Method for measuring the degree of crosslinking of pressure sensitive adhesive
A method for measuring the degree of crosslinking of pressure sensitive adhesive. The method, having the advantages of simple steps and short measuring time, comprises immersing a transparent substrate coated with a pressure sensitive adhesive in a solvent. After a specific period, the haze of the transparent substrate is measured. The obtained haze is compared with a predetermined reference, thereby determining the degree of crosslinking of the pressure sensitive adhesive.
1. A method for measuring the degree of crosslinking of pressure sensitive adhesive, comprising:
providing a transparent substrate coated with a pressure sensitive adhesive;
immersing the transparent substrate in a solvent;
measuring the haze of the transparent substrate; and
comparing the obtained haze with a predetermined reference, thereby concluding the degree of crosslinking of the pressure sensitive adhesive.
2. The method as claimed in claim 1 , wherein the transparent substrate comprises substrate employed in LCD or transparent optical film.
3. The method as claimed in claim 1 , wherein the transparent substrate is glass.
4. The method as claimed in claim 1 , wherein the transparent substrate comprises triacetate cellulose film, release film, antireflection film, or polarizing film.
5. The method as claimed in claim 1 , wherein the pressure sensitive adhesive comprises natural rubber pressure sensitive adhesive, synthetic rubber pressure sensitive adhesive, or alkene polymer pressure sensitive adhesive.
6. The method as claimed in claim 1 , wherein the pressure sensitive adhesive is polyacrylate.
7. The method as claimed in claim 1 , wherein the transparent substrate is immersed in the solvent for 2˜4 min.
8. The method as claimed in claim 1 , wherein the solvent comprises alcohol, alkane, ether, or ester.
9. The method as claimed in claim 1 , wherein the solvent comprises methanol, ethanol, n-propanol, i-propanol, n-butanol, n-hexane, ethyl ether, tetrahydrofuran, or ethyl acetate.
10. The method as claimed in claim 1 , wherein the predetermined reference indicates the relationship between haze and gel fraction.