IP Library Granted Patent US 11,090,881
Granted Patent B2
US 11,090,881 · App. 15/027,800 · Granted Aug 17, 2021

In-situ desizing for liquid infusion processes

Inventors: John D. Riehl (Hebron, CT); Charles R. Watson (Windsor, CT)
Assignee: RAYTHEON TECHNOLOGIES CORPORATION
B29C70/48B29B13/00B29B13/023B29C33/10B29B2013/002B29B2013/005B29K2079/08B29L2009/00
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Quick Facts
Patent No.
US 11,090,881
App. No.
15/027,800
Granted
Aug 17, 2021
Kind
B2
Abstract

A method of molding a component includes the steps of providing a plurality of fibers, applying the fibers with a low temperature sizing to form a plurality of sized fibers, forming a preform from the plurality of sized fibers, placing the preform in a mold, and de-sizing the preform by heating the mold to an initial temperature that is sufficient to break down the low temperature sizing to a gaseous phase. A molding apparatus is also disclosed.

Claims (31)

1. A method of molding a component comprising the steps of:

(a) providing a plurality of fibers;

(b) applying the fibers with a low temperature sizing to form a plurality of sized fibers;

(c) forming a preform from the plurality of sized fibers;

(d) placing the preform in a mold; and

(e) de-sizing the preform by heating the mold to an initial temperature that is sufficient to break down the low temperature sizing to a gaseous phase.

2. The method according to claim 1 , wherein the plurality of fibers are high temperature fibers formed from a material that is capable of being processed at a temperature that is 600 degrees Fahrenheit or greater.

3. The method according to claim 2 , wherein the plurality of fibers are comprised of a polyimide-matrix composite material.

4. The method according to claim 2 , wherein the low temperature sizing is comprised of a material capable of complete decomposition at temperatures less than 850 degrees Fahrenheit.

5. The method according to claim 1 , including (f) removing the gaseous phase of the low temperature sizing from the mold via at least one of a vacuum pressure and a positive pressure.

6. The method according to claim 5 , including (g) heating the mold to an infusion temperature and injecting an infusion liquid to completely infuse the preform with the infusion liquid.

7. The method according to claim 6 , including (h) heating the mold to a curing temperature for a predetermined period of time to provide a cured preform.

8. The method according to claim 1 , wherein the preform is comprised of a non-pre-impregnated material.

9. The method according to claim 1 , wherein the preform comprises a three-dimensional dry-shaped preform.

10. The method according to claim 9 , wherein the dry-shaped preform is formed by at least one of braiding and weaving.

11. The method according to claim 1 , wherein the preform comprises a stack of tackified fabric.

12. A method of molding a component comprising the steps of:

(a) providing a plurality of fibers;

(b) applying the fibers with a low temperature sizing to form a plurality of sized fibers;

(c) forming a preform from the plurality of sized fibers;

(d) placing the preform in a mold;

(e) de-sizing the preform by heating the mold to an initial temperature that is sufficient to break down the low temperature sizing to a gaseous phase;

(f) removing the gaseous phase of the low temperature sizing from the mold;

(g) heating the mold to an infusion temperature and injecting an infusion liquid to infuse the preform; and

(h) heating the mold to a curing temperature to form a cured polyimide-matrix composite material.

13. The method according to claim 12 , wherein step (g) is performed subsequent to step (f).

14. The method according to claim 12 , wherein the low temperature sizing is comprised of a material capable of complete decomposition at temperatures less than 850 degrees Fahrenheit.

15. The method according to claim 14 , wherein the infusion liquid is resin.

16. The method according to claim 14 , wherein step (f) includes removing the gaseous phase with a vacuum pump.

17. The method according to claim 14 , wherein the plurality of fibers are high temperature fibers formed from a material that is capable of being processed at a temperature that is 600 degrees Fahrenheit or greater.

18. The method according to claim 17 , wherein the plurality of fibers are comprised of a polyimide-matrix composite material.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
CHANGE OF NAME Recorded Apr 22, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 052472/0871 →
Continuity (2)
Provisional Application 61900430 · Nov 6, 2013
Related Publication 20160243772A1 · Aug 25, 2016