IP Library Granted Patent US 8,747,795
Granted Patent B2
US 8,747,795 · App. 13/430,362 · Granted Jun 10, 2014

Process for production of nickel carbonate

Inventors: Tiago Valentim Berni (Belo Horizonte, BR); Antonio Clareti Pereira (Belo Horizonte, BR); Felipe Hilario Guimar{hacek over (a)}es (Sào José da Lapa, BR)
Assignee: Vale S.A.
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Quick Facts
Patent No.
US 8,747,795
App. No.
13/430,362
Granted
Jun 10, 2014
Kind
B2
Abstract

Aspects of the present invention refers to a process for production of nickel carbonate including preparing a magnesium salt solution, contacting the solution with a stream of gaseous CO 2 , keeping pH between 4 and 10 and temperature between 0 and 100° C., during up to 5 hours to produce a first mixture, contacting the first mixture with a nickel sulphate solution to produce a second mixture, performing a separation of liquid and solid portions of the second mixture, and feeding the magnesium salt solution with the liquid portion. This process recycles the reagent used for producing nickel carbonate and yields a final product that is easy to handle and transport.

Claims (10)

1. A process for production of nickel carbonate comprising the following steps:

a) preparing a magnesium salt solution;

b) contacting said solution with a stream of gaseous CO 2 while keeping a pH between 4 and 10 and a temperature between 0 and 100° C. during up to 5 hours to produce a first mixture;

c) contacting the first mixture with a nickel sulphate solution to produce a second mixture;

d) performing a separation of liquid and solid portions of said second mixture;

e) feeding step a) with said liquid portion.

2. The process according to claim 1 , wherein the magnesium salt solution is a magnesium sulphate solution.

3. The process according to claim 1 , wherein the contacting of the magnesium salt solution with a stream of gaseous CO 2 occurs in a packet column.

4. The process according to claim 1 , further comprising using a neutralizing agent in step b to the keep pH between 4 and 10.

5. The process according to claim 4 , wherein the neutralizing agent is magnesium oxide.

Assignments (2)
CHANGE OF ADDRESS Recorded Sep 13, 2017
From: VALE S.A.
To: VALE S.A.
Reel/Frame 043849/0613 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 17, 2012
From: BERNI, TIAGO V.; PEREIRA, ANTONIO C.; GUIMARAES, FELIPE H.
To: VALE S/A
Reel/Frame 028571/0817 →
Continuity (2)
Provisional Application 61467683 · Mar 25, 2011
Related Publication 20120269713A1 · Oct 25, 2012