IP Library Granted Patent US 7,419,515
Granted Patent B2
US 7,419,515 · App. 11/201,941 · Granted Sep 2, 2008

Multi-phase distillate fuel compositions and concentrates containing emulsified boric acid

Assignee: Advanced Lubrication Technology, Inc.
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Quick Facts
Patent No.
US 7,419,515
App. No.
11/201,941
Granted
Sep 2, 2008
Kind
B2
Abstract

Disclosed is a multiphase fuel composition formed of an emulsion containing (a) a distillate fuel first phase, (b) a second phase formed of boric acid and a liquid that is a solvent for boric acid, but immiscible in the first phase, such as glycerol, and (c) a surfactant.

Claims (39)

1. A multiphase distillate fuel composition comprising:

an emulsion containing

(a) a first phase comprised of a distillate fuel;

(b) a second phase, the second phase comprised of

(i) boric acid and

(ii) an organic liquid that is a solvent for boric acid, but immiscible in the first phase; and

(c) a surfactant,

wherein the concentration of boric acid is from about 5 wt. % to about 17.5 wt. %, based on the weight of the fuel composition.

2. The multiphase distillate fuel composition in accordance with claim 1 wherein the organic liquid that is a solvent for boric acid, but immiscible in the first phase is a lower alkyl polyol, acetate, acetone, methanol, ethanol, 1-propanol, 2-methyl-1-propanol, or 3-methyl-1-butanol.

3. The multiphase distillate fuel composition in accordance with claim 2 wherein the organic liquid that is a solvent for boric acid, but immiscible in the first phase is glycerol.

4. The multiphase distillate fuel composition in accordance with claim 1 wherein the second phase contains from about 10 to about 25 wt. %, boric acid and from about 90 to about 75 wt. %, liquid, based on the weight of the second phase.

5. The multiphase distillate fuel composition in accordance with claim 1 wherein the distillate fuel is diesel fuel, jet fuel, kerosene, and mixtures thereof.

6. The multiphase distillate fuel composition in accordance with claim 1 wherein the distillate fuel is low sulfur diesel fuel.

7. The multiphase distillate fuel composition in accordance with claim 1 wherein the concentration of the first phase is from about 30 to about 70 wt. %, and the concentration of the second phase is from about 30 to about 70 wt. %, based on the weight of the fuel composition.

8. The multiphase distillate fuel composition in accordance with claim 1 wherein the concentration of the first phase is from about 45 to about 55 wt. %, and the concentration of the second phase is from about 45 to about 55 wt. %, based on the weight of the fuel composition.

9. A multiphase distillate fuel composition comprising:

an emulsion containing

(a) a first phase comprised of diesel fuel, jet fuel, or kerosene;

(b) a second phase, the second phase comprised of

(i) boric acid and

(ii) glycerol; and

(c) a surfactant,

wherein the concentration of boric acid is from about 5 wt. % to about 17.5 wt %. based on the weight of the fuel composition.

10. The multiphase distillate fuel composition in accordance with claim 9 wherein the distillate fuel is low sulfur diesel fuel.

11. A multiphase distillate fuel composition comprising:

an emulsion containing

(a) a first phase comprised of a low sulfur diesel fuel;

(b) a second phase, the second phase comprised of

(i) boric acid and

(ii) an organic liquid that is a solvent for boric acid, but immiscible in the first phase; and

(c) a surfactant,

wherein the concentration of boric acid is from about 5 wt. % to about 17.5 wt. %. based on the weight of the fuel composition.

12. A multiphase distillate fuel composition according to claim 1 , wherein the boric acid has a particle size of less than 65 microns.

13. A multiphase distillate fuel composition according to claim 1 , wherein the boric acid has a particle size of about 2.5 microns to 65 microns.

14. A multiphase distillate fuel composition according to claim 1 , wherein the boric acid has a particle size of about 0.5 to about 1 micron.

15. A multiphase distillate fuel composition according to claim 1 , comprising about 0.5 to about 1.5 wt. % surfactant based on the weight of the fuel composition.

16. A multiphase distillate fuel composition according to claim 1 , wherein the surfactant is selected from the group consisting of tristyrylphenol ethoxylates, EO/PO/EO block copolymers, sodium salts of sulfonated naphthalenesulfonic acid-formaldehyde condensation products, lignosulfonates, PO/EO butanol copolymers, block copolymers of polyhydroxystearic acid and polyalkylene glycols, and partially hydrolysed or fully hydrolysed polyvinyl acetate.

17. A multiphase distillate fuel composition according to claim 1 , wherein the surfactant comprises PO/EO butanol copolymers or block copolymers of polyhydroxystearic acid and polyalkylene glycols.

18. A multiphase distillate fuel composition according to claim 1 , wherein the boric acid has a particle size of 65 microns to 100 microns.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY NAME PREVIOUSLY RECORDED AT REEL: 033254 FRAME: 0254. ASSIGNOR(S) HEREBY CONFIRMS THE LIEN. Recorded Jul 22, 2014
From: JEFFREY H. SANDS T/A NASSAU ARMS
To: ADVANCED LUBRICATION TECHNOLOGY, INC.
Reel/Frame 033378/0750 →
LIEN Recorded Jun 30, 2014
From: SCHRAGGER, ANDREW J; JEFFREY H. SANDS T/A NASSAU ARMS
To: ADVNACED LUBRIACITON TECHNOLOGY, INC.
Reel/Frame 033254/0254 →
THIRD AMENDED SEC. AGMT. Recorded Jun 27, 2012
From: ADVANCED LUBRICATION TECHNOLOGY, INC.
To: CHARLES FOSCUE, NOTES COLLATERAL AGENT FOR SECURED PARTY
Reel/Frame 028448/0471 →
SECOND AMENDED SEC. AGMT. Recorded Jun 25, 2012
From: ADVANCED LUBRICATION TECHNOLOGY, INC.
To: CHARLES FOSCUE, NOTES COLLATERAL AGENT FOR SECURED PARTY
Reel/Frame 028434/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 10, 2005
From: OLLIGES, WILLIAM E.
To: ADVANCED LUBRICATION TECHNOLOGY, INC.
Reel/Frame 016893/0163 →
Continuity (1)
Related Publication 20070033862A1 · Feb 15, 2007