IP Library Granted Patent US 9,925,529
Granted Patent B2
US 9,925,529 · App. 14/768,119 · Granted Mar 27, 2018

Photocatalytic element for purification and disinfection of air and water and method for the production thereof

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Quick Facts
Patent No.
US 9,925,529
App. No.
14/768,119
Granted
Mar 27, 2018
Kind
B2
Abstract

The invention relates to the purification and disinfection of air and water. A photocatalytic element consists of sintered glass beads with a pore volume fraction from 20% to 40% and a pore size from 0.1 to 0.5 mm, the surface of which is coated with a titanium dioxide powder, having a specific surface area of 150-400 m 2 /g, at the rate of 0.5-2% relative to the total mass of the photocatalytic element. The surface of the glass beads has a relief shape with a relief depression of 0.5-10 μm. The method for producing the photocatalytic element comprises sintering the glass beads at a temperature that is 5-20° C. higher than the glass softening temperature, modifying the bead surface with chemical etching agents, and coating the bead surface with the titanium dioxide powder from a water suspension at a pH of 2.9±0.1.

Claims (8)

1. A photocatalytic element for air and water purification and disinfection comprising:

sintered glass beads covered with titanium dioxide powder, wherein the sintered glass beads have open porosity with a pore size of 0.1 mm to 0.5 mm with a pore volume fraction from 20% to 40%;

the sintered glass beads' surface has a relief shape with a relief depth of 0.5 to 10 micron; and

titanium dioxide powder specific surface area is 150 to 400 m 2 /g with a weight percentage of the titanium dioxide powder of 0.5 to 2% of the photocatalytic element's weight.

2. A method for the production of the photocatalytic element according to claim 1 , comprising:

sintering of glass beads, sintered glass beads' surface modification, and titanium dioxide powder application on the sintered glass beads' modified surface, wherein the glass beads are sintered at a temperature 5 to 20° C. above the glass softening point, and prior to the titanium dioxide powder application the sintered glass beads' surface is modified by etching chemicals, and the titanium dioxide powder is applied onto the sintered glass beads' surface from a titanium dioxide powder aqueous suspension with the pH value=2.9±0.1.

3. The method for the production of the photocatalytic element according to claim 2 , wherein:

modification of the sintered glass beads' surface by etching chemicals consists in consecutive treatment with concentrated hydrofluoric acid during 1 to 5 minutes and concentrated sulfuric acid during 1 to 5 minutes.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 28, 2021
From: OOO "KRASNOE POLE"; IPKHF RAN; NTSCHRAN; OOO "TIOKRAFT"
To: OOO "KRASNOE POLE"
Reel/Frame 056073/0746 →
PARTIAL ASSIGNMENT (25%) Recorded Aug 24, 2015
From: BALIKHIN, IGOR LVOVICH; BERESTENKO, VICTOR IVANOVICH; DOMASHNEV, IGOR ANATOLEVICH; KABACHNIKOV, EVGENY NIKOLAEVICH; KURKIN, EVGENY NIKOLAEVICH; TROITSKY, VLADIMIR NIKOLAEVICH
To: OOO "KRASNOE POLE"
Reel/Frame 036424/0724 →
PARTIAL ASSIGNMENT (25%) Recorded Aug 24, 2015
From: BALIKHIN, IGOR LVOVICH; BERESTENKO, VICTOR IVANOVICH; DOMASHNEV, IGOR ANATOLEVICH; KABACHNIKOV, EVGENY NIKOLAEVICH; KURKIN, EVGENY NIKOLAEVICH; TROITSKY, VLADIMIR NIKOLAEVICH
To: IPKHF RAN
Reel/Frame 036432/0532 →
PARTIAL ASSIGNMENT (25%) Recorded Aug 24, 2015
From: BALIKHIN, IGOR LVOVICH; BERESTENKO, VICTOR IVANOVICH; DOMASHNEV, IGOR ANATOLEVICH; KABACHNIKOV, EVGENY NIKOLAEVICH; KURKIN, EVGENY NIKOLAEVICH; TROITSKY, VLADIMIR NIKOLAEVICH
To: NTSCHRAN
Reel/Frame 036432/0677 →
PARTIAL ASSIGNMENT (25%) Recorded Aug 24, 2015
From: BALIKHIN, IGOR LVOVICH; BERESTENKO, VICTOR IVANOVICH; DOMASHNEV, IGOR ANATOLEVICH; KABACHNIKOV, EVGENY NIKOLAEVICH; KURKIN, EVGENY NIKOLAEVICH; TROITSKY, VLADIMIR NIKOLAEVICH
To: OOO "TIOKRAFT"
Reel/Frame 036432/0957 →