IP Library Granted Patent US 10,696,926
Granted Patent B2
US 10,696,926 · App. 15/880,152 · Granted Jun 30, 2020

Stable unit dose compositions with high water content and structured surfactants

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Quick Facts
Patent No.
US 10,696,926
App. No.
15/880,152
Granted
Jun 30, 2020
Kind
B2
Abstract

Stable unit dose compositions with high water content are provided. Such unit dose compositions include an aqueous composition having a water activity of from about 0.60 to about 0.95 and a water-soluble container formed from a water-soluble or water-dispersible film material. In one embodiment, the aqueous composition includes water in an amount of 20% to 70% by weight, a structured surfactant system which is in the form of a lamellar structure, and a salt which promotes the formation of the lamellar structure. The surfactant system may include: (1) a linear alkylbenzene sulfonate (LAS) and/or an alcohol ethoxylsulfate (AES), (2) a non-ionic surfactant, and (3) a fatty acid. The unit dose compositions can prevent the enclosed liquid detergent composition with a high level of water content from dissolving or pre-maturely dispersing the water-soluble container due to the lamellar structure of the composition.

Claims (66)

1. A unit dose detergent product comprising:

(a) a water-soluble container formed from a water-soluble or water-dispersible film material;

(b) an aqueous composition comprising:

(i) water present in an amount of about 20% to about 70% by weight;

(ii) a surfactant system present in an amount of about 15% to about 70% by weight; wherein the surfactant system is a lamellar structured system; and

(iii) a salt present in an amount of about 0.5% to about 25% by weight;

wherein the aqueous composition has a water activity of from about 0.65 to about 0.95;

wherein the surfactant system comprises:

(1) a linear alkylbenzene sulfonate (LAS) in an amount of about 10% to about 20% by weight; an alcohol ethoxylsulfate (AES) in an amount of about 20% to about 40% by weight;

(2) an alcohol ethoxylate (AE) in an amount of about 20% to about 50% by weight; and

(3) a fatty acid in an amount of about 1% to about 15% by weight.

2. The unit dose detergent product of claim 1 ,

wherein water is present in an amount of about 30% to about 60% by weight;

wherein the structured surfactant system is present in an amount of about 25% to about 55% by weight; and

wherein the salt is present in an amount of about 2% to about 10% by weight.

3. The unit dose detergent product of claim 1 ,

wherein the salt contains a cation and an anion, wherein the cation is selected from the group consisting of sodium, calcium, potassium, magnesium, quaternary ammonium, pyridinium, tris(2-hydroxyethyl)methyl ammonium, and a mixture thereof, and the anion is selected from the group consisting of a halide, phosphate, sulphate, formate, acetate, citrate, maleate, succinate, methylsulfate, and a mixture thereof.

4. The unit dose detergent product of claim 3 ,

wherein the salt is sodium chloride, sodium citrate, sodium formate, or a mixture thereof.

5. The unit dose detergent product of claim 1 ,

wherein

the structured surfactant system is present in an amount of about 40% to about 70% by weight; and

the salt is present in an amount of about 0.5% to about 5% by weight.

6. The unit dose detergent product of claim 1 ,

wherein

the structured surfactant system is present in an amount of about 15% to 35% by weight; and

the salt is present in an amount of about 5% to about 20% by weight.

7. The unit dose detergent product of claim 1 ,

wherein

the structured surfactant system is present in an amount of about 35% to about 45% by weight.

8. The unit dose detergent product of claim 1 ,

wherein the aqueous composition from about 30% to about 55% by weight of water.

9. The unit dose detergent product of claim 1 ,

wherein the aqueous composition has a water activity of from about 0.80 to about 0.90.

10. The unit dose detergent product of claim 1 ,

wherein the aqueous composition further comprises a saccharide, an organic solvent, or a combination thereof, as a water binding agent.

11. The unit dose detergent product of claim 1 ,

wherein the aqueous composition does not contain a water binding agent selecting from a saccharide, an organic solvent, and a mixture thereof.

12. A unit dose detergent product comprising:

(a) a water-soluble container formed from a water-soluble or water-dispersible film material;

(b) an aqueous composition comprising:

(i) water present in an amount of about 20% to about 70% by weight;

(ii) a surfactant system present in an amount of about 15% to about 70% by weight; wherein the surfactant system is a lamellar structured system; and

(iii) a salt present in an amount of about 0.5% to about 25% by weight;

wherein the surfactant system comprises:

(1) a linear alkylbenzene sulfonate (LAS); an alcohol ethoxylsulfate (AES),

(2) an alcohol ethoxylate (AE), and

(3) a fatty acid;

wherein the weight ratio of LAS:AES:AE is about 1:2:3; and

wherein the aqueous composition has a water activity of from about 0.65 to about 0.95.

13. The unit dose detergent product of claim 12 ,

wherein water is present in an amount of about 30% to about 60% by weight;

wherein the structured surfactant system is present in an amount of about 25% to about 55% by weight; and

wherein the salt is present in an amount of about 2% to about 10% by weight.

14. The unit dose detergent product of claim 12 , wherein the salt contains a cation and an anion, wherein the cation is selected from the group consisting of sodium, calcium, potassium, magnesium, quaternary ammonium, pyridinium, tris(2-hydroxyethyl)methyl ammonium, and a mixture thereof, and the anion is selected from the group consisting of a halide, phosphate, sulphate, formate, acetate, citrate, maleate, succinate, methylsulfate, and a mixture thereof.

15. The unit dose detergent product of claim 12 , wherein

the structured surfactant system is present in an amount of about 40% to about 70% by weight; and

the salt is present in an amount of about 0.5% to about 5% by weight.

16. The unit dose detergent product of claim 12 , wherein

the structured surfactant system is present in an amount of about 15% to 35% by weight; and

the salt is present in an amount of about 5% to about 20% by weight.

17. The unit dose detergent product of claim 12 , wherein

the structured surfactant system is present in an amount of about 35% to about 45% by weight.

18. The unit dose detergent product of claim 12 , wherein the aqueous composition from about 30% to about 55% by weight of water.

19. The unit dose detergent product of claim 12 , wherein the aqueous composition further comprises a saccharide, an organic solvent, or a combination thereof, as a water binding agent.

20. The unit dose detergent product of claim 12 , wherein the aqueous composition does not contain a water binding agent selecting from a saccharide, an organic solvent, and a mixture thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: HENKEL IP & HOLDING GMBH
To: HENKEL AG & CO. KGAA
Reel/Frame 059357/0267 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2018
From: CAMIRE, CASEY ELPHEGE; AKEEM, PATRICK SHANE; MOSER, CYNTHIA L; PIORKOWSKI, DANIEL THOMAS; STOTT II, DAVID S.
To: HENKEL IP & HOLDING GMBH
Reel/Frame 045048/0877 →