IP Library Granted Patent US 8,354,361
Granted Patent B2
US 8,354,361 · App. 13/236,332 · Granted Jan 15, 2013

Method of using dithiazines and derivatives thereof in the treatment of wells

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Quick Facts
Patent No.
US 8,354,361
App. No.
13/236,332
Granted
Jan 15, 2013
Kind
B2
Abstract

Corrosion of metallic tubulars in an oil, gas or geothermal well may be inhibited by introducing into the well a dithiazine derivative of the formula: wherein R 14 is a C 1 -C 24 straight chain or branched alkyl group; or a C 6 -C 24 aryl or arylalkyl group; R 15 is a C 1 -C 6 alkyl or a C 6 -C 30 aryl or alkylaryl group; and X is chlorine, bromine or iodine. The dithiazine may be isolated from a whole spent fluid (WSF) formed by reaction of hydrogen sulfide and a triazine. Alternately, the whole spent fluid containing dithiazine or dithiazine derivative and a corrosion inhibiting formulation may be used to inhibit corrosion in the well.

Claims (16)

1. A method of inhibiting corrosion during the treatment of a subterranean formation which comprises introducing into a gas or oil well a corrosive inhibiting effective amount of a dithiazine of the formula:

wherein:

R 14 is a C 1 -C 24 straight chain or branched alkyl group; or a C 6 -C 24 aryl or arylalkyl group;

R 15 is a C 1 -C 6 alkyl or a C 6 -C 30 aryl or alkylaryl group; and

X is chlorine, bromine or iodine.

2. The method of claim 1 , wherein R 14 is a C 1 -C 12 straight chain or branched alkyl group.

3. The method of claim 1 , wherein X is —Cl.

4. The method of claim 1 , wherein the dithiazine is of formula (IV).

5. The method of claim 4 , wherein R 14 is methyl.

6. The method of claim 1 , wherein the dithiazine is of formula (V).

7. The method of claim 6 , wherein R 15 is benzyl or naphthylmethyl.

8. The method of claim 7 , wherein R 14 is methyl.

9. The method of claim 1 , wherein R 14 is methyl or phenyl.

10. The method of claim 8 , wherein R 15 is benzyl.

11. The method of claim 9 , wherein R 14 is methyl.

12. The method of claim 4 , wherein R 14 is phenyl.

Assignments (3)
CHANGE OF NAME Recorded Mar 8, 2022
From: BAKER HUGHES, A GE COMPANY, LLC
To: BAKER HUGHES HOLDINGS LLC
Reel/Frame 059339/0130 →
CHANGE OF NAME Recorded Feb 16, 2022
From: BAKER HUGHES INCORPORATED
To: BAKER HUGHES, A GE COMPANY, LLC
Reel/Frame 059126/0517 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 19, 2011
From: TAYLOR, GRAHAME NIGEL
To: BAKER HUGHES INCORPORATED
Reel/Frame 026929/0404 →