.

4. The method of claim 1 , wherein the peroxyacetic acid comprises up to 1000 ppm for poultry.

5. The method of claim 1 , wherein the peroxyacetic acid comprises up to 230 ppm for red meat.

6. The method of claim 1 , wherein the peroxyacetic acid comprises from 1 ppm to about 1000 ppm for red meat.

7. The method of claim 3 where the buffered acid is a safe acid.

8. The method of claim 1 wherein the peroxyacetic acid is added to the aqueous stream before the addition of the at least one strong acid.

9. The method of claim 3 , wherein the at least one buffered acid comprises hydrochloric acid (HCl).

10. The method of claim 3 , wherein the at least one buffered acid comprises sulfuric acid (H 2 SO 4 ).

11. The method of claim 3 , wherein the at least one buffered acid comprises phosphoric acid (H 3 PO 4 ).

12. A method of decontaminating a poultry product, comprising the steps of:

(a) establishing an aqueous flowing stream;

(b) introducing at least one strong acid into the aqueous flowing stream, wherein the at least one strong acid is selected from a group consisting of hydrochloric acid, sulfuric acid, and phosphoric acid;

(c) providing a peroxyacetic acid;

(d) admixing the peroxyacetic acid with the aqueous flowing stream separately from the at least one strong acid to provide an antimicrobial composition, wherein the concentration of said at least one strong acid is from about 5 to about 35 percent of the composition, wherein the pH of the composition is from about 0.5 to about 3.5, and wherein the peroxyacetic acid is less than 100 ppm; and

(e) applying the composition directly to the poultry product on at least one endpoint selected from the group consisting of a mist, a spray, a dip, a deluge, a flume, an electrostatic application, and atomization.

13. The method of claim 12 , wherein the at least one strong acid further comprises at least one buffered acid selected from a group consisting of hydrochloric acid, sulfuric acid, and phosphoric acid.

14. A method of decontaminating a red meat product, comprising the steps of:

(a) establishing an aqueous flowing stream;

(b) introducing at least one strong acid into the aqueous flowing stream, wherein the at least one strong acid is selected from a group consisting of hydrochloric acid, sulfuric acid, and phosphoric acid;

(c) providing a peroxyacetic acid;

(d) admixing the peroxyacetic acid with the aqueous flowing stream separately from the at least one strong acid to provide an antimicrobial composition, wherein the concentration of said at least one strong acid is from about 5 to about 35 percent of the composition, wherein the pH of the composition is from about 0.5 to about 3.5, and wherein the concentration of the peroxyacetic acid ranges from 1 ppm to about 1000 ppm; and

(e) applying the composition directly to the red meat product on at least one endpoint selected from the group consisting of a mist, a spray, a dip, a deluge, a flume, an electrostatic application, and atomization.

15. The method of claim 14 , wherein the at least one strong acid further comprises at least one buffered acid selected from a group consisting of hydrochloric acid, sulfuric acid, and phosphoric acid.

Assignments (5)
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 050605/0305 Recorded Feb 3, 2020
From: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
To: PEROXYCHEM LLC
Reel/Frame 051777/0957 →
SECURITY INTEREST Recorded Oct 2, 2019
From: PEROXYCHEM LLC
To: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
Reel/Frame 050605/0305 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 19, 2018
From: SYNERGY TECHNOLOGIES, INC.
To: PEROXYCHEM LLC
Reel/Frame 046912/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 3, 2015
From: ALLEN, RANDALL R.; KNOCKE, JAMES; PARKER, CARLETON J., III; YORK, JASON; DIDATO, DEAN T.
To: SYNERGY TECHNOLOGIES, INC.
Reel/Frame 035080/0001 →
SECURITY INTEREST Recorded Jun 17, 2014
From: SYNERGY TECHNOLOGIES, INC.
To: RIDGESTONE BANK
Reel/Frame 033183/0764 →