Method for producing rare earth sintered magnet
View Patent ↗The present invention provides a method for producing a long and large-sized rare earth sintered magnet having a large size in a magnetic field application direction in which a single magnet body in each portion has uniform and high magnetic characteristics. Disclosed is a method for producing a rare earth sintered magnet, including particular steps of: 1) preparing a slurry; 2) preparing a cavity that is enclosed with a mold, an upper punch and a lower punch; 3) applying a magnetic field of 1.5 T or more in the cavity, and supplying the slurry at a flow rate of 20 to 600 cm 3 /second, to fill the cavity with the slurry; 4) producing a molded body of the alloy powder by press molding in the magnetic field; and 5) sintering the molded body.
1. A method for producing a rare earth sintered magnet, comprising the steps of:
1) preparing a slurry including an alloy powder and a dispersion medium at a predetermined ratio, the alloy powder containing a rare earth element, iron and boron;
2) preparing a cavity enclosed with a mold, and an upper punch and a lower punch, at least one of the upper punch and the lower punch being movable toward and away from the other one in the mold, at least one of the upper punch and the lower punch including an outlet for discharging the dispersion medium of the slurry;
3) applying a magnetic field of 1.5 T or more in the cavity in the direction parallel to the direction in which at least one of the upper punch and the lower punch is movable, and supplying the slurry at a flow rate of 20 to 600 cm 3 /second to fill the cavity with the slurry;
4) producing a molded body of the alloy powder by press molding in the magnetic field, the upper punch and the lower punch coming closer to each other while applying the magnetic field; and
5) sintering the molded body;
wherein the cavity has a length of 10 mm or more in the direction in which at least one of the upper punch and the lower punch is movable,
the slurry has a concentration of 84 to 90% by mass of the alloy powder, and
in the direction in which at least one of the upper punch and the lower punch is movable, a ratio (L 0 /LF) of the length (L 0 ) of a cavity before press molding in the magnetic field to the length (LF) of the molded body is within a range of 1.1 to 1.4.
2. The method for producing a rare earth sintered magnet according to claim 1 , wherein the flow rate of the slurry is within a range of 20 to 400 cm 3 /second.
3. The method for producing a rare earth sintered magnet according to claim 1 , wherein the flow rate of the slurry is within a range of 20 to 200 cm 3 /second.
4. The method for producing a rare earth sintered magnet according to claim 1 , wherein the flow rate of slurry is 200 to 600 cm 3 /second.