IP Library Granted Patent US 8,088,251
Granted Patent B2
US 8,088,251 · App. 12/445,590 · Granted Jan 3, 2012

Process for improving paper strength

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Quick Facts
Patent No.
US 8,088,251
App. No.
12/445,590
Granted
Jan 3, 2012
Kind
B2
Abstract

The present invention provides a process for preparing a paper or paper board of improved strength which comprises the steps of i) providing a cellulosic thick stock, ii) diluting the thick stock of step i) to form a thin stock, iii) draining the thin stock of step ii) on a wire to form a web, and iv) drying the web of step iii) to form paper or paper board, wherein the cellulosic thick stock of step (i) comprises organic polymeric microparticles, as well as paper obtainable by above process.

Claims (22)

1. A process for preparing a paper or paper board which comprises the steps of:

i) providing a cellulosic thick stock,

ii) diluting the thick stock of step i) to form a thin stock,

iii) draining the thin stock of step ii) on a wire to form a web, and

iv) drying the web of step iii) to form paper or paper board,

wherein the cellulosic thick stock of step (i) comprises anionic organic polymeric microparticles,

wherein the organic polymeric microparticles are formed from a composition comprising at least one acrylic anionic monomer and at least one acrylic non-ionic monomer,

wherein the acrylic non-ionic monomer is at least one of (meth)acrylamide; an N—C 1-4 -alkyl (meth)acrylamide; an N,N-di(C 1-4 -alkyl) (meth)acrylamide; or a C 1-4 -alkyl(meth)acrylate, and

the acrylic anionic monomer is at least one of (meth)acrylic acid; 2-acrylamido-2-methyl-1-propanesulfonic acid; or salts thereof, and

wherein the acrylic anionic monomer and the acrylic non-ionic monomer are present in the composition in a weight ratio of 80/20 to 20/80.

2. The process of claim 1 , wherein the polymeric microparticles are formed in the presence of a cross-linking agent.

3. The process of claim 1 , wherein the weight ratio of acrylic anionic monomer/acrylic non-ionic monomer is 70/30 to 50/50.

4. The process of claim 1 , wherein the acrylic non-ionic monomer is (meth)acrylamide.

5. The process of claim 4 , wherein the acrylic non-ionic monomer is acrylamide.

6. The process of claim 1 , wherein the acrylic anionic monomer is (meth)acrylic acid or salts thereof.

7. The process of claim 6 , wherein the acrylic anionic monomer is acrylic acid or a salt thereof.

8. The process of claim 1 , wherein the acrylic non-ionic monomer is acrylamide and the acrylic anionic monomer is acrylic acid or a salt thereof, and the acrylic anionic monomer and the acrylic non-ionic monomer are present in a weight ratio of 70/30 to 50/50.

9. The process of claim 1 , wherein the paper or paperboard has improved strength compared to paper or paperboard prepared without the anionic organic polymeric microparticles added to the cellulosic thick stock of step (i).

10. The process of claim 9 , wherein the paper or paperboard has improved wet web strength.

11. The process of claim 9 , wherein the paper or paperboard has improved dry strength.

12. The process of claim 1 , wherein the process does not include addition of starch prior to step (iv).

13. The process of claim 1 , wherein the anionic organic polymeric microparticles are added as an aqueous dispersion having a solids content of below 1% by weight.

Assignments (13)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (ABL) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: BANK OF AMERICA, N.A, AS COLLATERAL AGENT
Reel/Frame 061432/0958 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
SECURITY AGREEMENT (TERM) Recorded Sep 13, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 061431/0851 →
SECURITY AGREEMENT (NOTES) Recorded Sep 13, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061431/0865 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: BASF SE
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 059206/0621 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 5, 2011
From: BUWONO, SULEMAN; REDDIHOUGH, GARY; DOGGE, JOZEF MARIA LEONARDUS
To: CIBA CORPORATION
Reel/Frame 026231/0888 →
ASSET TRANSFER AGREEMENT Recorded May 5, 2011
From: CIBA CORPORATION
To: BASF SE
Reel/Frame 026228/0384 →