IP Library Patent Application 10983202
Patent Application
App. No. 10/983,202

Propranolol formulations

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Quick Facts
Patent No.
US None
App. No.
10/983,202
Filed
Nov 5, 2004
Art Unit
1615
USPC
424/469
Abstract

Controlled-release propranolol formulations comprise a core comprising a pharmaceutically acceptable propranolol salt and an inert core; and a coating disposed on the core, the coating comprising about 70:30 to about 85:15 of ethylcellulose:polyvinylpyrrolidone or about 60:40 to about 75:25 of ethylcellulose:hydroxypropylmethylcellulose.

Claims (41)

1 . A composition comprising:

a core comprising a pharmaceutically acceptable propranolol salt disposed on an inert core; and

a coating disposed on the core, the coating comprising about 70:30 to about 85:15 of ethylcellulose:polyvinylpyrrolidone, or about 60:40 to about 75:25 of ethylcellulose:hydroxypropylmethylcellulose.

2 . The composition of claim 1 , wherein the inert core comprises a sugar sphere having a diameter of about 500 to about 710 micrometers.

3 . The composition of claim 1 , wherein the coating comprises 10 wt % to about 17 wt % of the total weight of the coated cores.

4 . The composition of claim 1 , wherein the coating comprises about 12 wt % to about 15 wt % of the total weight of the coated cores.

5 . The composition of claim I, wherein the coating comprises ethylcellulose having a viscosity of 5 cps to about 20 cps at 20° C. and polyvinylpyrrolidone having a viscosity of about 5.5 to 8.5 cps at 20° C.

6 . The composition of claim 1 , wherein the coating comprises ethylcellulose having a viscosity of 5 cps to about 20 cps at 20° C. and hydroxypropylmethylcellulose having a viscosity of about 5 to about 18 cps at 20° C.

7 . The composition of claim 1 , exhibiting a dissolution profile in a pH 6.8 medium such that:

less than 10 wt % of the propranolol is released at 1 hour;

39 wt % to 69 wt % of the propranolol is released at 6 hours; and

greater than 80 wt % of the propranolol is released at 15 hours.

8 . The composition of claim 1 , exhibiting a dissolution profile in a pH 6.8 medium such that:

less than 10 wt % of the propranolol is released at 1 hour;

44 wt % to 64 wt % of the propranolol is released at 6 hours; and

greater than 80 wt % of the propranolol is released at 15 hours.

9 . The composition of claim 1 , exhibiting a dissolution profile in 0.1 M HCl such that:

less than 10 wt % of the propranolol is released at 1 hour;

35 wt % to 65 wt % of the propranolol is released at 6 hours; and

greater than 80 wt % of the propranolol is released at 15 hours.

10 . The composition of claim 1 , exhibiting a dissolution profile in 0.1 M HCl such that:

less than 10 wt % of the propranolol is released at 1 hour;

40 wt % to 60 wt % of the propranolol is released at 6 hours; and

greater than 80 wt % of the propranolol is released at 15 hours.

11 . The composition of claim 1 , wherein the coated core comprises no added organic acid.

12 . A dosage form comprising:

a core comprising a pharmaceutically acceptable propranolol salt disposed on an inert core; and

a coating disposed on the core, the coating comprising hydroxypropylmethylcellulose, polyvinylpyrrolidone, or a combination thereof; and ethylcellulose;

wherein the dosage form comprises one type of controlled-release coated core; and

wherein the average C max of the dosage form is about 105 ng/mL to about 270 ng/mL and the average AUC 0-∞ of the dosage form is about 2100 ng hr/mL to about 5400 ng hr/mL when measured under fasting conditions, or

wherein the average C max of the dosage form is about 70 ng/mL to about 216 ng/mL and the average AUC 0-∞ of the dosage form is about 1400 ng hr/mL to about 4725 ng hr/mL when measure under fed conditions.

13 . The dosage form of claim 12 , wherein the coating comprises about 70:30 to about 85:15 of ethylcellulose:polyvinylpyrrolidone.

14 . The dosage form of claim 12 , wherein the coating comprises about 60:40 to about 75:25 of ethylcellulose:hydroxypropylmethylcellulose.

15 . The dosage form of claim 12 , wherein the ethylcellulose has a viscosity of 5 cps to about 20 cps at 20° C. and the polyvinylpyrrolidone has a viscosity of about 5.5 to 8.5 cps at 20° C.

16 . The dosage form of claim 12 , wherein the coating comprises about 60 wt % to about 75 wt % of ethylcellulose and about 25 wt % to about 40 wt % of hydroxypropylmethylcellulose.

17 . The dosage form of claim 16 , wherein the coating comprises ethylcellulose having a viscosity of 5 cps to about 20 cps at 20° C. and hydroxypropylmethylcellulose having a viscosity of about 5 to about 18 cps at 20° C.

18 . The dosage form of claim 12 , wherein the coated core comprises no added organic acid.

19 . The dosage form of claim 12 , wherein the dosage form comprises a capsule.

20 . A method of treating a human, comprising administering a pharmaceutically effective amount of the dosage form of claim 13 to a human in need of treatment for angina, cardiac arrhythmia, or hypertension.

21 . The method of claim 20 , wherein the coated core comprises no added organic acid.

22 . The method of claim 20 , wherein the dosage form comprises a capsule.

Assignments (8)
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Nov 1, 2012
From: DEUTSCHE BANK AG, LONDON BRANCH
To: ACTAVIS GROUP PTC EHF
Reel/Frame 029227/0314 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Nov 1, 2012
From: DEUTSCHE BANK AG, LONDON BRANCH
To: ACTAVIS GROUP HF
Reel/Frame 029229/0470 →
PATENT SECURITY AGREEMENT SUPPLEMENT Recorded Dec 10, 2010
From: ACTAVIS GROUP PTC EHF.
To: DEUTSCHE BANK AG, LONDON BRANCH
Reel/Frame 025463/0758 →
GRANT OF SECURITY INTEREST Recorded Nov 28, 2007
From: ACTAVIS GROUP HF, A PUBLIC LIMITED COMPANY
To: DEUTSCHE BANK AG, LONDON BRANCH, AS SECURITY AGENT
Reel/Frame 020166/0803 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2007
From: BANK OF AMERICA, N.A.
To: ALPHARMA INC.
Reel/Frame 020107/0037 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2006
From: ALPHARMA INC.
To: ACTAVIS GROUP HF
Reel/Frame 017691/0757 →
SECURITY AGREEMENT Recorded Nov 21, 2005
From: ALPHARMA INC.
To: BANK OF AMERICA, N.A., AS AGENT
Reel/Frame 016800/0358 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 8, 2004
From: HEINICKE, GRANT
To: ALPHARMA, INC.
Reel/Frame 015435/0329 →