IP Library Granted Patent US 7,824,462
Granted Patent B2
US 7,824,462 · App. 10/550,439 · Granted Nov 2, 2010

Metallic nanoparticles as orthopedic biomaterial

Assignee: Purdue Research Foundation
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Quick Facts
Patent No.
US 7,824,462
App. No.
10/550,439
Granted
Nov 2, 2010
Kind
B2
Abstract

A composition for use as a prosthetic biomaterial and associated method. The biomaterial exhibits cytocompatibility, mechanical functionality and osteoblast adhesion between the implant and interfacing surface. The biomaterial is metallic, has a grain size less than about 500 nanometers and has a surface roughness of less than about 800 nm rms.

Claims (38)

1. A biomaterial for use in implantable orthopedic prosthetic devices wherein said biomaterial comprises consolidated nanoparticles and

a. exhibits cytocompatibility with interfacing biological cells;

b. exhibits mechanical functionality with interfacing biological cells;

c. exhibits osteoblast adhesion between the implant and the interfacing biological cells; wherein the biomaterial

d. is a metal;

e. has a grain size less than about 500 nanometers; and

f. has a surface roughness less than about 500 nanometers root mean square (nm rms).

2. A biomaterial as in claim 1 wherein the surface roughness is between 11 and 356 nanometers root mean square.

3. A biomaterial as in claim 2 which consists essentially of a titanium based metal.

4. A biomaterial as in claim 3 wherein the titanium based metal has a particle size of less than about 500 nanometers and a surface roughness of about 11 nanometers root mean square.

5. A biomaterial as in claim 4 wherein said titanium based metal is commercially pure titanium.

6. A biomaterial as in claim 1 wherein said metal is a titanium based alloy consisting essentially of, on a weight percent basis, of about 11% titanium, 39% aluminum and 50% vanadium.

7. A biomaterial as in claim 1 wherein the metal, on a weight percent basis, is a cobalt-chrome-molybdenum alloy consisting essentially of about 3% cobalt, 70% chromium and 27% molybdenum with the particle size less than about 200 nanometers and the surface roughness less than about 356 nanometers root mean square.

8. A biomaterial as in claim 1 wherein said metal is a powder.

9. A biomaterial as in claim 8 wherein said powder is consolidated and compressed so as to form a surface for interfacing with biological tissue.

10. A biomaterial as in claim 8 wherein said powder is compressed at room temperature.

11. A method of forming an implantable orthopedic prosthetic device including the steps of:

(a) providing a metal biomaterial in powder form;

1. which exhibits cytocompatibility within interfacing biological cells;

2. exhibits mechanical functionality with interfacing biological cells; and

3. exhibits osteoblast adhesion between the implant and interfacing biological cells;

(b) compressing the powder in the absence of binders or sintering temperatures so as to form a consolidated composition comprising a surface for interfacing with biological cells, said consolidated composition having a grain size less than about 500 nanometers; and a surface roughness between about 11 and 360 nanometers root mean square.

12. A biomaterial for use in implantable orthopedic prosthetic devices wherein said biomaterial comprises consolidated nanoparticles and

a. exhibits cytocompatibility with interfacing biological cells;

b. exhibits mechanical functionality with interfacing biological cells;

c. exhibits osteoblast adhesion between the implant and the interfacing biological cells; wherein the biomaterial

d. is a metal; and

e. has a particle size between 200 and 500 nanometers and a surface roughness between 11 and 360 nanometers root mean square.

13. A biomaterial for use in implantable orthopedic prosthetic devices wherein said biomaterial:

a. exhibits cytocompatibility with interfacing biological cells;

b. exhibits mechanical functionality with interfacing biological cells;

c. exhibits osteoblast adhesion between the implant and the interfacing biological cells; wherein the biomaterial

d. is a metal;

e. has a particle size less than 500 nanometers, and

f. has a surface roughness less than 500 nanometers root mean square (nm rms).

14. A biomaterial as in claim 13 wherein the surface roughness is between 11 and 356 nanometers root mean square.

15. A biomaterial as in claim 14 which consists essentially of a titanium based metal.

16. A biomaterial as in claim 13 wherein the metal on a weight percent basis, is a cobalt-chrome-molybdenum alloy consisting essentially of about 3% cobalt, 70% chromium and 27% molybdenum with the surface roughness less than about 356 nanometers root mean square.

Assignments (4)
CONFIRMATORY LICENSE Recorded May 24, 2010
From: PURDUE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 024428/0334 →
CONFIRMATORY LICENSE Recorded Jun 8, 2006
From: PURDUE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 017745/0592 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECIVING PARTY DATA OF THE PATENT ASSIGNMENT. (ASSIGNEE NAME AND ADDRESS) PREVIOUSLY RECORDED ON REEL 016646 FRAME 0497. ASSIGNOR(S) HEREBY CONFIRMS THE ENTIRE RIGHT, TITLE AND INTEREST OF PATENT APPLICATION.. Recorded Oct 26, 2005
From: WEBSTER, THOMAS J.; EJIOFOR, JEREMIAH U.
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 016687/0028 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 17, 2005
From: WEBSTER, THOMAS J.; EJIOFOR, JEREMIAH U.
To: BUNN-O-MATIC CORPORATION
Reel/Frame 016646/0497 →
Continuity (2)
Provisional Application 6045822700 · Mar 27, 2003
Related Publication 20060204538A1 · Sep 14, 2006