IP Library Granted Patent US 7,041,973
Granted Patent B2
US 7,041,973 · App. 10/841,851 · Granted May 9, 2006

Method and device for the mass-spectrometric analysis of gases

Assignee: Thermo Electron (Bremen) GmbH
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Quick Facts
Patent No.
US 7,041,973
App. No.
10/841,851
Granted
May 9, 2006
Kind
B2
Abstract

The invention relates to a method for operating a mass spectrometer, in particular a static mass spectrometer, with an ion source and an analyzer. The invention likewise concerns the mass spectrometer. According to the invention, a gas admitted into the mass spectrometer is bonded in a concentrated manner on a cooled surface and then ionized.

Claims (16)

1. Method of operating a static mass spectrometer ( 10 ), with an ion source ( 12 ) and an analyzer ( 14 ), comprising the steps of:

a) evacuating the mass spectrometer;

b) admitting a gas into the mass spectrometer;

c) bonding the gas in a concentrated manner on a surface with the ion source of the mass spectrometer by cooling said surface;

d) ionizing the gas on the cooled surface within the ion source; and

e) analyzing the ionized gas in the analyzer.

2. Method according to claim 1 , characterized in that the gas is cooled only to the extent that diffusion movements are still possible on the cooled surface.

3. Method according to claim 2 , characterized in that the gas is ionized by an electric field (field ionization).

4. Method according to claim 2 , characterized in that the gas is ionized by electron impact.

5. Method according to claim 2 , characterized in that the gas is ionized by irradiation with laser light.

6. Method according to claim 1 , characterized in that the gas is ionized by an electric field (field ionization).

7. Method according to claim 1 , characterized in that the gas is ionized by electron impact.

8. Method according to claim 2 , characterized in that the gas is ionized by irradiation with laser light.

9. Method according to claim 1 , characterized in that the gas is cooled to temperatures in the range of approximately 42 K to 60 K.

10. Method according to claim 1 , characterized in that the gas is cooled until a liquid or solid state of aggregation is reached.

11. Method according to claim 1 , characterized in that the initial pressure in the mass spectrometer is approximately 10 −9 mbar (10 −7 Pa).

Assignments (2)
CHANGE OF NAME Recorded Jul 23, 2010
From: THERMO ELECTRON (BREMEN) GMBH
To: THERMO FISHER SCIENTIFIC (BREMEN) GMBH
Reel/Frame 024733/0161 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 23, 2004
From: SCHLUTER, HANS-JURGEN
To: THERMO ELECTRON (BREMEN) GMBH
Reel/Frame 015608/0685 →
Priority Claims (1)
DE 103 21 648 · May 13, 2003 · national
Continuity (1)
Related Publication 20050001159A1 · Jan 6, 2005