IP Library Granted Patent US 9,353,003
Granted Patent B2
US 9,353,003 · App. 14/208,422 · Granted May 31, 2016

Hydraulic composition with prolonged open time

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Quick Facts
Patent No.
US 9,353,003
App. No.
14/208,422
Granted
May 31, 2016
Kind
B2
Abstract

The presently disclosed and claimed inventive concept(s) relates generally to a hydraulic composition with a prolonged open time. More particularly, the composition comprises at least one cement retarder and at least one accelerator. The presently disclosed and claimed inventive concept(s) further relates to a dry mortar composition comprising the hydraulic composition having prolonged open time without deterioration of the other cement tile adhesive properties such as workability, setting time, strength development and sag resistance.

Claims (19)

1. A composition, comprising:

sodium polyphosphate; and

at least one accelerator selected from the group consisting of sodium thiocyanate, calcium formate, calcium chloride, and combinations thereof,

wherein when the composition is combined with a cementitious tile adhesive that (a) has a water factor of 0.26 and (b) comprises 0.4 wt % methyl hydroxyethyl cellulose, 35 wt % Cement 52.5 R, and 64.4 wt % Sand F35 on a dry weight basis, to produce a product, the product has (i) an open time in a range of from about 40 minutes to about 55 minutes and (ii) a setting time in a range of from about 800 minutes to about 950 minutes.

2. The hydraulic composition of claim 1 , further comprising a cellulose ether.

3. The hydraulic composition of claim 2 , wherein the cellulose ether is selected from the group consisting of alkylcelluloses, hydroxyalkylcellluloses, alkylhydroxyalkylcelluloses, and combinations thereof.

4. A dry cement mortar, comprising:

cement;

sodium polyphosphate; and

at least one accelerator selected from the group consisting of sodium thiocyanate, calcium formate, calcium chloride, and combinations thereof.

5. The dry cement mortar of claim 4 , wherein the sodium polyphosphate is in a range of about 0.001 to about 0.5 wt % based on the total weight of the dry cement mortar.

6. The dry cement mortar of claim 5 , wherein the sodium polyphosphate is in a range of about 0.005 to about 0.3 wt % based on the total weight of the dry cement mortar.

7. The dry cement mortar of claim 6 , wherein the sodium polyphosphate is in a range of about 0.01 to about 0.05 wt % based on the total weight of the dry cement mortar.

8. The dry cement mortar of claim 4 , wherein the accelerator is in a range of about 0.01 to about 1 wt % based on the total weight of the dry cement mortar.

9. The dry cement mortar of claim 8 , wherein the accelerator is in a range of about 0.05 to about 0.5 wt % based on the total weight of the dry cement mortar.

10. The dry cement mortar of claim 9 , wherein the accelerator is in a range of about 0.1 to about 0.3 wt % based on the total weight of the dry cement mortar.

11. A method for making a cementitious tile adhesive comprising the steps of:

mixing the hydraulic composition of claim 1 , a cement and an optional component; and

admixing the amount of water required for processing to a settable mortar.

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Jan 10, 2020
From: THE BANK OF NOVA SCOTIA
To: AVOCA LLC; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES LLC
Reel/Frame 051557/0504 →
SECURITY AGREEMENT Recorded Jul 3, 2017
From: AVOCA, INC.; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES, INC.
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 043084/0753 →
CHANGE OF NAME Recorded May 18, 2017
From: HERCULES INCORPORATED
To: HERCULES LLC
Reel/Frame 042497/0331 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 15, 2014
From: HOHN, WILFRIED ADOLF; HUCKO, STEFAN; KINDLER, ALEXANDER ADOLPHE; NILLES, VERA LOUISE; WUNDERLICH, MARTIN
To: HERCULES INCORPORATED
Reel/Frame 032676/0427 →