IP Library Patent Application 13101529
Patent Application
App. No. 13/101,529

CELLULOSE GUMS WITH REDUCED VARIABILILTY AND METHOD FOR PRODUCING SAME

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Patent No.
US None
App. No.
13/101,529
Abstract

A process for reducing the variability in commercial production lots of cellulose gums, such as cellulose ethers, in which inert substances, such as sucrose, salt, maltodextrin, or other relatively are blended with the cellulose gums to create products that exhibit less variability in certain a functional property, such as aqueous viscosity than commercial production lots which have not been subjected to the blending process.

Claims (26)

1 . A method of producing a standardized cellulose gum composition having a standardized functional property at a defined concentration comprising forming a plurality of blends of a first cellulose gum having a first functionality with an adjusting agent selected from the group of one or more second cellulose gums and one or more inert soluble diluents and blends thereof over a range of ratios;

measuring the functionality of said plurality of blends to establish a functionality curve;

forming a standardized blend of cellulose gum and said adjusting agent having a desired standard functionality by combining said first cellulose gum with said adjusting agent in relative amount conforming to said standardization curve.

2 . The method claimed in claim 1 wherein said functionality is viscosity.

3 . The method claimed in claim 2 wherein said first functionality is high viscosity and said adjusting agent is a cellulose gum having a lower viscosity than said first cellulose gum second functionality is low functionality relative to said high functionality.

4 . The method claimed in claim 1 wherein said functionality is gel stabilization.

5 . The method claimed in claim 1 wherein said functionality is protein stabilization.

6 . The method of producing a standardized cellulose gum composition of claim 1 wherein the cellulose ether is selected from the group consisting of hydroxyethylcellulose (HEC), hydroxypropyl cellulose (HPC), methylcellulose (MC), carboxymethylcellulose (CMC) and methylhydroxyethylcellulose.

7 . The method of producing a standardized cellulose gum composition of claim 6 wherein the cellulose ether comprises carboxymethylcellulose (CMC).

8 . The method for producing a standardized cellulose gum composition of claim 1 wherein the cellulose gum to be standardized is dry blended with the adjusting agent.

9 . The method for producing a standardized cellulose gum composition of claim 1 wherein the standardizing agent is a sugar.

10 . The method for producing a standardized cellulose gum composition of claim 1 wherein the standardizing agent is a salt.

11 . The method for producing a standardized cellulose gum composition of claim 10 wherein the standardizing agent is a sugar selected from the group consisting of sucrose, dextrose and fructose.

12 . The method for producing a standardized cellulose gum composition of claim 10 wherein the standardizing agent is a salt selected from the group consisting of NaCl and KCl.

13 . The method for producing a standardized cellulose gum composition of claim 1 wherein the standardizing agent is a filler or pigment conventionally used in water-based paints, for example chalk, dolomite, calcium carbonate, perlite, talc, kaolin, mica, gypsum, feldspar, calcite, titanium dioxide, zinc dioxide, etc.

14 . The method for producing a standardized cellulose gum composition of claim 1 wherein the standardizing agent is a mineral filler selected from the group consisting of calcium hydrate hemi hydrate, ground gypsum, Portland cement, calcium carbonate, clays, and powdered silica.

15 . A method for producing a standardized cellulose gum composition comprising the steps of:

a. dissolving a sample of cellulose gum to be standardized at various concentrations in a solvent to generate a functional property calibration curve; and

b. blending the cellulose gum to be standardized with an amount of a standardizing agent determined through the use of the functional property calibration curve to generate a standardized cellulose gum composition.

16 . The method for producing a standardized cellulose gum composition of claim 15 wherein the cellulose gum is a cellulose ether.

17 . The method for producing a standardized cellulose gum composition of claim 15 wherein the cellulose ether is selected from the group consisting of hydroxyethylcellulose (HEC), hydroxypropyl cellulose (HPC), methylcellulose (MC), carboxymethylcellulose (CMC) and methylhydroxyethylcellulose.

18 . The method for producing a standardized cellulose gum composition of claim 17 wherein the cellulose ether comprises carboxymethylcellulose (CMC).

19 . The method for producing a standardized cellulose gum composition of claim 15 wherein the cellulose gum to be standardized is dry blended with the standardizing agent.

20 . The method for producing a standardized cellulose gum composition of claim 15 , wherein the standardizing agent is a sugar.

21 . The method for producing a standardized cellulose gum composition of claim 15 wherein the standardizing agent is a salt.

22 . The method for producing a standardized cellulose gum composition of claim 20 , wherein the standardizing agent is a sugar selected from the group consisting of sucrose, dextrose and fructose.

Assignments (3)
RELEASE OF PATENT SECURITY AGREEMENT Recorded Mar 18, 2013
From: THE BANK OF NOVA SCOTIA
To: ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC; AQUALON COMPANY; ISP INVESTMENTS INC.; HERCULES INCORPORATED
Reel/Frame 030025/0320 →
SECURITY AGREEMENT Recorded Sep 16, 2011
From: ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC; HERCULES INCORPORATED; AQUALON COMPANY; ISP INVESTMENT INC.
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 026918/0052 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 5, 2011
From: HINES, MARK EDWARD; LEIPOLD, DIANNE PATRICIA
To: HERCULES INCORPORATED
Reel/Frame 026232/0210 →