IP Library Granted Patent US 8,476,367
Granted Patent B1
US 8,476,367 · App. 13/017,317 · Granted Jul 2, 2013

Pelletized plastic compounds and method of manufacture

Inventor: George D. Howell (Arlington, TX)
Assignee: Spartech Corporation
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Quick Facts
Patent No.
US 8,476,367
App. No.
13/017,317
Granted
Jul 2, 2013
Kind
B1
Abstract

A pellet is formed by a method includes, in one embodiment, dispersing up to about 95% by weight of thermoset rubber particles into a carrier resin to form the plastic compound. The carrier resin includes an olefin block copolymer. The method also includes the steps of extruding the plastic compound through a die having at least one die hole to form at least one extrudate filament, cutting the at least one extrudate filament to a predetermined length to form a plurality of pellets, conveying the pellets to a separator/centrifugal dryer in water having a temperature of about 170° F. or greater, and separating the pellets from the water in the separator/centrifugal dryer so that the pellets are substantially dry upon removal from the separator/centrifugal dryer. The resultant pelletized plastic compound has a flex modulus of less than about 20,000 pounds per square inch (psi).

Claims (47)

1. A pellet formed by a method comprising the steps of:

dispersing from about 30% to about 95% by weight of thermoset rubber particles into a carrier resin to form a plastic compound, weight percent based on the total weight of the plastic compound, the carrier resin comprising an olefin block copolymer, wherein the olefin block copolymer comprises an ethylene-1-octene block copolymer and is present in the plastic compound in an amount of from about 5% to about 70% by weight based on the total weight of the plastic compound;

extruding the plastic compound through a die having at least one die hole to form at least one extrudate filament;

cutting the at least one extrudate filament to a predetermined length to form at least one pellet;

conveying the at least one pellet in water to a separator/centrifugal dryer, the water having a temperature of about 170° F. or greater; and

separating the at least one pellet from the water in the separator/centrifugal dryer, the at least one pellet substantially dry upon removal from the separator/centrifugal dryer, the pelletized plastic compound having a flex modulus of less than about 20,000 pounds per square inch (psi).

2. The pellet in accordance with claim 1 wherein the method further comprises the step of conveying the substantially dry at least one pellet to a storage container.

3. The pellet in accordance with claim 1 wherein the step of conveying the at least one pellet in water to a separator comprises conveying the at least one pellet to a separator in water having a temperature of about 170° F. to about 200° F.

4. The pellet in accordance with claim 1 wherein the thermoset rubber particles comprise at least one of neoprene rubber particles and ethylene-propylene-diene monomer (EPDM) rubber particles.

5. The pellet in accordance with claim 1 wherein the pelletized plastic compound has a flex modulus of less than about 12,000 psi.

6. A method of pelletizing a plastic compound, said method comprising:

dispersing from about 30% to about 95% by weight of thermoset rubber particles into a carrier resin to form the plastic compound, the carrier resin comprising an olefin block copolymer, wherein the olefin block copolymer comprises an ethylene-1-octene block copolymer and is present in the plastic compound in an amount of from about 5% to about 70% by weight based on the total weight of the plastic compound;

extruding the plastic compound through a die having at least one die hole to form at least one extrudate filament;

cutting the at least one extrudate filament to a predetermined length to form a plurality of pellets;

conveying the pellets to a separator/centrifugal dryer in water having a temperature of about 170° F. or greater; and

separating the pellets from the water in the separator/centrifugal dryer so that the pellets are substantially dry upon removal from the separator/centrifugal dryer, the pelletized plastic compound having a flex modulus of less than about 20,000 pounds per square inch (psi).

7. The method in accordance with claim 6 further comprising conveying the substantially dry pellets to a storage container.

8. The method in accordance with claim 6 wherein the water temperature is about 170° F. to about 200° F.

9. The method in accordance with claim 6 wherein the thermoset rubber particles comprise at least one of neoprene rubber particles and ethylene-propylene-diene monomer (EPDM) rubber particles.

10. The method in accordance with claim 6 wherein the pelletized plastic compound having a flex modulus of less than about 12,000 psi.

11. A pellet formed by a method comprising the steps of:

mixing from about 30% to about 95% by weight of thermoset rubber particles and a carrier resin together to form a plastic compound, weight percent based on the total weight of the plastic compound, the carrier resin comprising an olefin block copolymer, wherein the olefin block copolymer comprises an ethylene-1-octene block copolymer and is present in the plastic compound in an amount of from about 5% to about 70% by weight based on the total weight of the plastic compound;

directing the plastic compound into a pelletizer apparatus comprising a die and a knife blade;

extruding the plastic compound through the die to form an extrudate;

cutting the extrudate with the knife blade to form pellets of the plastic compound;

conveying the pellets to a separator/centrifugal dryer by a stream of water having a temperature of about 170° F. or greater; and

separating the pellets from the water in the separator/centrifugal dryer, the pellets substantially dry upon removal from the separator/centrifugal dryer, the pelletized plastic compound having a flex modulus of less than about 20,000 pounds per square inch (psi).

12. The pellet in accordance with claim 11 wherein the method further comprises the step of conveying the substantially dry pellets to a storage container.

13. The pellet in accordance with claim 11 wherein the step of conveying the pellets to a separator comprises conveying the pellets to a separator by a stream of water having a temperature of about 170° F. to about 200° F.

14. The pellet in accordance with claim 11 wherein the thermoset rubber particles comprise at least one of neoprene rubber particles and ethylene-propylene-diene monomer (EPDM) rubber particles.

15. The pellet in accordance with claim 11 wherein the pelletized plastic compound has a flex modulus of less than about 12,000 psi.

16. A method of pelletizing a plastic compound, said method comprising:

mixing from about 30% to about 95% by weight of thermoset rubber particles and a carrier resin together to form a plastic compound, weight percent based on the total weight of the plastic compound, the carrier resin comprising an olefin block copolymer, wherein the olefin block copolymer comprises an ethylene-1-octene block copolymer and is present in the plastic compound in an amount of from about 5% to about 70% by weight based on the total weight of the plastic compound;

directing the plastic compound into a pelletizer apparatus comprising a die and a knife blade;

extruding the plastic compound through the die to form an extrudate;

cutting the extrudate with the knife blade to form pellets of the plastic compound;

conveying the pellets to a separator/centrifugal dryer by a stream of water having a temperature of about 170° F. or greater; and

separating the pellets from the water in the separator/centrifugal dryer, the pellets substantially dry upon removal from the separator/centrifugal dryer, the pelletized plastic compound having a flex modulus of less than about 20,000 pounds per square inch (psi).

17. The method in accordance with claim 16 further comprising conveying the substantially dry pellets to a storage container.

18. The method in accordance with claim 16 wherein the water temperature is about 170° F. to about 200° F.

19. The method in accordance with claim 16 wherein the thermoset rubber particles comprise at least one of neoprene rubber particles and ethylene-propylene-diene monomer (EPDM) rubber particles.

20. The method in accordance with claim 16 wherein the pelletized plastic compound having a flex modulus of less than about 12,000 psi.

21. A pelletized plastic compound comprising:

a carrier resin; and

from about 30% to about 95% by weight of thermoset rubber particles dispersed into said carrier resin, weight percent based on the total weight of the plastic compound, said carrier resin comprising an olefin block copolymer, wherein said pelletized plastic compound has a flex modulus less than about 20,000 pounds per square inch (psi), and wherein the olefin block copolymer comprises an ethylene-1-octene block copolymer and is present in the plastic compound in an amount of from about 5% to about 70% by weight based on the total weight of the plastic compound.

22. The pelletized plastic compound in accordance with claim 21 wherein said thermoset rubber particles comprise at least one of neoprene rubber particles and ethylene-propylene-diene monomer (EPDM) rubber particles.

23. The pelletized plastic compound in accordance with claim 21 wherein said pelletized plastic compound has a flex modulus less than about 12,000 psi.

Assignments (14)
RELEASE OF SECURITY INTEREST Recorded May 7, 2021
From: BNP PARIBAS, AS COLLATERAL AGENT
To: SPARTECH LLC
Reel/Frame 056174/0836 →
CHANGE OF NAME Recorded Jul 13, 2020
From: POLYONE CORPORATION
To: AVIENT CORPORATION
Reel/Frame 053197/0141 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Dec 27, 2019
From: SPARTECH LLC
To: BNP PARIBAS, AS COLLATERAL AGENT
Reel/Frame 051431/0602 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT APPLICATION NUMBER 15/057724 PREVIOUSLY RECORDED ON REEL 043288 FRAME 0273. ASSIGNOR(S) HEREBY CONFIRMS THE PARTIAL RELEASE OF SECURITY INTEREST IN PATENTS. Recorded Oct 24, 2017
From: WELLS FARGO CAPITAL FINANCE, LLC, AS ADMINISTRATIVE AGENT
To: POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
Reel/Frame 044310/0989 →
PARTIAL RELEASE OF SECURITY INTERESTS IN PATENTS Recorded Jul 21, 2017
From: WELLS FARGO CAPITAL FINANCE, LLC, AS ADMINISTRATIVE AGENT
To: POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
Reel/Frame 043288/0273 →
NOTICE OF PARTIAL RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 21, 2017
From: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
Reel/Frame 043291/0827 →
RELEASE OF SECURITY INTEREST Recorded Jul 19, 2017
From: CITIBANK, N.A.
To: POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
Reel/Frame 043046/0137 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT APPLICATION NUMBER 14/501,050 PREVIOUSLY RECORDED ON REEL 037101 FRAME 0448. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT SECURITY AGREEMENT. Recorded Jan 27, 2016
From: POLYONE CORPORATION; COLORMATRIX HOLDINGS, INC.; POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 037603/0208 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT APPL. NO. 14/501,050 PREVIOUSLY RECORDED AT REEL: 037113 FRAME: 0144. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY AGREEMENT. Recorded Jan 7, 2016
From: POLYONE CORPORATION; COLORMATRIX HOLDINGS, INC.; POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
To: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 037508/0012 →
SECURITY AGREEMENT Recorded Nov 19, 2015
From: POLYONE CORPORATION; COLORMATRIX GROUP, INC.; COLORMATRIX HOLDINGS, INC.; THE COLORMATRIX CORPORATION; GAYSON SILICONE DISPERSIONS, INC.; POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
To: CITIBANK, N.A,, AS ADMINISTRATIVE AGENT
Reel/Frame 037146/0724 →
PATENT SECURITY AGREEMENT Recorded Nov 16, 2015
From: POLYONE CORPORATION; COLORMATRIX HOLDINGS, INC.; POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
To: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 037113/0144 →
SECURITY INTEREST Recorded Nov 12, 2015
From: POLYONE CORPORATION; COLORMATRIX HOLDINGS, INC.; POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 037101/0448 →
MERGER Recorded Feb 27, 2014
From: SPARTECH CORPORATION
To: POLYONE DESIGNED STRUCTURES AND SOLUTIONS LLC
Reel/Frame 032310/0933 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2011
From: HOWELL, GEORGE D.
To: SPARTECH CORPORATION
Reel/Frame 025773/0004 →