Method for transferring graphene using a hot press
The present invention relates to a method for transferring graphene using a hot press, comprising: a step of contacting graphene, having a thermal-releasable sheet attached thereto, with a target substrate; and a step of pressing and heating the graphene having the thermal-releasable sheet attached thereto and the target substrate using the upper press and lower press of a hot press so as to separate the thermal-releasable sheet and the graphene and transfer the separated graphene to the target substrate. The present invention also relates to a graphene-transfer hot press apparatus for said transfer process.
1. A graphene transferring method, comprising:
making contact of graphene to which a thermal-releasable sheet is attached with a target substrate;
separating the thermal-releasable sheet from the graphene and transferring the separated graphene onto the target substrate at the same time by pressurizing and heating the graphene to which the thermal-releasable sheet is attached and the target substrate in between a first press and a second press opposite the first press;
wherein the target substrate is adhered to the second press during the transferring of the graphene, by a vacuum atmosphere formed by a plurality of vacuum lines in the second press to prevent the target substrate from slipping on the second press;
wherein temperatures of heat generated by the first press and the second press are independently controlled; and
wherein the thermal-releasable sheet includes viscous resin.
2. The graphene transferring method of claim 1 , wherein the thermal-releasable sheet is released in a range of from about 90° C. to about 150° C.
3. The graphene transferring method of claim 1 , wherein the target substrate includes a flexible substrate or a rigid substrate.
4. The graphene transferring method of claim 3 , wherein the rigid substrate includes what is selected from the group consisting of a glass substrate, an ITO substrate, a Si substrate, a SiO2 substrate, a metal substrate, and combinations thereof.
5. The graphene transferring method of claim 3 , wherein the flexible substrate includes what is selected from the group consisting of polyethylene terephthalate (PET), polyimide, polyethylene naphthalate (PEN), polycarbonate (PC), an elastomer polymer, and combinations thereof.
6. The graphene transferring method of claim 5 , wherein the elastomer polymer includes polydimethylsiloxane (PDMS), poly (methylmethacrylate) (PMMA), or silicone rubber.
7. The graphene transferring method of claim 1 , wherein a temperature of the heating is in a range of from about 80° C. to about 200° C.
8. The graphene transferring method of claim 1 , wherein during the heating process, a temperature of the first press is equal to or different from a temperature of the second press.
9. The graphene transferring method of claim 1 , wherein during the pressurizing process, a pressure is in a range of from about 300 psi to about 2,000 psi.
10. The graphene transferring method of claim 1 , wherein the graphene is formed by supplying a reaction gas containing a carbon source and heat onto the target substrate and making a reaction therebetween.
11. The graphene transferring method of claim 1 , further including:
after the transferring of the separated graphene onto the target substrate, washing the transferred graphene.
12. The graphene transferring method of claim 1 , wherein the graphene to which the thermal-releasable sheet is attached includes one or more layers of graphene.
13. The graphene transferring method of claim 1 , further comprising:
forming a vacuum atmosphere between the thermal-releasable sheet and the first press, so that the thermal-releasable sheet is adhered to the first press during the separating of the thermal-releasable sheet from the graphene.
14. The graphene transferring method of claim 1 , wherein the graphene is heated by heat generated by the first press and the second press.