IP Library Granted Patent US 9,155,251
Granted Patent B2
US 9,155,251 · App. 13/776,970 · Granted Oct 13, 2015

Producing method for the artificial peat moss from natural cellulose fiber

Inventors: Wen-Tung Chou (Changhua County, TW); Ming-Yi Lai (Changhua County, TW); Kun-Shan Huang (Tainan, TW)
Assignee: ACELON CHEMICAL AND FIBER CORPORATION
A01G1/001D01D1/02D01D5/06D01D5/26D01D10/02D01D10/06D01F1/02D01F1/10D01F2/00D01F2/02D02G1/02D02G1/0206
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Quick Facts
Patent No.
US 9,155,251
App. No.
13/776,970
Granted
Oct 13, 2015
Kind
B2
Abstract

The present invention provides a producing method for the artificial peat moss from natural cellulose fiber. The producing method comprises following steps in successive order manner. Firstly, blend natural pulp with N-methylmorpholine N-oxide (NMMO) as dissolving solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as stabilizer in proper mixing ratio to yield a preliminary quasi-dope. Secondly, stir and dehydrate the preliminary quasi-dope to form dope. Thirdly, spin the dope by dry jet wet spinning method to yield filament bundle of cellulose. Fourthly, orderly perform coagulating with regenerating, water rinsing, twisting with plying and cutting processes on the filament bundle of cellulose to yield a preliminary artificial peat moss of natural cellulose fiber. Finally, per drying process of post-treatment on the preliminary artificial peat moss of natural cellulose fiber to obtain final artificial peat moss of natural cellulose fiber of the present invention.

Claims (20)

1. A method for producing an artificial peat moss from natural cellulose fiber comprising the following steps in successive order:

(a) producing a preliminary quasi-dope of mixed cellulose mucilage by combining a wood pulp with a dissolving solvent and a stabilizer, wherein the dissolving solvent is N-methylmorpholine N-oxide (NMMO) and the stabilizer is 1, 3-phenylene-bis 2-oxazoline (BOX);

(b) blending and dissolving the preliminary quasi-dope of mixed cellulose mucilage of step (a) by stirring the preliminary quasi-dope of mixed cellulose mucilage at a temperature of 50° C.-70° C. in a high speed agitator;

(c) producing a homogenized mucilaginous dope by dehydrating the blended and dissolved preliminary quasi-dope of mixed cellulose mucilage of step (b) in a vacuum film evaporator at a temperature of 80° C.-120° C. for 5 minutes;

(d) producing a filament bundle of cellulose by feeding the homogenized mucilaginous dope of step (c) into a spinning machine via a metering pump, then spinning the homogenized mucilaginous dope and using a dry-jet wet spinning method to extrude the homogenized mucilaginous dope from the spinneret;

(e) producing a plurality of spinning tows each comprising an untwisted bundle of continuous filaments of about 2,500 deniers by coagulating the filament bundle of cellulose of step (d) in a coagulation bath then rinsing the coagulated filament bundle of cellulose with water; and

(f) producing the artificial peat moss by twisting, calendering and cutting the plurality of spinning tows of step (e) using the following sub-steps:

(i) plying the plurality of spinning tows with a cover filament thereby preventing de-twisting of the spinning tows in subsequent sub-steps;

(ii) forming a spun yarn of 25,000-30,000 deniers by laterally feeding the plurality of spinning tows of sub-step (i) into a hollow spindle and twisting the spindle, wherein the hollow spindle is twisted at a speed of 1,800-10,800 rpm thereby regulating the amount of twist to 200-1,200 twists per meter (TPM);

(iii) calendering the spun yarn of substep (ii) by passing the spun yarn through calender rollers; and

(iv) forming the artificial peat moss by cutting the calendered spun yarn of substep (iii) with a cutter.

2. The method of claim 1 , wherein the method comprises an additional step (g) as follows:

(g) drying the artificial peat moss of step (f) by heating the artificial peat moss in a drum dryer at a temperature of 120° C.-15° C. for 30-60 minutes.

3. The method of claim 1 , wherein the concentration of the N-methylmorpholine N-oxide (NMMO) in step (a) is 45-75%.

4. The method of claim 1 , wherein the pH of the artificial peat moss is 6.0-7.2.

5. The method of claim 1 , wherein the Electrical Conductivity (EC) value of the artificial peat is lower than the EC value of natural sphagnum moss.

6. The method of claim 1 , wherein the wood pulp comprises pulp cellulose of short staple or long filament with an a-cellulose content of over 65% and a degree of polymerization (DP) of 500-1200.

7. The method of claim 1 , wherein step (c) decreases the water content of the blended and dissolved preliminary quasi-dope of mixed cellulose mucilage of step (b) by 5%-13%.

8. The method of claim 1 , wherein in step (f) the feeding frequencies for the calender rollers and the cutter are adjusted so that so the length of the artificial peat moss is 3cm - 30 cm.

9. The method of claim 1 , wherein the hollow spindle of step (f) is driven by a high-speed motor by using a cog belt or toothed belt to couple the hollow spindle to the high-speed motor.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 30, 2020
From: ACELON CHEMICALS AND FIBER CORPORATION
To: LIN, CHIH-HSIN
Reel/Frame 053930/0946 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2013
From: CHOU, WEN-TUNG; LAI, MING-YI; HUANG, KUN-SHAN
To: ACELON CHEMICAL AND FIBER CORPORATION
Reel/Frame 029875/0280 →
Priority Claims (1)
TW 101147471 A · Dec 14, 2012 · national
Continuity (1)
Related Publication 20140165463A1 · Jun 19, 2014