IP Library Granted Patent US 7,163,996
Granted Patent B2
US 7,163,996 · App. 10/973,128 · Granted Jan 16, 2007

Polyamides

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,163,996
App. No.
10/973,128
Granted
Jan 16, 2007
Kind
B2
Abstract

Polyamides useful as hotmelt adhesives and having improved resistance to hydrocarbons such as gasoline are obtained by reacting a) an acid component containing at least one C 6 to C 22 aliphatic dicarboxylic acid and b) an amine component containing at least one straight chain alkylene diamine having from 2 to 8 carbon atoms and at least one heterocyclic secondary diamine. The amine component may optionally also contain at least one branched chain alkylene diamine having from 3 to 10 carbon atoms and/or at least one C 24 to C 48 dimer amine.

Claims (20)

1. A polyamide which is the reaction product of a) an acid component comprising one or more C 6 to C 22 aliphatic dicarboxylic acids, wherein at least 90 mole % of said acid component is comprised of said one or more C 6 to C 22 aliphatic dicarboxylic acids and b) an amine component comprising at least one straight chain alkylene diamine having from 2 to 8 carbon atoms and at least one heterocyclic secondary diamine.

2. A polyamide according to claim 1 wherein the amine component is additionally comprised of at least one branched chain alkylene diamine having from 3 to 10 carbon atoms.

3. A polyamide according to claim 1 wherein the amine component is additionally comprised of at least one C 24 to C 48 dimer amine.

4. A polyamide according to claim 1 wherein the amine component is additionally comprised of at least one C 24 to C 48 dimer amine and at least one branched chain alkylene diamine having from 3 to 10 carbon atoms.

5. A polyamide according to claim 1 wherein the amine component comprises piperazine.

6. A polyamide according to claim 1 wherein the amine component comprises piperazine and ethylenediamine.

7. A polyamide according to claim 1 wherein the amine component comprises 2-methyl-1,5-pentanediamine.

8. A polyamide according to claim 1 wherein the acid component comprises at least one C 10 to C 14 aliphatic dicarboxylic acid.

9. A polyamide according to claim 1 wherein the amine component comprises hexamethylenediamine.

10. A polyamide according to claim 1 wherein the acid component comprises sebacic acid.

11. A polyamide according to claim 1 wherein the amine component comprises at least one straight chain alkylene diamine having from 2 to 4 carbon atoms.

12. A polyamide according to claim 1 wherein the straight chain alkylene diamine is ethylenediamine.

13. A polyamide according to claim 1 wherein the amine component additionally comprises at least one C 32 to C 40 dimer amine.

14. A polyamide according to claim 1 wherein the amine component additionally comprises at least one C 36 dimer amine.

15. A polyamide according to claim 1 wherein the amine component comprises piperazine, ethylene diamine, and 2-methyl-1,5-pentanediamine.

16. A polyamide obtained by condensation polymerization of a mixture of monomers consisting essentially of sebacic acid, ethylenediamine, piperazine, at least one dimer amine and 2-methyl-1,5-pentanediamine.

17. A polyamide obtained by condensation polymerization of a mixture of monomers consisting essentially of octadecanedicarboxylic acid, hexamethylenediamine and piperazine.

18. A polyamide according to claim 17 wherein the equivalent ratio of hexamethylenediamine:piperazine is at least 0.1:1 and is no greater than to 0.4:1.

19. A polyamide obtained by condensation polymerization of a mixture of monomers consisting essentially of a) one or more dicarboxylic acids selected from the group consisting of dodecanedicarboxylic acid and sebacic acid, b) hexamethylenediamine and c) piperazine.

20. A polyamide according to claim 19 wherein the equivalent ratio of hexamethylenediamine:piperazine is at least 0.6:1 and independently is no greater than 1.4:1.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2015
From: HENKEL US IP LLC
To: HENKEL IP & HOLDING GMBH
Reel/Frame 035100/0776 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2014
From: HENKEL CORPORATION
To: HENKEL US IP LLC
Reel/Frame 034184/0396 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2004
From: NATANIEL, TINA; HEINRICH, DWIGHT
To: HENKEL CORPORATION
Reel/Frame 015934/0025 →