Furnace
A furnace, in particular for an electro thermal atomization device of an atom absorption spectrometer, has a heatable heat duct in which is mounted a trial platform. The trial platform is essentially basin-shaped with radially inward-turned rims, at least at its free ends. In order to make ongoing improvements in a furnace of the aforementioned type, so that the trial platform has an increased lifetime along with high reproducibility of measurements and simple operation as well as low cost, the trial platform features a geometric structure stabilization device which reduces the ratio of effective volume of the trial platform to the rim volume.
1. Furnace, for an electro thermal atomization device of an atom absorption spectrometer, with a heatable heat duct inside which there is mounted a trial platform, which has a platform length and is essentially basin-shaped with radially inward-turned rims, at least at its free ends, each of the rims having a rim thickness and a rim height, characterized in that the trial platform has a geometric structure stabilization device that reduces the ratio of effective volume of the trial platform to a rim volume occupied by the rims of the trial platform.
2. Furnace in accordance with claim 1 , characterized in that the furnace is a heated graphite atomizer that, is transversally heatable.
3. Furnace in accordance with claim 1 , characterized in that the trial platform is integrated in the heat duct.
4. Furnace in accordance with claim 3 , characterized in that the trial platform is formed of graphite as base material, on which an overcoating is applied pyrolytically.
5. Furnace in accordance with claim 4 , characterized in that the geometric structure stabilization device is formed by a reduction of the platform length.
6. Furnace in accordance with claim 5 , characterized in that the reduction of the platform length is in the range from 10 to 40 percent.
7. Furnace in accordance with claim 4 , characterized in that the geometric structure stabilization device is formed by an increase in the rim thickness.
8. Furnace in accordance with claim 7 , characterized in that the increase in rim thickness is in the range between 10 and 50 percent.
9. Furnace in accordance with claim 4 , characterized in that the geometric structure stabilization device is formed by an increase in the rim height of the trial platform.
10. Furnace in accordance with claim 9 , characterized in that the increase in the rim height is in the range between 40 and 250 percent.
11. Furnace in accordance with claim 10 , characterized in that the geometric structure stabilization device simultaneously includes a reduction of the platform length and/or an increase in the rim thickness and/or an increase in the rim height.
12. Furnace in accordance with claim 11 , characterized in that the increase in the rim thickness and/or the increase in the rim height is found at least on one end of the trial platform.
13. Furnace in accordance with claim 5 , characterized in that the reduction of the platform length is in the range from 15 to 35 percent.
14. Furnace in accordance with claim 5 , characterized in that the reduction of the platform length is in the range from 20 to 35 percent.
15. Furnace in accordance with claim 8 , characterized in that the increase in rim thickness is in the range between 25 and 45 percent.
16. Furnace in accordance with claim 8 , characterized in that the increase in rim thickness is in the range between 30 and 40 percent.
17. Furnace in accordance with claim 10 , characterized in that the increase in rim height is in the range between 80 and 200 percent.
18. Furnace in accordance with claim 10 , characterized in that the increase in rim height is in the range between 100 and 150 percent.