IP Library Granted Patent US 7,696,252
Granted Patent B2
US 7,696,252 · App. 10/703,094 · Granted Apr 13, 2010

Process for the production of emulsions and dispersions

Assignee: Australian National University
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Quick Facts
Patent No.
US 7,696,252
App. No.
10/703,094
Granted
Apr 13, 2010
Kind
B2
Abstract

Methods for the formation of colloidal suspensions. The method includes combining an aqueous substance with a second substance that is normally immiscible with the aqueous substance, to form a mixture, and before, during or after the combining removing dissolved gases from one or both of the aqueous and second substance, whereby the aqueous and second substances mix and form a colloidal suspension. The methods for the formation of colloidal suspensions include methods for the formation of emulsions as well as particulate dispersions. The methods used to form the colloidal suspensions in accordance with the present invention produce colloidal suspensions that are stable for periods from an hour to several weeks in the absence of surfactants or stabilizing agents.

Claims (36)

1. A process for the production of an oil emulsion, comprising:

combining an aqueous liquid with

an oil, to form a mixture,

wherein the mixture is formed in the absence of a surfactant, and in the absence of an emulsion stabilizing polymer and in the absence of a stabilizing agent; and

before, during or after said combining removing dissolved gases from the mixture, the oil, or the aqueous liquid;

thus forming an oil emulsion, which does not comprise either a surfactant, an emulsion stabilizing polymer or a stabilizing agent;

wherein the removing dissolved gases comprises removing at least 99 per cent of the dissolved gas present in the mixture, the oil or the aqueous liquid; and

wherein said oil emulsion is formed without mechanical action.

2. The process of claim 1 wherein said oil emulsion is stable for a period of from one hour to several weeks.

3. The process of claim 1 wherein removing dissolved gases comprises creating a vacuum.

4. The process of claim 1 wherein said oil is a hydrocarbon water-insoluble oil, a fluorocarbon water-insoluble oil, or combinations thereof.

5. The process of claim 1 wherein said emulsion comprises a material selected from the group consisting of a pharmaceutical treating agent, a paint, a dye, a combustion fuel, a fuel additive, a food additive, a food product, a perfume, a cosmetic product, a hygiene product, a dermatological product, an insect repellent, a mineral, and a combination thereof.

6. the process of claim 1 wherein said removing of dissolved gases comprises removing at least 99.99 per cent of the dissolved gas present in the mixture.

7. The process of claim 1 wherein said removing of dissolved gases comprises removing at least 99.999 per cent of the dissolved gas present in the mixture.

8. The process of claim 1 wherein said removing of dissolved gases comprises removing from 99 to 99.99 per cent of the dissolved gas present in the mixture.

9. A process for the production of an oil emulsion, comprising:

combining an aqueous liquid with

an oil, to form a mixture,

wherein the mixture is formed in the absence of a surfactant, and in the absence of an emulsion stabilizing polymer and in the absence of a stabilizing agent; and

before, during or after said combining removing dissolved gases from the mixture, the oil, or the aqueous liquid;

thus forming an oil emulsion, which does not comprise either a surfactant, an emulsion stabilizing polymer or a stabilizing agent;

wherein the removing dissolved gases comprises removing at least 99 per cent of the dissolved gas present in the mixture, the oil or the aqueous liquid; and

wherein removing dissolved gases comprises:

freezing the oil and the aqueous liquid; and

creating a vacuum.

10. The process as in claim 9 , wherein creating a vacuum comprises lowering the pressure to a pressure of less than about twenty Torr.

11. The process as in claim 9 , wherein creating a vacuum comprises lowering the pressure to a pressure of less than about twenty milliTorr.

12. The process of claim 9 wherein said oil emulsion is formed with mechanical action.

13. The process of claim 9 wherein said oil emulsion is stable for a period of from one hour to several weeks.

14. The process as in any of claims 9 wherein creating a vacuum comprises lowering the pressure to a pressure of less than about twenty Torr.

15. The process as in any of claims 9 wherein creating a vacuum comprises lowering the pressure to a pressure of less than about twenty milliTorr.

16. The process of claim 9 wherein said oil is a hydrocarbon water-insoluble oil, a fluorocarbon water-insoluble oil, or combinations thereof.

17. The process of 9 wherein said emulsion comprises a material selected from the group consisting of a pharmaceutical treating agent, a paint, a dye, a combustion fuel, a fuel additive, a food additive, a food product, a perfume, a cosmetic product, a hygiene product, a dermatological product, an insect repellent, a mineral, and a combination thereof.

18. The process of claim 9 wherein said removing of dissolved gases comprises removing at least 99.99 per cent of the dissolved gas present in the mixture.

19. The process of claim 9 wherein said removing of dissolved gases comprises removing at least 99.999 per cent of the dissolved gas present in the mixture.

20. The process of claim 9 wherein said removing of dissolved gases comprises removing from 99 to 99.99 per cent of the dissolved gas present in the mixture.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2011
From: THE AUSTRALIAN NATIONAL UNIVERSITY
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 026905/0816 →
CONFIRMATORY LICENSE Recorded Dec 29, 2010
From: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 025570/0987 →
CONFIRMATORY LICENSE Recorded Aug 12, 2010
From: UNIVERSITY OF CALIFORNIA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 024826/0893 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 30, 2004
From: PASHLEY, RICHARD M.
To: REGENTS OF THE UNIVERSITY OF CALIFORNIA, THE; AUSTRALIAN NATIONAL UNIVERSITY
Reel/Frame 015274/0650 →
Continuity (1)
Related Publication 20050096398A1 · May 5, 2005