IP Library Granted Patent US 8,679,352
Granted Patent B2
US 8,679,352 · App. 13/050,931 · Granted Mar 25, 2014

Method and system for processing of aquatic species

Inventors: Laurent Olivier (Vero Beach, FL); Greg Havemann (Pearland, TX); Paul Antalik (Palm Bay, FL); Brandi Alderson (Melbourne, FL)
Assignee: PA LLC
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Quick Facts
Patent No.
US 8,679,352
App. No.
13/050,931
Granted
Mar 25, 2014
Kind
B2
Abstract

Disclosed herein is a method and system of recovering multiple products from industrial-scale production of a biomass of an aquatic species.

Claims (49)

1. A process of recovering multiple products from biomass of an aquatic species comprising:

providing the biomass;

lysing the biomass to generate a lysed biomass;

separating the lysed biomass to generate a juice and a first solid phase;

filtering the juice to generate a filtered juice and a second solid phase;

clarifying the filtered juice to generate a clarified juice and a third solid phase;

coagulating protein from the clarified juice to generate a broth comprising the wet protein concentrate;

separating the wet protein concentrate from the broth;

drying the wet protein concentrate to generate a dry protein concentrate;

producing a wet bio-crude using the first solid phase;

drying the wet bio-crude to generate at least one product selected from a dry bio-crude and a carbohydrate-rich meal;

wherein the multiple products comprise products selected from the dry protein concentrate, dry bio-crude, and carbohydrate-rich meal; and

wherein at least 50% of the protein in the multiple products is in the dry protein concentration.

2. The process of claim 1 , wherein the providing step comprises:

producing the biomass of an aquatic species on an industrial scale; and

harvesting the biomass.

3. The process of claim 1 , wherein the separating step comprises pressing the lysed biomass.

4. The process of claim 3 , wherein the pressing comprises using at least one of a belt press, a fan press, a rotary press, a screw press, a filter press, and finisher press.

5. The process of claim 1 , wherein at least one of: the first solid phase, the second solid phase, the third solid phase, and the broth, is/are used to recover the bio-crude and the carbohydrate-rich meal.

6. The process of claim 1 , wherein the aquatic species comprises a species of Lemna.

7. The process of claim 1 , wherein the lysing comprises using at least one of: a ball mill a colloid mill, a knife mill, a hammer mill, a grinding mill, a puree machine, and a filter press.

8. The process of claim 1 , wherein the juice comprises soluble protein.

9. The process of claim 1 comprising pressing at least one of the first solid phase, the second solid phase, or the third solid phase to generate a second juice and a bio-crude.

10. The process of claim 9 , wherein the second juice is combined with the juice.

11. The process of claim 9 , wherein the further pressing is carried out using a screw press.

12. The process of claim 9 , further comprising drying the bio-crude.

13. The process of claim 12 , wherein the drying is carried out using at least one of: a spin flash dryer, a spray dryer, a drum dryer, a flash dryer, a fluid bed dryer, a double drum dryer, and a rotary dryer.

14. The process of claim 1 , wherein the filtering is carried out using at least one of: a vibratory separator, a vibrating screen filter, a circular vibratory separator, a linear/inclined motion shaker, a decanter centrifuge, and a filter press.

15. The process of claim 14 , wherein the vibratory separator comprises at least one vibrating screen filter.

16. The process of claim 1 , wherein the clarifying comprises centrifuging and/or further filtration of the filtered juice.

17. The process of claim 16 , wherein the clarifying comprises use of at least one of a high-speed multi disc stack centrifuge, microfiltration and ultrafiltration.

18. The process of claim 1 , wherein the clarified juice is stored in a chilled storage tank.

19. The process of claim 1 , wherein the coagulating comprises lowering the pH of the clarified juice.

20. The process of claim 19 , wherein the pH is lowered to below about 6.

21. The process of claim 19 , wherein the pH is lowered to below about 5.

22. The process of claim 19 , wherein the pH is lowered to about 4.5.

23. The process of claim 19 , wherein lowering the pH comprises using at least one acid selected from hydrochloric acid, nitric acid, and sulfuric acid.

24. The process of claim 1 , wherein the coagulating is carried out using a precipitator comprising at least one heat exchanger.

25. The process of claim 24 , wherein the at least one heat exchanger comprises at least one plate, or tube or steam injection heat exchanger.

26. The process of claim 1 , wherein the coagulating comprises heating the clarified juice to a first temperature to generate a broth; and cooling the broth to a second temperature.

27. The process of claim 26 , wherein the first temperature is from about 40° C. to about 100° C.

28. The process of claim 26 , wherein the second temperature is below about 40° C.

29. The process of claim 26 , wherein the second temperature is below about 30° C.

30. The process of claim 1 , wherein the separating comprises using a high speed multi-disk stack centrifuge.

31. The process of claim 1 , wherein the wet protein concentrate is stored in a chilled storage tank.

32. The process of claim 1 , further comprising drying the wet protein concentrate to generate a dry protein concentrate.

33. The process of claim 32 , wherein the drying is carried out using a spray dryer, a drum dryer, spin flash dryer, a flash dryer, a fluid bed dryer, a double drum dryer, and a rotary dryer.

34. The process of claim 1 , further comprising contacting a material selected from the group consisting of the third solid phase and the clarified juice with at least one of: an alcohol, a solvent, or water, and with an acid catalyst, to form a mixture, separating the mixture into a liquid and a solid, whereby lipids and ash-forming components in the material are segregated into the liquid.

35. The process of claim 1 , further comprising, either before or directly after the lysing, washing the biomass using an aqueous solvent.

Assignments (11)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 15, 2026
From: LEMNATURE AQUAFARMS CORPORATION
To: LEMNA PRO LTD
Reel/Frame 074866/0259 →
CHANGE OF NAME Recorded Dec 19, 2022
From: PARABEL NUTRITION, INC.
To: LEMNATURE AQUAFARMS CORPORATION
Reel/Frame 062169/0842 →
CHANGE OF NAME Recorded Apr 14, 2020
From: PARABEL LTD.
To: PARABEL NUTRITION, INC.
Reel/Frame 052396/0163 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 29, 2014
From: OLIVIER, LAURENT
To: PA LLC
Reel/Frame 032083/0276 →
ASSET TRANSFER AGREEMENT Recorded May 10, 2013
From: PA LLC
To: PARABEL LTD.
Reel/Frame 030407/0701 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 19, 2013
From: PA LLC
To: PARABEL LTD.
Reel/Frame 030253/0024 →
SECURITY INTEREST Recorded Mar 15, 2013
From: PARABEL LTD.
To: DHABI CAYMAN ONE LIMITED
Reel/Frame 030115/0290 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jan 29, 2013
From: LV ADMINISTRATIVE SERVICES, INC.
To: PA LLC
Reel/Frame 029717/0703 →
SECURITY AGREEMENT Recorded Feb 16, 2012
From: PA LLC
To: LV ADMINISTRATIVE SERVICES, INC.
Reel/Frame 027727/0512 →
SECURITY AGREEMENT Recorded Feb 16, 2012
From: PA LLC
To: LV ADMINISTRATIVE SERVICES, INC.
Reel/Frame 027727/0561 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2011
From: HAVEMANN, GREGORY; ANTALIK, PAUL; ALDERSON, BRANDI
To: PA LLC
Reel/Frame 027167/0099 →
Continuity (2)
Provisional Application 61314736 · Mar 17, 2010
Related Publication 20120110901A1 · May 10, 2012