IP Library Patent Application 11001609
Patent Application
App. No. 11/001,609

Galantamine formulations

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Quick Facts
Patent No.
US None
App. No.
11/001,609
Filed
Dec 1, 2004
Art Unit
1618
USPC
424/464
Abstract

Galantamine formulations substantially free of microcrystalline cellulose, lactose, and/or starch are described.

Claims (52)

1 . A pharmaceutical solid dosage formulation, comprising:

galantamine or a pharmaceutically acceptable salt thereof; and

a pharmaceutically acceptable excipient, with the proviso that the formulation does not contain microcrystalline cellulose; and

wherein the formulation exhibits a dissolution profile such that after 10 minutes at least about 90% of the galantamine or galantamine salt is released after combining the dosage formulation with 500 ml of purified water at 37° C. in Apparatus 2 (USP, <711> Dissolution, paddle, 50 rpm).

2 . The formulation of claim 1 , wherein the galantamine salt is galantamine hydrobromide.

3 . The formulation of claim 1 , wherein the excipient is selected from the group consisting of lactose-based material; cellulosic material, excluding microcrystalline cellulose; starch; sugar; sugar alcohol; saccharide; polysaccharide; dibasic calcium phosphate, calcium sulfate, and combinations thereof.

4 . The formulation of claim 1 , further comprising a disintegrant.

5 . The formulation of claim 4 , wherein the disintegrant is selected from the group consisting of partially pregelatinized starch, pregelatinized starch, polyvinylpyrrolidone, croscarmellose, croscarmellose sodium, sodium starch glycolate, crospovidone, and combinations thereof.

6 . The formulation of claim 1 , wherein the formulation provides an AUC after administration that is more than 80 percent and less than 120 percent of the AUC provided between 0 and 24 hours after administration by the same strength dosage form of galantamine hydrobromide

wherein the same strength dosage form of galantamine hydrobromide comprises colloidal silicon dioxide in a weight ratio to galantamine hydrobromide of about 0.0234:1,

crospovidone in a weight ratio to galantamine hydrobromide of about 0.585:1,

hydroxypropyl methylcellulose in a weight ratio to galantamine hydrobromide of about 0.488:1,

lactose monohydrate in a weight ratio to galantamine hydrobromide of about 7.53:1,

magnesium stearate in a weight ratio to galantamine hydrobromide of about 0.0585:1,

microcrystalline cellulose in a weight ratio to galantamine hydrobromide of about 2.51:1,

propylene glycol in a weight ratio to galantamine hydrobromide of about 0.188:1,

talc in a weight ratio to galantamine hydrobromide of about 0.0975:1, and titanium dioxide in a weight ratio to galantamine hydrobromide of about 0.146:1.

7 . A tablet comprising the formulation of claim 1 .

8 . The tablet of claim 7 , further comprising a film coating disposed on the surface of the tablet.

9 . A pharmaceutical solid dosage formulation, comprising:

galantamine or a pharmaceutically acceptable salt thereof; and

a pharmaceutically acceptable excipient,

with the proviso that the solid dosage formulation, excluding an optional coating disposed on the solid dosage formulation,

i) does not contain a cellulosic material, or

ii) does not contain starch.

10 . The formulation of claim 9 , wherein the galantamine salt is galantamine hydrobromide.

11 . The formulation of claim 9 , wherein the excipient is selected from the group consisting of lactose-based material; sugar; sugar alcohol; saccharide; polysaccharide; dibasic calcium phosphate, calcium sulfate, and combinations thereof.

12 . The formulation of claim 9 , further comprising a disintegrant.

13 . The formulation of claim 12 , wherein the disintegrant is selected from the group consisting of polyvinylpyrrolidone, croscarmellose, croscarmellose sodium, crospovidone, and combinations thereof.

14 . A tablet comprising the formulation of claim 9 .

15 . An immediate release solid pharmaceutical dosage formulation, comprising:

galantamine or a pharmaceutically acceptable salt thereof; and

a pharmaceutically acceptable excipient, with the proviso that the formulation does not contain a lactose-based material and wherein the formulation is directly compressible.

16 . The formulation of claim 15 , wherein the galantamine salt is galantamine hydrobromide.

17 . The formulation of claim 16 , wherein the excipient is selected from the group consisting of cellulosic material, excluding microcrystalline cellulose; starch; sugar; sugar alcohol; saccharide; polysaccharide; dibasic calcium phosphate, calcium sulfate, and combinations thereof.

18 . The formulation of claim 15 , further comprising a disintegrant.

19 . A tablet comprising the formulation of claim 15 .

20 . A process of preparing a pharmaceutical solid dosage formulation, comprising:

blending galantamine or a pharmaceutically acceptable salt thereof with an excipient and disintegrant to form a preblend;

blending the preblend with a glidant and optional additives to form a blend; and

forming the blend into tablets using direct compression; wherein the solid dosage formulation is free of an excipient selected from the group consisting of microcrystalline cellulose, lactose, starch, and combinations thereof.

21 . The process of claim 20 , further comprising blending the preblend with a an excipient to form an intermediate blend that is then blended with the glidant.

22 . A pharmaceutical solid dosage formulation, comprising:

(a) galantamine hydrobromide;

(b) lactose-based excipient; and

(c) crospovidone, partially pregelatinized maize starch or a combination of the foregoing; and wherein the solid dosage formulation is free of microcrystalline cellulose.

23 . The formulation of claim 22 , wherein the lactose-based excipient comprises lactose impalpable and spray dried lactose monohydrate.

24 . A tablet comprising the formulation of claim 22 .

25 . A method of treating a patient with Alzheimer's disease, comprising orally administering a therapeutically effective amount of the formulation of claim 1 to a patient.

26 . A method of treating a patient with Alzheimer's disease, comprising orally administering a therapeutically effective amount of the formulation of claim 9 to a patient.

27 . A method of treating a patient with Alzheimer's disease, comprising orally administering a therapeutically effective amount of the formulation of claim 15 to a patient.

28 . A method of treating a patient with Alzheimer's disease, comprising orally administering a therapeutically effective amount of the formulation of claim 22 to a patient.

Assignments (8)
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Nov 1, 2012
From: DEUTSCHE BANK AG, LONDON BRANCH
To: ACTAVIS GROUP PTC EHF
Reel/Frame 029227/0314 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Nov 1, 2012
From: DEUTSCHE BANK AG, LONDON BRANCH
To: ACTAVIS GROUP HF
Reel/Frame 029229/0470 →
PATENT SECURITY AGREEMENT SUPPLEMENT Recorded Dec 10, 2010
From: ACTAVIS GROUP PTC EHF.
To: DEUTSCHE BANK AG, LONDON BRANCH
Reel/Frame 025463/0758 →
GRANT OF SECURITY INTEREST Recorded Nov 28, 2007
From: ACTAVIS GROUP HF, A PUBLIC LIMITED COMPANY
To: DEUTSCHE BANK AG, LONDON BRANCH, AS SECURITY AGENT
Reel/Frame 020166/0803 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2007
From: BANK OF AMERICA, N.A.
To: ALPHARMA INC.
Reel/Frame 020107/0037 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2006
From: ALPHARMA INC.
To: ACTAVIS GROUP HF
Reel/Frame 017691/0757 →
SECURITY AGREEMENT Recorded Nov 21, 2005
From: ALPHARMA INC.
To: BANK OF AMERICA, N.A., AS AGENT
Reel/Frame 016800/0358 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2004
From: TANG, LIJUAN; BOEHM, GARTH; DUNDON, JOSEPHINE
To: ALPHARMA, INC.
Reel/Frame 016055/0175 →