IP Library Granted Patent US 12,286,364
Granted Patent B1
US 12,286,364 · App. 18/674,615 · Granted Apr 29, 2025

System and method for extracting boron from feed water

Inventors: Kirk M. Pumphrey (San Jose, CA); Kenneth Aoki (Woodland, CA); Darrell R. Aoki (Woodland, CA)
C02F1/42C02F1/008C02F1/441C02F2101/108C02F2103/001C02F2301/066C02F2303/16
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Quick Facts
Patent No.
US 12,286,364
App. No.
18/674,615
Granted
Apr 29, 2025
Kind
B1
Abstract

In a method for extracting boron from feed water, boron is extracted from feed water received as irrigation runoff water from an agricultural source at a pressurized vessel located at a first location, the pressurized vessel including a boron-selective resin bed. The pressurized vessel is uncoupled from the agricultural source, wherein the boron-selective resin bed is boron-saturated. The pressurized vessel comprising the boron-saturated resin bed is transported to a second location. The pressurized vessel comprising the boron-saturated resin bed is coupled to a boron extraction system at the second location. An acid-based solution is injected into the boron-saturated resin bed, causing the boron to be released from the resin bed and into a boron solution. The boron solution is drained from the pressurized vessel into a holding tank.

Claims (64)

1. A method for extracting boron from feed water, the method comprising:

at a pressurized vessel located at a first location, the pressurized vessel comprising a boron-selective resin bed, extracting boron from feed water received as irrigation runoff water from an agricultural source;

uncoupling the pressurized vessel from the agricultural source, wherein the boron-selective resin bed is boron-saturated;

transporting the pressurized vessel comprising the boron-saturated resin bed to a second location;

coupling the pressurized vessel comprising the boron-saturated resin bed to a boron extraction system at the second location;

at the boron extraction system at the second location:

performing a backwash operation on the boron-saturated resin bed within the pressurized vessel;

injecting an acid-based solution from a first storage tank into the boron-saturated resin bed, causing the boron to be released from the resin bed and into a boron solution;

draining the boron solution from the pressurized vessel into a holding tank;

performing an acid displacement rinse operation on the resin bed within the pressurized vessel;

subsequent the performing the acid displacement rinse operation, injecting a caustic solution from a second storage tank into the resin bed, the caustic solution recharging the resin bed for extracting the boron from the feed water;

performing a caustic displacement rinse operation on the resin bed for preparing the resin bed for receiving the feed water;

performing a resin bed rinse operation on the resin bed, wherein the resin bed rinse operation has an input flow rate higher than an input flow rate of the backwash operation; and

distributing surplus water of the acid displacement rinse operation and the caustic displacement rinse operation to an agricultural operation site for irrigation operations.

2. The method of claim 1 , wherein the performing the backwash operation comprises:

injecting reverse osmosis water into the pressurized vessel through an opening in the pressurized vessel.

3. The method of claim 1 , further comprising:

draining the backwash operation into a surplus tank.

4. The method of claim 1 , wherein the acid-based solution is injected into the pressurized vessel through an opening in the pressurized vessel.

5. The method of claim 1 , wherein the boron solution is drained through an opening in the pressurized vessel.

6. The method of claim 1 , further comprising:

during the draining, monitoring a boron concentration level of the boron solution in the pressurized vessel; and

responsive to the boron concentration level falling below a threshold boron concentration level, ceasing the draining of the boron solution from the pressurized vessel into the holding tank.

7. The method of claim 6 , further comprising:

subsequent the ceasing the draining of the boron solution from the pressurized vessel into the holding tank, draining residual boron solution into the first storage tank.

8. The method of claim 1 , wherein the acid displacement rinse operation is performed using reverse osmosis (RO) water.

9. The method of claim 1 , further comprising:

draining the acid displacement rinse operation into a surplus tank.

10. The method of claim 1 , wherein the caustic solution comprises a hydroxide.

11. The method of claim 10 , wherein the hydroxide comprises at least one of: potassium hydroxide (KOH), sodium hydroxide (NaOH), sodium carbonate (Na 2 CO 3 ).

12. The method of claim 1 , wherein the caustic displacement rinse operation is performed using reverse osmosis (RO) water.

13. The method of claim 1 , further comprising:

returning the caustic solution injected into the resin bed to the second storage tank.

14. The method of claim 1 , wherein the backwash operation has an input flow rate higher than an input flow rate of the injecting the acid solution and an input flow rate of the injecting the caustic solution.

15. The method of claim 1 , further comprising:

receiving the feed water at the resin bed for extracting the boron from the feed water.

16. The method of claim 1 , further comprising:

extracting boric acid from the boron solution.

17. The method of claim 1 , further comprising:

processing surplus water of the backwash operation and the resin bed rinse operation at a reverse osmosis system for generating reverse osmosis water for providing the reverse osmosis water to the backwash operation, the acid displacement rinse operation, the caustic displacement rinse operation, and the resin bed rinse operation.

18. The method of claim 1 , wherein the method generates substantially zero waste such that the boron solution is stored in the holding tank for further processing, the caustic solution injected into the resin bed is returned to the second storage tank, surplus water of the backwash operation and the resin bed rinse operation is used for generating reverse osmosis water, and the surplus water of the acid displacement rinse operation and the caustic displacement rinse operation is returned to the agricultural source of the feed water.

19. A method for extracting boron from feed water, the method comprising:

at a pressurized vessel located at a first location, the pressurized vessel comprising a boron-selective resin bed, extracting boron from feed water received as irrigation runoff water from an agricultural source;

uncoupling the pressurized vessel from the agricultural source, wherein the boron-selective resin bed is boron-saturated;

transporting the pressurized vessel comprising the boron-saturated resin bed to a second location;

coupling the pressurized vessel comprising the boron-saturated resin bed to a boron extraction system at the second location;

at the boron extraction system at the second location:

performing a backwash operation using reverse osmosis water on the boron-saturated resin bed within the pressurized vessel;

draining the reverse osmosis water of the backwash operation into a surplus tank;

injecting an acid-based solution from a first storage tank into the boron-saturated resin bed, causing the boron to be released from the resin bed and into a boron solution;

draining the boron solution from the pressurized vessel into a holding tank;

during the draining, monitoring a boron concentration level of the boron solution in the pressurized vessel;

responsive to the boron concentration level falling below a threshold boron concentration level, ceasing the draining of the boron solution from the pressurized vessel into the holding tank;

subsequent the ceasing the draining of the boron solution from the pressurized vessel into the holding tank, draining residual boron solution into the first storage tank;

performing an acid displacement rinse operation within the pressurized vessel using reverse osmosis water;

draining the reverse osmosis water of the acid displacement rinse operation into the surplus tank;

subsequent the draining the reverse osmosis water of the acid displacement rinse operation, injecting a caustic solution from a second storage tank into the resin bed, the caustic solution recharging the resin bed for extracting the boron from the feed water;

performing a caustic displacement rinse operation on the resin bed using reverse osmosis water for preparing the resin bed for receiving the feed water;

draining the reverse osmosis water of the caustic displacement rinse operation into the surplus tank;

performing a resin bed rinse operation on the resin bed using reverse osmosis water, wherein the resin bed rinse operation has an input flow rate higher than an input flow rate of the backwash operation;

draining the reverse osmosis water of the resin bed rinse operation in the surplus tank; and

distributing output of the surplus tank to an agricultural operation site for irrigation operations, such that surplus water of the backwash operation, the acid displacement rinse operation, the caustic displacement rinse operation, and the resin bed rinse operation are distributed to the agricultural operation site.

20. The method of claim 19 , further comprising:

extracting boric acid from the boron solution.

Continuity (1)
Continuation 18336893 · Jun 16, 2023
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