IP Library Granted Patent US 7,481,974
Granted Patent B2
US 7,481,974 · App. 11/060,459 · Granted Jan 27, 2009

Method and apparatus for sterilizing containers

Assignee: Charles Sizer
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Quick Facts
Patent No.
US 7,481,974
App. No.
11/060,459
Granted
Jan 27, 2009
Kind
B2
Abstract

A method ( 20 ) and apparatus ( 100 ) for sterilizing packaging ( 102 ) is disclosed herein. The method ( 20 ) applies a solution of hydrogen peroxide onto the packaging ( 102 ) and an alkaline solution to react with the hydrogen peroxide to generate hydroxyl radicals to kill microorganism. The use of an alkaline solution allows the sterilization process to proceed at a lower temperature and a faster rate. A solution of sodium hydroxide is the preferred alkaline solution. The temperature of the process is preferably below 100° C.

Claims (28)

1. A method for sterilizing packaging, the method comprising:

applying a hydrogen peroxide solution having from 1% to 50% hydrogen peroxide to packaging, the hydrogen peroxide solution applied at a temperature ranging from 35° C. to 100° C.;

permitting the hydrogen peroxide solution to activate on the packaging for an activation period;

applying an alkaline solution to the packaging subsequent to the activation period, the alkaline solution having a pH in the range of 10-14, the alkaline solution applied at a temperature ranging from 35° C. to 100° C.; and

rinsing the packaging with sterile water to remove the residue alkaline solution and residue hydrogen peroxide.

2. The method according to claim 1 wherein the alkaline solution is a sodium hydroxide solution.

3. The method according to claim 1 wherein the alkaline solution is a solution of 0.05 Normal sodium hydroxide having a pH of approximately 12.5.

4. The method according to claim 1 wherein the hydrogen peroxide solution has a concentration of approximately 35% hydrogen peroxide.

5. The method according to claim 1 wherein the packaging is a PET bottle, a polyethylene bottle or a polypropylene bottle.

6. The method according to claim 1 wherein the solution of hydrogen peroxide is first applied to the packaging and the activation period is 30 seconds and then the alkaline solution is applied to the packaging to reaction with the hydrogen peroxide to generate hydroxyl radicals.

7. A method for sterilizing a plastic bottle, the method comprising:

applying a hydrogen peroxide solution having from 30% to 40% hydrogen peroxide to an exterior surface of the plastic bottle and an interior surface of the plastic bottle, the hydrogen peroxide solution applied at a temperature ranging from 40° C. to 60° C.;

permitting the hydrogen peroxide solution to activate on the exterior surface of the plastic bottle and the interior surface of the plastic bottle for an activation period;

applying a solution of 0.05 Normal sodium hydroxide to the exterior surface of the plastic bottle and the interior surface of the plastic bottle subsequent to the activation period, the solution of 0.05 Normal sodium hydroxide having a pH in the range of 11-13, the solution of 0.05 Normal sodium hydroxide applied at a temperature ranging from 50° C. to 75° C.; and

rinsing the packaging with sterile water to remove the residue sodium hydroxide and residue hydrogen peroxide.

8. The method according to claim 7 wherein the plastic bottle is a PET bottle, a polyethylene bottle or a polypropylene bottle.

9. The method according to claim 7 wherein the solution of hydrogen peroxide is applied as a vapor.

10. A method for sterilizing packaging at a low temperature, the method comprising:

applying a hydrogen peroxide solution having from 1% to 50% hydrogen peroxide to packaging, the hydrogen peroxide solution applied at a temperature no greater than 65° C.;

permitting the hydrogen peroxide solution to activate on the packaging for an activation period ranging from 1 second to 30 seconds;

applying an alkaline solution to the packaging subsequent to the activation period, the alkaline solution having a pH in the range of 10-14, the alkaline solution applied at a temperature no greater than 65° C.; and

rinsing the packaging with sterile water to remove the residue alkaline solution and residue hydrogen peroxide.

11. The method according to claim 10 wherein the alkaline solution is a solution of 0.05 Normal sodium hydroxide having a pH of approximately 12.5.

12. The method according to claim 10 wherein the hydrogen peroxide solution has a concentration of approximately 35% hydrogen peroxide.

13. The method according to claim 10 wherein the packaging is a PET bottle, a polyethylene bottle or a polypropylene bottle.

14. The method according to claim 10 wherein the solution of hydrogen peroxide is first applied to the packaging and the activation period is 30 seconds and then the alkaline solution is applied to the packaging to reaction with the hydrogen peroxide to generate hydroxyl radicals.

15. The method according to claim 10 further comprising filling the sterilized packaging with a food product.

16. The method according to claim 15 wherein the food product is a high acid food product.

Assignments (8)
SECURITY INTEREST Recorded Sep 10, 2019
From: DAIRYVATIVE TECHNOLOGIES, INC.
To: PAOLELLA, DAVID F.
Reel/Frame 050330/0343 →
NOTICE OF DEFAULT OF SECURITY AGREEMENT Recorded Sep 3, 2019
From: DAIRYVATIVE TECHNOLOGIES, INC.
To: PAOLELLA, DAVID F.
Reel/Frame 050255/0751 →
CHANGE OF NAME Recorded Sep 3, 2019
From: DAIRYVATIVE TECHNOLOGIES, LLC
To: DAIRYVATIVE TECHNOLOGIES, INC.
Reel/Frame 050260/0297 →
SECURITY INTEREST Recorded Jan 8, 2019
From: DAIRYVATIVE TECHNOLOGIES, INC.
To: PAOLELLA, DAVID F.
Reel/Frame 047927/0758 →
SECURITY INTEREST Recorded Dec 21, 2018
From: DAIRYVATIVE TECHNOLOGIES, INC.
To: PAOLELLA, DAVID M.
Reel/Frame 047843/0825 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 18, 2013
From: SIZER, CHARLES E.
To: DAIRYVATIVE TECHNOLOGY, LLC
Reel/Frame 029655/0444 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2007
From: UNIVERSAL FOOD AND BEVERAGE COMPANY
To: SIZER, CHARLES E
Reel/Frame 019615/0047 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 17, 2005
From: SIZER, CHARLES E.
To: UNIVERSAL FOOD & BEVERAGE CO.
Reel/Frame 016310/0065 →
Continuity (1)
Related Publication 20060182653A1 · Aug 17, 2006