IP Library Granted Patent US 8,716,262
Granted Patent B2
US 8,716,262 · App. 12/645,765 · Granted May 6, 2014

Nucleoside phosphoramidates

Inventors: Michael Joseph Sofia (Doylestown, PA); Jinfa Du (New Hope, PA); Peiyuan Wang (Glen Rock, NJ); Dhanapalan Nagarathnam (Bethany, CT)
Assignee: Gilead Pharmasset LLC
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Quick Facts
Patent No.
US 8,716,262
App. No.
12/645,765
Granted
May 6, 2014
Kind
B2
Abstract

A nucleoside compound having activity against hepatitis C virus is disclosed.

Claims (42)

1. A compound represented by formula I, or its stereoisomers, salts, or pharmaceutically acceptable salts thereof:

wherein

Z is

R 1 is hydrogen or phenyl; R 2 is hydrogen; R 3a is hydrogen; R 3b is CH 3 ; R 4 is hydrogen, i Pr, or cyclopentyl; R 5 is hydrogen; R 6 is CH 3 ; X is F; R 8 is OMe, —N(—CH 2 CH 2 CH 2 —), OBn, or OH; and R 9 is NH 2 .

2. A pharmaceutical composition comprising a pharmaceutically acceptable medium and the compound according to claim 1 .

3. A method of treatment of a subject infected with a virus selected from the group consisting of hepatitis C virus, West Nile virus, yellow fever virus, dengue virus, rhinovirus, polio virus, hepatitis A virus, bovine viral diarrhea virus or Japanese encephalitis virus which comprises administering to the subject a therapeutically effective amount of the compound according to claim 1 .

4. The method of treatment according to claim 3 wherein the subject is infected with hepatitis C virus.

5. A method of treatment in a subject in need thereof, which comprises contacting at least one hepatitis C virus infected cell with at least one compound according to claim 1 .

6. A compound represented by formula I, or a stereoisomer thereof:

wherein

Z is

R 1 is hydrogen or phenyl; R 2 is hydrogen; R 3a is hydrogen; R 3b is CH 3 ; R 4 is hydrogen, i Pr, or cyclopentyl; R 5 is hydrogen; R 6 is CH 3 ; X is F; R 8 is OMe, —N(—CH 2 CH 2 CH 2 —), OBn, or OH; and R 9 is NH 2 .

7. A pharmaceutical composition comprising a pharmaceutically acceptable medium and the compound according to claim 6 .

8. A method of treatment of a subject infected with a virus selected from the group consisting of hepatitis C virus, West Nile virus, yellow fever virus, dengue virus, rhinovirus, polio virus, hepatitis A virus, bovine viral diarrhea virus or Japanese encephalitis virus which comprises administering to the subject a therapeutically effective amount of the compound according to claim 6 .

9. The method of treatment according to claim 8 wherein the subject is infected with hepatitis C virus.

10. A method of treatment in a subject in need thereof, which comprises contacting at least one hepatitis C virus infected cell with at least one compound according to claim 6 .

11. The compound of claim 1 wherein R 8 is OMe.

12. The compound of claim 11 wherein R 1 is phenyl.

13. The compound of claim 12 wherein R 4 is i Pr.

14. The compound of claim 12 wherein R 4 is cyclopentyl.

15. The compound of claim 12 wherein R 4 is hydrogen.

16. The compound of claim 11 wherein R 1 and R 4 are both hydrogen.

17. The compound of claim 1 wherein R 8 is OH.

18. The compound of claim 17 wherein R 1 is phenyl.

19. The compound of claim 18 wherein R 4 is i Pr.

20. The compound of claim 18 wherein R 4 is cyclopentyl.

21. The compound of claim 18 wherein R 4 is hydrogen.

22. The compound of claim 17 wherein R 1 and R 4 are both hydrogen.

23. A compound or its stereoisomer thereof selected from among

24. The compound of claim 23 or its stereoisomer thereof selected from among

25. A pharmaceutical composition comprising a pharmaceutically acceptable medium and the compound according to claim 11 .

26. A pharmaceutical composition comprising a pharmaceutically acceptable medium and the compound according to claim 17 .

27. A pharmaceutical composition comprising a pharmaceutically acceptable medium and the compound according to claim 23 .

28. A method of treatment of a subject infected with a virus selected from the group consisting of hepatitis C virus, West Nile virus, yellow fever virus, dengue virus, rhinovirus, polio virus, hepatitis A virus, bovine viral diarrhea virus or Japanese encephalitis virus which comprises administering to the subject a therapeutically effective amount of the compound according to claim 11 .

29. The method of treatment according to claim 28 wherein the subject is infected with hepatitis C virus.

30. A method of treatment in a subject in need thereof, which comprises contacting at least one hepatitis C virus infected cell with at least one compound according to claim 11 .

31. A method of treatment of a subject infected with a virus selected from the group consisting of hepatitis C virus, West Nile virus, yellow fever virus, dengue virus, rhinovirus, polio virus, hepatitis A virus, bovine viral diarrhea virus or Japanese encephalitis virus which comprises administering to the subject a therapeutically effective amount of the compound according to claim 17 .

32. The method of treatment according to claim 31 wherein the subject is infected with hepatitis C virus.

33. A method of treatment in a subject in need thereof, which comprises contacting at least one hepatitis C virus infected cell with at least one compound according to claim 17 .

34. A method of treatment of a subject infected with a virus selected from the group consisting of hepatitis C virus, West Nile virus, yellow fever virus, dengue virus, rhinovirus, polio virus, hepatitis A virus, bovine viral diarrhea virus or Japanese encephalitis virus which comprises administering to the subject a therapeutically effective amount of the compound according to claim 23 .

35. The method of treatment according to claim 34 wherein the subject is infected with hepatitis C virus.

36. A method of treatment in a subject in need thereof, which comprises contacting at least one hepatitis C virus infected cell with at least one compound according to claim 23 .

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 30, 2022
From: GILEAD PHARMASSET LLC
To: GILEAD SCIENCES, INC.
Reel/Frame 060218/0152 →
CHANGE OF NAME Recorded Apr 18, 2012
From: PHARMASSET, INC.
To: GILEAD PHARMASSET LLC
Reel/Frame 028070/0167 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 22, 2010
From: NAGARATHNAM, DHANAPALAN
To: PHARMASSET, INC.
Reel/Frame 024112/0294 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 19, 2010
From: SOFIA, MICHAEL JOSEPH; DU, JINFA; WANG, PEIYUAN
To: PHARMASSET, INC.
Reel/Frame 024110/0570 →
Continuity (2)
Provisional Application 61140423 · Dec 23, 2008
Related Publication 20110015146A1 · Jan 20, 2011