IP Library Granted Patent US 7,919,291
Granted Patent B2
US 7,919,291 · App. 12/405,125 · Granted Apr 5, 2011

Method for producing ethanol using raw starch

Assignee: Poet Research, Inc.
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Quick Facts
Patent No.
US 7,919,291
App. No.
12/405,125
Granted
Apr 5, 2011
Kind
B2
Abstract

The present invention relates to methods for producing high levels of alcohol during fermentation of plant material, and to the high alcohol beer produced. The present invention also relates to methods for producing high protein distiller's dried grain from fermentation of plant material, and to the high protein distiller's dried grain produced. The present invention further relates to reduced stack emissions from drying distillation products from the production of ethanol.

Claims (20)

1. A method for producing ethanol from ground corn which method comprises:

providing an aqueous composition comprising ground corn sized such that more than 50% of the ground corn passes through a 0.5 mm screen, an fungal acid amylase and a glucoamylase under conditions which produce glucose including a pH of 3 to 6, a temperature of 25° C. to 40° C., and a solids content 20 to 50 weight percent; and

fermenting the glucose in the presence of a yeast and in the absence of added protease, under conditions which produce ethanol wherein said conditions include a pH of 3 to 6 and maintaining a glucose concentration in the aqueous composition of less than 1 weight percent after 12 hours of saccharification and fermentation, wherein said method produces at least 18 volume percent ethanol.

2. The method of claim 1 , wherein the aqueous composition of ground corn, fungal acid amylase and glucoamylase is maintained at a pH of from about 4.0 to 5.0.

3. The method of claim 1 , wherein the amount of said fungal acid amylase to dry solids in said composition ranges from about 0.1 to about 10 fungal acid amylase units per gram of said dry solids.

4. The method of claim 3 , wherein the amount of said glucoamylase to dry solids in said composition ranges from about 0.5 to about 6 glucoamylase units per gram of said dry solids.

5. A method for producing ethanol from ground corn which method comprises:

providing an aqueous composition comprising ground corn sized such that the ground corn passes through a 0.5 mm screen, an fungal acid amylase and a glucoamylase under conditions which produce glucose including a pH of 3 to 6, a temperature of 25° C. to 40° C., and a solids content of 20 to 50 weight percent; and

fermenting the glucose in the presence of a yeast and in the absence of added protease, under conditions which produce ethanol wherein said conditions include a pH of 3 to 6 and maintaining a glucose concentration in the aqueous composition of less than about 2 weight percent;

wherein the production of glucose and the fermentation of glucose to ethanol is conducted in a simultaneous process, and further wherein said method produces at least 18 volume percent ethanol.

6. The method of claim 5 , wherein the aqueous composition of ground corn, fungal acid amylase and glucoamylase is maintained at a pH of from about 4.0 to 5.0.

7. The method of claim 5 , wherein the amount of said fungal acid amylase to dry solids in said composition ranges from about 0.1 to about 10 fungal acid amylase units per gram of said dry solids.

8. The method of claim 5 , wherein the glucose concentration during fermentation is maintained at less than about 1 weight percent.

9. The method of claim 5 , wherein during the production of ethanol, the pH is maintained at 3-4.5 during the first half of the fill cycle and at 4.5-6.0 during the second half of the fill cycle.

10. The method of claim 7 , wherein the amount of said glucoamylase to dry solids in said composition ranges from about 0.5 to about 6 glucoamylase units per gram of said dry solids.

11. A method for producing ethanol from ground corn which method comprises:

providing an aqueous composition comprising ground corn sized such that the ground corn passes through a 0.5 mm screen, an fungal acid amylase and a glucoamylase under conditions which produce glucose wherein said conditions include a pH of 3 to 6, a temperature of 30° C. to 35° C., a solids content of 25 to 45 weight percent, an amount of said fungal amylase to dry solids in said composition which is between 0.1 and 10 fungal acid amylase units per gram of said dry solids, and an amount of said glucoamylase to dry solids in said composition which is between 0.5 and 6 glucoamylase units per gram of said dry solids; and

fermenting the glucose in the presence of a yeast and in the absence of added protease, under conditions which produce ethanol wherein said conditions comprise an initial temperature of about 35° C. which temperature is decreased during fermentation to a temperature of about 30° C., and maintaining a glucose concentration in the aqueous composition of less than 2 weight percent after 12 hours of saccharification and fermentation wherein the production of glucose and the fermentation of glucose to ethanol is conducted in a simultaneous process, and further wherein said method produces at least 18 volume percent ethanol.

12. The process of claim 11 , wherein said process is a continuous process.

13. The process of claim 11 , wherein said process is conducted for about 48 to 96 hours.

Assignments (8)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2021
From: LEWIS, STEPHEN M.; VAN HULZEN, SHON ERRON; FINCK, JOHN MICHAEL; ROTH, DEBBIE LYNN
To: BROIN AND ASSOCIATES
Reel/Frame 058086/0656 →
SECURITY INTEREST Recorded Apr 3, 2020
From: POET RESEARCH, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 052312/0801 →
SECURITY INTEREST Recorded Apr 2, 2020
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052295/0712 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 035603/0778 Recorded Apr 2, 2020
From: JPMORGAN CHASE BANK N.A., AS ADMINISTRATIVE AGENT
To: POET, LLC; POET RESEARCH, INC.; POET PLANT MANAGEMENT, LLC; POET INVESTMENTS, INC.; POET BIOMASS, LLC; POET DESIGN AND CONSTRUCTION, INC.; RISK MANAGEMENT ASSOCIATES, INC.; POET NUTRITION, INC.; POET RESEARCH CENTER, LLC (FORMERLY KNOWN AS POET RESEARCH CENTER, INC.); POET LEASING, LLC; POET NUTRITION INTERNATIONAL, INC.
Reel/Frame 052299/0676 →
RELEASE OF PATENT, TRADEMARK AND COPYRIGHT SECURITY INTEREST Recorded May 6, 2015
From: BOKF, N.A., DBA BANK OF OKLAHOMA
To: POET RESEARCH, INC. F/K/A BROIN AND ASSOCIATES, INC.; POET, LLC F/K/A BROIN COMPANIES, LLC; POET INVESTMENTS, INC. F/K/A BROIN ENTERPRISES, INC.; POET PLANT MANAGEMENT, LLC
Reel/Frame 035603/0610 →
ACKNOWLEDGEMENT OF SECURITY INTEREST IN PATENTS Recorded May 6, 2015
From: POET, LLC; POET RESEARCH, INC.; POET PLANT MANAGEMENT, LLC; POET INVESTMENTS, INC.; POET BIOMASS, LLC; POET DESIGN AND CONSTRUCTION, INC.; RISK MANAGEMENT ASSOCIATES, INC.; POET NUTRITION, INC.; POET RESEARCH CENTER, INC.; POET LEASING, LLC; POET NUTRITION INTERNATIONAL, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 035603/0778 →
SECURITY AGREEMENT Recorded Feb 11, 2011
From: POET RESEARCH, INC.
To: BOKF, NA, D/B/A BANK OF OKLAHOMA
Reel/Frame 025783/0430 →
CHANGE OF NAME Recorded May 12, 2010
From: BROIN AND ASSOCIATES, INC.
To: POET RESEARCH, INC.
Reel/Frame 024376/0418 →
Continuity (4)
Continuation 11676965 · Feb 20, 2007
Continuation 10798226 · Mar 10, 2004
Provisional Application 60453442 · Mar 10, 2003
Related Publication 20100041116A1 · Feb 18, 2010