IP Library Granted Patent US 7,291,229
Granted Patent B2
US 7,291,229 · App. 10/659,327 · Granted Nov 6, 2007

Method of surface treatment of titanium metal

Assignees: Osaka Prefecture; Tanaka Limited; SDC Incorporated
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Quick Facts
Patent No.
US 7,291,229
App. No.
10/659,327
Granted
Nov 6, 2007
Kind
B2
Abstract

A method of carburizing treatment is proposed in which if carburizing is carried out at a low temperature, carbon will not turn amorphose and deposit on the surface of a titanium metal but reliably penetrate into between metallic atoms. It is a method of surface treatment of a titanium metal comprising the steps of heating the titanium metal to a temperature of 400-690° C. in a cleaning gas atmosphere containing hydrogen gas, subjecting the surface of the titanium metal to cleaning by applying a DC voltage of 200-1500 V, and plasma carburizing in an atmosphere comprising a carburizing gas having an atomic weight ratio of hydrogen atoms (H) to carbon atoms (C) adjusted to 1≦H/C≦9 at a pressure of 13-400 Pa and a temperature of 400-690° C. Ionization reaction in the gas is suppressed suitably. Because there exists no excessive carbon which is not used for carburization but turns soot or glass-like carbon, in the atmosphere during carburization, carburizing reaction progresses smoothly.

Claims (5)

1. A method of surface treatment of a titanium metal comprising

plasma carburizing in an atmosphere comprising a carburizing gas having a composition thereof adjusted such that an (H/C) atomic weight ratio of hydrogen atoms (H) to carbon atoms (C) is 1≦H/C≦9 at a pressure of 13-400 Pa and a temperature of 400-690° C.

2. A method of surface treatment of a titanium metal comprising heating the titanium metal to a temperature of 400-690° C. in a cleaning gas atmosphere containing hydrogen gas,

subjecting the surface of the titanium metal to cleaning by applying a DC voltage of 200-1500 V, and

plasma carburizing in an atmosphere comprising a carburizing gas having a composition thereof adjusted such that an (H/C) atomic weight ratio of hydrogen atoms (H) to carbon atoms (C) is 1≦H/C≦9 at a pressure of 13-400 Pa and a temperature of 400-690° C.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 044794 FRAME: 0161. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER . Recorded Feb 12, 2018
From: TECHNOLOGY RESEARCH INSTITUTE OF OSAKA PREFECTURE
To: OSAKA RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE AND TECHNOLOGY
Reel/Frame 045302/0840 →
MERGER Recorded Feb 1, 2018
From: TECHNOLOGY RESEARCH INSTITUTE OF OSAKA PREFECTURE
To: OSAKA RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE AND TECHNOLOGY
Reel/Frame 044794/0161 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2012
From: OSAKA PREFECTURE
To: TECHNOLOGY RESEARCH INSTITUTE OF OSAKA PREFECTURE
Reel/Frame 029312/0150 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2003
From: ISHII, EIICHI; SONE, TAKUMI; SATO, YUKIHIRO; DEMIZU, KEI; KAKUTANI, HIDEO; TANAKA, KOICHI; TANAKA, SHINICHI; TSUJI, NORIYOSHI
To: OSAKA PREFECTURE; TANAKA LIMITED; SDC INCORPORATED
Reel/Frame 014813/0289 →
Priority Claims (1)
JP 2000-211518 · Jul 12, 2000 · national
Continuity (2)
Continuation In Part 0990226000 · Jul 11, 2001
Related Publication 20040084113A1 · May 6, 2004