Manufacturing method of metal paste
View Patent ↗A metal paste, in which a filler mainly composed of metal is mixed with good dispersibility, is manufactured with good productivity at a low cost without generating a foil of the metal. A paste-like material (referred to as a paste material hereafter) containing a metal filler is fed into a gap between a pair of rotating whetstones 11 and 12 which are relatively rotated while facing with each other having a specified gap therebetween, to pass and discharge therein. The paste material is thus kneaded and dispersed. In addition, the paste material is kneaded and dispersed by suppressing the generation of a metal foil, adjusting the gap to a specified interval dg and feeding the paste material into the interval while applying thereon a predetermined positive pressure and/or negative pressure.
1. A manufacturing method of a metal paste having a viscosity of 60(Pa·s) or larger at a measured value by a rotational viscometer rotating at a shear rate of 2s −1 , or 30(Pa·s) or larger at the measured value by the rotational viscometer rotating at a shear rate of 10s −1 , comprising:
feeding a paste-like material containing a metal filler into a gap between whetstones which are relatively rotated while facing with each other,
kneading, mixing and dispersing the paste-like material containing a metal filler while keeping the temperature of 40° C. to 80° C. so that the viscosity of the paste-like material containing a metal filler is within a range of 10 to 40(Pa·s) measured by the rotational viscometer rotating at a shear rate of 2s −1 , and within a range of 2 to 20(Pa·s) measured by the rotational viscometer rotating at a shear rate of 10s −1 ,
and by adjusting a gap interval “dg” of the whetstones in a range of (⅕) “dm” to 2 “dm” when the gap interval of the whetstones is represented by “dg” and a maximum particle size of the metal filler in the paste material is represented by “dm.”
2. The manufacturing method of the metal paste according to claim 1 , wherein the paste material is kneaded and dispersed, while applying a pressure difference of 0.01 MPa to 0.5MPa between the paste material fed into the whetstones and the paste material fed out from the whetstones.
3. The manufacturing method of the metal paste according to claim 1 , wherein the viscosity of the metal paste of 60(Pa·s) or larger at a measured value by a rotational viscometer rotating at a shear rate of 2s −1 , or the viscosity of 30(Pa·s) or larger at the measured value by the rotational viscometer rotating at a shear rate of 10s −1 are observed at room temperature.