IP Library Granted Patent US 7,608,292
Granted Patent B2
US 7,608,292 · App. 10/684,748 · Granted Oct 27, 2009

Method of processing soy protein

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Quick Facts
Patent No.
US 7,608,292
App. No.
10/684,748
Granted
Oct 27, 2009
Kind
B2
Abstract

A method of processing a proteinaceous material, the method entails (1) blending the proteinaceous material with alcohol and a reducing agent and (2) maintaining a combination having the proteinaceous material and the reducing agent at a greater than ambient temperature for a holding period of at least about five minutes to form a proteinaceous product.

Claims (40)

1. A method of processing a proteinaceous material the method comprising:

blending the proteinaceous material with alcohol and a reducing agent to form a mixture wherein the percentage of alcohol in the mixture is in the range of between about 5 to about 20 percent by weight;

maintaining the mixture at a temperature greater than 90° C. and a pressure greater than 10 psig for a holding period at least about five minutes to form a proteinaceous product; and

removing all or essentially all of the alcohol by venting the pressure on the proteinaceous product, the proteinaceous product with enhanced solubility and preserved color characteristics.

2. The method of claim 1 wherein, the alcohol is present in the mixture during the holding period.

3. The method of claim wherein the proteinaceous material comprises oilseed material that comprises oilseed protein.

4. The method of claim 3 wherein the oilseed material comprises soy protein.

5. The method of claim 1 wherein the reducing agent comprises a source of SO 2 .

6. The method of claim 1 wherein the reducing agent comprises an alkali metal sulfite, an alkali metal bisulfite, an alkali metal meta bisulfite, an alkali metal pyrosulfite, or any mixture of any of these.

7. The method of claim 1 wherein the reducing agent comprises sulfur dioxide, sodium sulfite, sodium bisulfite, sodium meta bisulfite, sodium pyrosulfite, potassium sulfite, potassium bisulfite, potassium meta bisulfite, potassium pyrosulfite, or any mixture of any of these.

8. The method of claim 1 wherein the alcohol is infinitely miscible in water.

9. The method of claim 1 wherein the alcohol comprises methanol, ethanol, propanol, or any mixture of any of these.

10. The method of claim 1 wherein the temperature ranges from about 100° C. to about 121° C.

11. The method of claim 1 wherein the holding period is at least about ten minutes.

12. The method of claim 11 wherein the holding period ranges from about ten to about thirty minutes.

13. The method of claim 1 , the method further comprising maintaining the combination comprising the proteinaceous material and the reducing agent at super-atmospheric pressure during the holding period.

14. The method of claim 13 wherein the super-atmospheric pressure ranges from about ten pounds per square inch gauge to about thirty pounds per square inch gauge.

15. A method of forming an animal feed, the method comprising combining the proteinaceous product of claim 1 with an animal feed component.

16. A method of processing a proteinaceous material the method comprising:

blending the proteinaceous material with a reducing agent to form a mixture;

maintaining the mixture at a temperature greater than 90° C. and a pressure greater than 10 psig in an autoclave for a holding period to form a proteinaceous product; and

removing all or substantially all of any alcohol present in the proteinaceous product by venting the pressure on the proteinaceous product, the proteinaceous product having enhanced solubility and preserved color characteristics.

17. The method of claim 16 wherein the proteinaceous material comprises oilseed material that comprises oilseed protein.

18. The method of claim 17 wherein the oilseed material comprises soy protein.

19. The method of claim 16 wherein the reducing agent comprises a source of SO 2 .

20. The method of claim 16 wherein the reducing agent comprises an alkali metal sulfite, an alkali metal bisulfite, an alkali metal meta bisulfite, an alkali metal pyrosulfite, or any mixture of any of these.

21. The method of claim 16 wherein the reducing agent comprises sulfur dioxide, sodium sulfite, sodium bisulfite, sodium meta bisulfite, sodium pyrosulfite, potassium

sulfite, potassium bisulfite, potassium meta bisulfite, potassium pyrosulfite, or any mixture of any of these.

22. The method of claim 16 wherein the greater than ambient temperature ranges from about 100° C. to about 121° C.

23. The method of claim 16 wherein the holding period lasts at least about five minutes.

24. The method of claim 16 wherein the holding period lasts at least about ten minutes.

25. The method of claim 16 wherein the holding period ranges from about ten minutes to about thirty minutes.

26. The method of claim 16 wherein the mixture further comprises an alcohol.

27. The method of claim 26 wherein the alcohol is infinitely miscible in water.

28. The method of claim 26 wherein the alcohol comprises methanol, ethanol, propanol, or any mixture of any of these.

29. A method of forming an animal feed, the method comprising combining the proteinaceous product of claim 16 with an animal feed component.

30. The method of claim 29 wherein the mixture of claim 20 further comprises alcohol and the method further comprises removing all or essentially all of any incorporated alcohol from the proteinaceous product.

31. The method of claim 1 wherein the mixture further comprises water.

32. The method of claim 1 wherein the proteinaceous material and reducing agent are combined with an aqueous solution to form the mixture, the aqueous solution comprising the alcohol and water.

33. The method of claim 16 wherein the mixture further comprises water.

Assignments (8)
CHANGE OF NAME Recorded Apr 23, 2015
From: LAND O'LAKES PURINA FEED LLC
To: PURINA ANIMAL NUTRITION LLC
Reel/Frame 035483/0749 →
RELEASE OF SECURITY INTEREST Recorded Dec 9, 2011
From: U.S. NATIONAL BANK ASSOCIATION
To: LAND O'LAKES, INC.
Reel/Frame 027358/0745 →
RELEASE OF SECURITY INTEREST Recorded Nov 22, 2009
From: JPMORGAN CHASE BANK, N.A.
To: LAND O'LAKES INC.; AGRICULTURAL INDEMNITY INSURANCE COMPANY; ALLIANCE MILK PRODUCTS, LLC; AMERICA'S COUNTRY STORES HOLDINGS, LLC; AMERICA'S COUNTRY STORES, LLC; CHEESE & PROTEIN INTERNATIONAL LLC; FEED SERVICES, LLC; FORAGE GENETICS, INC.; GOLDEN STATE FEEDS, LLC; GOLDEN VALLEY DAIRY PRODUCTS; HAY MARKETS INTERNATIONAL LLC; KIEL CHEESE, LLC; LAND O'LAKES HOLDINGS, INC.; LAND O'LAKES INTERNATIONAL DEVELOPMENT CORPORATION; LAND O'LAKES PURINA FEED LLC; LOL HOLDINGS II, INC.; MILK PRODUCTS, LLC; NORTHWEST FOOD PRODUCTS COMPANY, INC.; NORTHWEST FOOD PRODUCTS TRANSPORTATION, LLC; NUTRA-BLEND, L.L.C.; PAPILLON AGRICULTURAL PRODUCTS, INC.; PENNY-NEWMAN MILLING LLC; PMI AGRICULTURE L.L.C.; PMI NUTRITION INTERNATIONAL, LLC; PMI NUTRITION, LLC; PURINA MILLS, LLC; RESEARCH SEEDS, INC.; THOMAS PRODUCTS, LLC
Reel/Frame 023546/0901 →
SECURITY AGREEMENT Recorded Sep 21, 2006
From: LAND O'LAKES, INC.; AGRICULTURAL INDEMNITY INSURANCE COMPANY; ALLIANCE MILK PRODUCTS, LLC; AMERICA'S COUNTRY STORES HOLDINGS, LLC; AMERICA'S COUNTRY STORES, LLC; CHEESE & PROTEIN INTERNATIONAL LLC; FEED SERVICES, LLC; FORAGE GENETICS, INC.; GOLDEN STATE FEEDS, LLC; GOLDEN VALLEY DAIRY PRODUCTS; HAY MARKETS INTERNATIONAL LLC; KIEL CHEESE, LLC; LAND O'LAKES PURINA FEED LLC; LAND O'LAKES HOLDINGS, INC.; LAND O'LAKES INTERNATIONAL DEVELOPMENT CORPORATION; LOL HOLDINGS II, INC.; MILK PRODUCTS, LLC.; NORTHWEST FOOD PRODUCTS COMPANY, INC.; NORTHWEST FOOD PRODUCTS TRANSPORTATION, LLC; NUTRA-BLEND, LLC; PAPILLON AGRICULTURAL PRODUCTS, INC.; PENNY-NEWMAN MILLING LLC; PMI NUTRITION, LLC; PMI AGRICULTURE L.L.C.; PMI NUTRITION INTERNATIONAL, LLC; PURINA MILLS, LLC; RESEARCH SEEDS, INC.; THOMAS PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A. AS COLLATERAL AGENT
Reel/Frame 018279/0624 →
CHANGE OF NAME Recorded Dec 21, 2004
From: LAND O'LAKES FARMLAND FEED LLC
To: LAND O'LAKES PURINA FEED LLC
Reel/Frame 016087/0246 →
SECURITY INTEREST Recorded Jan 29, 2004
From: LAND O'LAKES, INC.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 014918/0368 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 17, 2003
From: MILLER, BILL L.; KAKADE, MADHU
To: LAND O'LAKES FARMLAND FEED LLC
Reel/Frame 014705/0559 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 14, 2003
From: MILLER, BILL L.; KAKADE, MADHU
To: LAND O'LAKES FARMLAND FEED LLC
Reel/Frame 014613/0565 →