IP Library Granted Patent US 7,076,025
Granted Patent B2
US 7,076,025 · App. 10/848,969 · Granted Jul 11, 2006

Method for detecting a mass density image of an object

Assignee: Illinois Institute of Technology
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Quick Facts
Patent No.
US 7,076,025
App. No.
10/848,969
Granted
Jul 11, 2006
Kind
B2
Abstract

A method for detecting a mass density image of an object. An x-ray beam is transmitted through the object and a transmitted beam is emitted from the object. The transmitted beam is directed at an angle of incidence upon a crystal analyzer. A diffracted beam is emitted from the crystal analyzer onto a detector and digitized. A first image of the object is detected from the diffracted beam emitted from the crystal analyzer when positioned at a first angular position. A second image of the object is detected from the diffracted beam emitted from the crystal analyzer when positioned at a second angular position. The first image and the second image are combined mathematically to derive a mass density image of the object.

Claims (116)

1. A method for detecting an image of an object, comprising:

transmitting an x-ray beam through the object and emitting from the object a transmitted beam;

directing the transmitted beam at an angle of incidence upon a crystal analyzer;

detecting a first image of the object from a first diffracted beam emitted from the crystal analyzer positioned at a first angular position;

detecting a second image of the object from a second diffracted beam emitted from the crystal analyzer positioned at a second angular position;

combining the first image and the second image to derive a refraction image; and

deriving a mass density image of the object from the refraction image.

2. The method of claim 1 , further comprising:

detecting the first image of the object from the first diffracted beam emitted from the crystal analyzer at a low rocking curve angle setting of the crystal analyzer, and

detecting the second image of the object from the second diffracted beam emitted from the crystal analyzer at a high rocking curve angle setting of the crystal analyzer.

3. The method of claim 1 , wherein the first image and the second image are exposed on a detector capable of producing a digitized image.

4. The method of claim 3 , wherein the exposed first image and the exposed second image are digitized.

5. The method of claim 4 , wherein the digitized images are mathematically combined to form a digitized refraction image.

6. The method of claim 5 , wherein the refraction image and the mass density image are defined on a pixel-by-pixel basis.

7. The method of claim 1 , wherein the crystal analyzer is one of a Laue crystal analyzer and a Bragg crystal analyzer.

8. The method of claim 1 , wherein the x-ray beam has an energy level of at least about 16 keV.

9. The method of claim 1 , wherein the x-ray beam has an energy level of at least about 40 kev.

10. The method according to claim 1 wherein the x-ray beam has an energy level in a range of approximately 16 keV to approximately 100 keV.

11. In a method according to claim 1 wherein the x-ray beam is diffracted by a monochromator which is matched in orientation and lattice planes to the crystal analyzer.

12. In a method according to claim 1 further comprising increasing a relative intensity of the image of the object by adjusting an angular position of the crystal analyzer.

13. In a method according to claim 12 wherein the angular position of the crystal analyzer is adjusted in steps of approximately 1 microradian increments.

14. The method of claim 1 , wherein the x-ray beam is monochromatic.

15. The method of claim 1 , wherein deriving amass density image of the object from the refraction image comprises using an algorithm including:

(

ρ

2

-

ρ

1

)

t

2

(

x

i

,

z

j

)

=

k

=

o

j

z

p

K

θ

(

x

i

,

z

j

)

.

where ρ 1 is the mass density of the matrix material, ρ 2 is the mass density of the embedded object, t 2 is the thickness of the embedded object, (x i z j ) represents a pixel in the x-z direction, and z p is the pixel size in the z-direction.

16. A method for detecting an image of an object, comprising:

transmitting an x-ray beam through the object and emitting from the object a transmitted beam;

directing the transmitted beam at an angle of incidence upon a crystal analyzer;

detecting a first image of the object from a first diffracted beam emitted from the crystal analyzer positioned at a first angular position;

detecting a second image of the object from a second diffracted beam emitted from the crystal analyzer positioned at a second angular position;

combining the first image and the second image to derive a refraction image; and

converting the refraction image to a mass density image of the object according to an algorithm comprising:

(

ρ

2

-

ρ

1

)

t

2

(

x

i

,

z

j

)

=

k

=

o

j

z

p

K

θ

(

x

i

,

z

j

)

.

where ρ 1 is the mass density of the matrix material, ρ 2 is the mass density of the embedded object, t 2 is the thickness of the embedded object (x i , z j ) represents a pixel in the x-z direction, and z p is the pixel size in the z-direction.

17. The method of claim 16 , further comprising:

detecting the first image of the object from the first diffracted beam emitted from the crystal analyzer at a low rocking curve angle setting of the crystal analyzer; and

detecting the second image of the object from the second diffracted beam emitted from the crystal analyzer at a high rocking curve angle setting of the crystal analyzer.

18. The method of claim 16 , wherein the first image and the second image each comprise a digitized image.

19. The method of claim 18 , wherein the first and second images are mathematically combined to form a digitized refraction image.

20. The method of claim 19 , wherein the refraction image and the mass density image are defined on a pixel-by-pixel basis.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 2, 2023
From: ILLINOIS INSTITUTE OF TECHNOLOGY
To: UNITED STATES GOVERNMENT
Reel/Frame 064466/0142 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 30, 2004
From: HASNAH, MOUMEN O.; CHAPMAN, LEROY DEAN
To: ILLINOIS INSTITUTE OF TECHNOLOGY
Reel/Frame 015731/0494 →
Continuity (1)
Related Publication 20050259788A1 · Nov 24, 2005