IP Library Granted Patent US 7,201,780
Granted Patent B2
US 7,201,780 · App. 11/454,052 · Granted Apr 10, 2007

Method for dyeing textiles

Assignee: Rohm and Haas Company
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Quick Facts
Patent No.
US 7,201,780
App. No.
11/454,052
Granted
Apr 10, 2007
Kind
B2
Abstract

A method for dyeing textiles with reducible dyes in the presence of borohydride and bisulfite.

Claims (9)

1. A method for dyeing textiles with reducible dyes; said method comprising steps of: forming a dyebath by the steps comprising:

(a) forming an initial aqueous mixture comprising water, a hydroxide compound, a bisulfite compound, a borohydride compound and a reducible dye;

(b) allowing said initial aqueous mixture to stand for 1 to 3 hours; and

(c) adding additional ingredients consisting essentially of a borohydride compound, a bisulfite compound, water and optionally hydroxides, surfactants, and finishing agents and

(ii) contacting the dyebath with a textile comprising cotton;

wherein the dyebath has a pH from 9 to 11 when formed.

2. The method of claim 1 in which the bisulfite compound is added in step (a) in an amount from 65 to 180 grams per liter of the initial aqueous mixture, the borohydride compound is added in step (a) in an amount from 2 to 6 grams per liter of the initial aqueous mixture.

3. The method of claim 2 in which the dyebath has a pH from 9.5 to 10.6 when formed and the reducible dye is an indigoid dye.

4. The method of claim 3 in which the bisulfite compound is sodium bisulfite and the borohydride compound is sodium borohydride.

Assignments (11)
RELEASE OF SECURITY INTEREST Recorded Apr 14, 2026
From: PNC BANK, NATIONAL ASSOCIATION, AS AGENT
To: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
Reel/Frame 074358/0202 →
RELEASE OF SECURITY INTEREST Recorded Jul 2, 2021
From: ANTARES CAPITAL LP
To: ASCENSUS SPECIALTIES LLC; ASCENSUS SPECIALTIES CALLERY LLC
Reel/Frame 056742/0897 →
SECURITY INTEREST Recorded Jun 30, 2021
From: ASCENSUS SPECIALTIES LLC
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 056721/0304 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jun 30, 2021
From: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY, AS COLLATERAL AGENT
To: ASCENSUS SPECIALTIES LLC; ASCENSUS SPECIALTIES CALLERY LLC F/K/A CALLERY, LLC
Reel/Frame 056728/0624 →
PATENT SECURITY AGREEMENT Recorded Oct 7, 2019
From: ASCENSUS SPECIALTIES LLC; CALLERY, LLC
To: THE NORTHWESTERN MUTUAL LIFE INSURANCE COMPANY, AS AGENT
Reel/Frame 050646/0905 →
RELEASE OF SECURITY INTEREST Recorded Sep 27, 2019
From: PNC BANK, NATIONAL ASSOCIATION
To: ASCENSUS SPECIALTIES LLC
Reel/Frame 050575/0001 →
SECURITY INTEREST Recorded Sep 24, 2019
From: ASCENSUS SPECIALTIES LLC; CALLERY, LLC
To: ANTARES CAPITAL LP, AS AGENT
Reel/Frame 050470/0746 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Sep 22, 2017
From: WILMINGTON TRUST NATIONAL ASSOCIATION
To: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
Reel/Frame 043954/0261 →
SECURITY INTEREST Recorded Apr 13, 2015
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: PNC BANK, NATIONAL ASSOCIATION, AS AGENT
Reel/Frame 035389/0885 →
SECURITY INTEREST Recorded Feb 11, 2015
From: VERTELLUS PERFORMANCE CHEMICALS LLC; VERTELLUS SBH HOLDINGS LLC; VSI ACQUISITION CORP.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 034942/0131 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2007
From: SCHOOLS, HARRIE PETER
To: ROHM AND HAAS COMPANY
Reel/Frame 018998/0515 →
Continuity (2)
Provisional Application 6069114700 · Jun 16, 2005
Related Publication 20060282957A1 · Dec 21, 2006