IP Library Granted Patent US 9,273,227
Granted Patent B2
US 9,273,227 · App. 13/786,462 · Granted Mar 1, 2016

Waterborne aqueous-alcohol soluble protein compositions, applications, and methods

Inventors: Leif Sedgewick Freeman (Sioux Falls, SD); John Warrent Lawton, Jr. (Sioux Falls, SD); Melvin Glenn Mitchell (Penrose, NC); Marvin Lynn Mitchell (Parker, CO); Laura Martin (Brookings, SD)
Assignee: POET RESEARCH, INC.
C09D189/00C07K1/145C07K14/425C07K14/4732C08J3/05C08K5/10C08L89/00C09J189/00D21H19/12C08J2389/00
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Quick Facts
Patent No.
US 9,273,227
App. No.
13/786,462
Granted
Mar 1, 2016
Kind
B2
Abstract

Waterborne aqueous-alcohol soluble protein compositions, methods of making the compositions, and applications thereof are disclosed. The dispersion compositions include protein, water, acid, and optionally an ester of a carboxylic acid. The methods of making the compositions including combining the protein, water, acid and optionally ester to form a dispersion without the benefit of alcohol. Applications include industrial and food applications, such as binders and coatings, for example paint binders or coatings for paper products and pharmaceuticals.

Claims (13)

1. A method, comprising:

combining a set of components in one or more steps to form a dispersion of an aqueous-alcohol soluble protein without the addition of alcohol, wherein the set of components comprises an amount of an aqueous-alcohol soluble protein, an amount of water, an amount of an acid, and an amount of an ester of a carboxylic acid, and further wherein combining comprises: dissolving the acid in water to form a first mixture; and, mixing the ester and the protein into the first mixture to form the dispersion.

2. A method according to claim 1 , wherein mixing comprises stirring, heating, and cooling.

3. A method according to claim 1 , further comprising: drying the dispersion.

4. A method according to claim 3 , further comprising: re-dispersing the dried dispersion in water.

5. A method according to claim 1 , further comprising preparing at least one of a binder or a coating from the dispersion.

6. A method according to claim 1 , further comprising preparing a paint composition, a composition for use in pharmaceutical applications, a composition for use in food applications, a varnish composition, or an adhesive composition using the dispersion.

7. A method, comprising:

combining a set of components in one or more steps to form a dispersion of an aqueous-alcohol soluble protein without the addition of alcohol, wherein the set of components comprises an amount of an aqueous-alcohol soluble protein, an amount of water, an amount of an acid, and an amount of an ester of a carboxylic acid, and further wherein combining comprises: dissolving ester and acid in water to form a first liquid portion; dissolving acid in water to form a second liquid portion; adding the first liquid portion to the protein to form a first mixture; stirring and heating the first mixture; heating the second liquid portion; heating water; alternatively adding while stirring the heated second liquid portion and the heated water in one or more steps to the first mixture to form a second mixture; and, cooling while stirring the second mixture to room temperature.

8. A method according to claim 7 , further comprising: drying the dispersion.

9. A method according to claim 8 , further comprising: re-dispersing the dried dispersion in water.

10. A method according to claim 7 , further comprising preparing at least one of a binder or a coating from the dispersion.

11. A method according to claim 7 , further comprising preparing a paint composition, a composition for use in pharmaceutical applications, a composition for use in food applications, a varnish composition, or an adhesive composition using the dispersion.

Assignments (11)
SECURITY INTEREST Recorded Apr 3, 2020
From: POET RESEARCH, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 052312/0801 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 035603/0778 Recorded Apr 2, 2020
From: JPMORGAN CHASE BANK N.A., AS ADMINISTRATIVE AGENT
To: POET, LLC; POET RESEARCH, INC.; POET PLANT MANAGEMENT, LLC; POET INVESTMENTS, INC.; POET BIOMASS, LLC; POET DESIGN AND CONSTRUCTION, INC.; RISK MANAGEMENT ASSOCIATES, INC.; POET NUTRITION, INC.; POET RESEARCH CENTER, LLC (FORMERLY KNOWN AS POET RESEARCH CENTER, INC.); POET LEASING, LLC; POET NUTRITION INTERNATIONAL, INC.
Reel/Frame 052299/0676 →
SECURITY INTEREST Recorded Apr 2, 2020
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052295/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 14, 2019
From: LAWTON, JOHN WARREN
To: POET RESEARCH, INC.
Reel/Frame 049173/0583 →
EMPLOYEE AGREEMENT Recorded Apr 30, 2019
From: LAWTON, JOHN
To: POET RESEARCH, INC.
Reel/Frame 049042/0931 →
CORRECTIVE ASSIGNMENT TO CORRECT THE CORRECT CONVEYING PARTY PREVIOUSLY RECORDED ON REEL 034983 FRAME 888. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 21, 2015
From: FREEMAN, LEIF SEDGEWICK; MITCHELL, MARVIN LYNN; MITCHELL, MELVIN GLENN
To: POET RESEARCH, INC.
Reel/Frame 035750/0873 →
ACKNOWLEDGEMENT OF SECURITY INTEREST IN PATENTS Recorded May 6, 2015
From: POET, LLC; POET RESEARCH, INC.; POET PLANT MANAGEMENT, LLC; POET INVESTMENTS, INC.; POET BIOMASS, LLC; POET DESIGN AND CONSTRUCTION, INC.; RISK MANAGEMENT ASSOCIATES, INC.; POET NUTRITION, INC.; POET RESEARCH CENTER, INC.; POET LEASING, LLC; POET NUTRITION INTERNATIONAL, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 035603/0778 →
RELEASE OF PATENT, TRADEMARK AND COPYRIGHT SECURITY INTEREST Recorded May 6, 2015
From: BOKF, N.A., DBA BANK OF OKLAHOMA
To: POET RESEARCH, INC. F/K/A BROIN AND ASSOCIATES, INC.; POET, LLC F/K/A BROIN COMPANIES, LLC; POET INVESTMENTS, INC. F/K/A BROIN ENTERPRISES, INC.; POET PLANT MANAGEMENT, LLC
Reel/Frame 035603/0610 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 25, 2015
From: MARTIN, LAURA
To: POET RESEARCH, INC.
Reel/Frame 035025/0174 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2015
From: REDFORD, STEVEN G.
To: POET RESEARCH, INC.
Reel/Frame 034983/0888 →
SECURITY INTEREST Recorded Aug 7, 2014
From: POET RESEARCH, INC. F/K/A BROIN AND ASSOCIATES, INC.
To: BOKF, NA DBA BANK OF OKLAHOMA
Reel/Frame 033494/0016 →
Continuity (1)
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