IP Library Granted Patent US 7,163,564
Granted Patent B2
US 7,163,564 · App. 10/698,183 · Granted Jan 16, 2007

Method for brightening virgin mechanical pulp

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Quick Facts
Patent No.
US 7,163,564
App. No.
10/698,183
Granted
Jan 16, 2007
Kind
B2
Abstract

A method for brightening virgin mechanical pulp. The method comprises combining: (i) an aqueous solution comprising sodium borohydride and sodium hydroxide; and (ii) an aqueous solution comprising sodium bisulfite, in a chemical mixer and adding output of the chemical mixer to an aqueous slurry of virgin mechanical pulp. The ratio of (moles bisulfite−moles hydroxide)/moles borohydride is from 0 to 7.8.

Claims (8)

1. A method for brightening virgin mechanical pulp; said method comprising combining: (i) an aqueous solution comprising sodium borohydride and sodium hydroxide; and (ii) an aqueous solution comprising sodium bisulfite, in a chemical mixer and adding output of the chemical mixer to an aqueous slurry of virgin mechanical pulp;

wherein a ratio of (moles bisulfite−moles hydroxide)/moles borohydride in from 4 to 7.5, and the output of the chemical mixer is added to the pulp slurry within 12 hours of mixing.

2. The method of claim 1 in which said ratio is from 5 to 7.

3. The method of claim 2 in which the output of the chemical mixer is added to the pulp slurry within 3 hours of mixing.

4. The method of claim 3 in which the chemical mixer is an in-line static mixer, and the output of the chemical mixer is substantially homogeneous prior to addition to the pulp slurry.

5. The method of claim 4 in which a ratio of sodium borohydride to pulp is from 0.015 weight % to 0.12 weight %, and said aqueous solution comprising sodium borohydride and sodium hydroxide comprises about 12% sodium borohydride and about 40% sodium hydroxide.

6. The method of claim 1 further comprising addition of at least one chelant to the pulp slurry.

7. The method of claim 6 in which the output of the chemical mixer is added to the pulp slurry within 3 hours of mixing.

Assignments (18)
RELEASE OF SECURITY INTEREST Recorded Apr 14, 2026
From: PNC BANK, NATIONAL ASSOCIATION, AS AGENT
To: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
Reel/Frame 074358/0202 →
RELEASE OF SECURITY INTEREST Recorded Jul 2, 2021
From: ANTARES CAPITAL LP
To: ASCENSUS SPECIALTIES LLC; ASCENSUS SPECIALTIES CALLERY LLC
Reel/Frame 056742/0897 →
SECURITY INTEREST Recorded Jun 30, 2021
From: ASCENSUS SPECIALTIES LLC
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 056721/0304 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jun 30, 2021
From: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY, AS COLLATERAL AGENT
To: ASCENSUS SPECIALTIES LLC; ASCENSUS SPECIALTIES CALLERY LLC F/K/A CALLERY, LLC
Reel/Frame 056728/0624 →
PATENT SECURITY AGREEMENT Recorded Oct 7, 2019
From: ASCENSUS SPECIALTIES LLC; CALLERY, LLC
To: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY, AS AGENT
Reel/Frame 050646/0905 →
RELEASE OF SECURITY INTEREST Recorded Sep 30, 2019
From: CB CORPORATE FINANCE, LLC
To: ASCENSUS SPECIALTIES LLC
Reel/Frame 050565/0873 →
RELEASE OF SECURITY INTEREST Recorded Sep 30, 2019
From: TCW ASSET MANAGEMENT COMPANY LLC
To: ASCENSUS SPECIALTIES LLC
Reel/Frame 050568/0610 →
RELEASE OF SECURITY INTEREST Recorded Sep 27, 2019
From: PNC BANK, NATIONAL ASSOCIATION
To: ASCENSUS SPECIALTIES LLC
Reel/Frame 050575/0001 →
RELEASE OF PATENT SECURITY AGREEMENT Recorded Sep 25, 2019
From: CB CORPORATE FINANCE, LLC
To: ASCENSUS SPECIALTIES LLC, FORMERLY KNOWN AS VERTELLUS PERFORMANCE CHEMICALS LLC; ASCENSUS SPECIALTIES SBH HOLDINGS LLC, VERTELLUS SBH HOLDINGS LLC; ASCENSUS SPECIALTIES ACQUISITION CORP., VSI ACQUISITION CORP.
Reel/Frame 050484/0097 →
SECURITY INTEREST Recorded Sep 24, 2019
From: ASCENSUS SPECIALTIES LLC; CALLERY, LLC
To: ANTARES CAPITAL LP, AS AGENT
Reel/Frame 050470/0746 →
CHANGE OF NAME Recorded May 1, 2018
From: VERTELLUS PERFORMANCE CHEMICALS LLC
To: ASCENSUS SPECIALTIES LLC
Reel/Frame 046047/0354 →
PATENT SECURITY AGREEMENT Recorded Sep 25, 2017
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: CB CORPORATE FINANCE, LLC
Reel/Frame 043991/0111 →
PATENT SECURITY AGREEMENT Recorded Sep 22, 2017
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: TCW ASSET MANAGEMENT COMPANY LLC, AS COLLATERAL AGENT
Reel/Frame 043953/0331 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Sep 22, 2017
From: WILMINGTON TRUST NATIONAL ASSOCIATION
To: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
Reel/Frame 043954/0261 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2015
From: ROHM AND HAAS COMPANY
To: VERTELLUS PERFORMANCE CHEMICALS LLC
Reel/Frame 035804/0378 →
SECURITY INTEREST Recorded Apr 13, 2015
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: PNC BANK, NATIONAL ASSOCIATION, AS AGENT
Reel/Frame 035389/0885 →
SECURITY INTEREST Recorded Feb 11, 2015
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 034942/0131 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 19, 2014
From: SIBIET, JEAN LUC; NAJIM, JOSEPH; KRISHNAN, SUNDAR CHELLAPPAN JAYA
To: ROHM AND HAAS COMPANY
Reel/Frame 034210/0993 →
Continuity (2)
Provisional Application 6042388700 · Nov 5, 2002
Related Publication 20040117914A1 · Jun 24, 2004