IP Library Granted Patent US 7,757,697
Granted Patent B2
US 7,757,697 · App. 11/610,121 · Granted Jul 20, 2010

Method for reducing nitrosamines in tobacco

Assignees: Swisher International, Inc.; University of Kentucky Research Foundation
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Quick Facts
Patent No.
US 7,757,697
App. No.
11/610,121
Granted
Jul 20, 2010
Kind
B2
Abstract

Nitrosamines are reduced in tobacco by treating a whole tobacco leaf with ferulic acid. Treatment is conducted by applying an aqueous solution of ferulic acid to the whole tobacco leaf immediately before, at, or after harvesting, or fire curing the whole tobacco leaf with wood smoke containing the ferulic acid.

Claims (18)

1. A method of reducing the formation of nitrosamines in a cured tobacco comprising:

applying an aqueous solution containing a ferulic acid compound on a whole tobacco leaf, prior to curing; and curing said whole tobacco leaf.

2. The method of claim 1 , wherein the aqueous solution of said ferulic acid compound is applied on the whole tobacco leaf between immediately before to immediately after harvesting of the tobacco plant, but prior to curing.

3. The method of claim 2 , wherein said applying is conducted by dipping said whole tobacco leaf in a bath of said aqueous solution after harvesting or by spraying said aqueous solution onto said whole tobacco leaf between immediately before to immediately after harvesting.

4. The method of claim 2 , wherein said applying is conducted between about three days before harvesting and about three days after harvesting.

5. The method of claim 2 wherein the ferulic acid compound is ferulic acid, an ester of ferulic acid, or both, and said aqueous solution comprises said ferulic acid compound, a surfactant and water.

6. The method of claim 2 , wherein said aqueous solution comprises said ferulic acid compound in an amount of about 0.1% to about 1% weight by volume, a surfactant and water.

7. The method of claim 2 , wherein said aqueous solution is applied to said whole tobacco leaf prior to harvest in an amount of about 50 gallons per acre.

8. The method of claim 2 , wherein said aqueous solution is applied to said whole tobacco leaf in an amount of about 0.01 ml per square inch of leaf.

9. The method of claim 5 , wherein said aqueous solution further comprises an alcohol.

10. The method of claim 6 , wherein said aqueous solution comprises said ferulic acid compound in an amount of about 0.2 to about 0.6% weight by volume.

11. The method of claim 6 , wherein said aqueous solution comprises said ferulic acid compound in an amount of about 0.25 to about 0.5% weight by volume.

12. The method of claim 6 , wherein said aqueous solution comprises said surfactant in an amount of about 0.1 to about 0.5% weight by volume.

13. The method of claim 6 , wherein said aqueous solution comprises said surfactant in an amount of about 0.2 to about 0.3% weight by volume.

14. The method of claim 9 , wherein said aqueous solution comprises said alcohol in an amount of about 1 to about 20% weight by volume.

15. The method of claim 14 , wherein said aqueous solution comprises said alcohol in an amount of about 1 to about 10% weight by volume.

16. The method of claim 6 , wherein said aqueous solution comprises 0.25% weight by volume of said ferulic acid compound and 0.25% weight by volume of said surfactant.

17. The method of claim 16 , wherein said aqueous solution further comprises a 2% ethanol solution.

Assignments (6)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS (RECORDED 4/25/2012 AT REEL/FRAME 28275/0661) Recorded Nov 24, 2014
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: SWISHER INTERNATIONAL, INC.
Reel/Frame 034443/0346 →
SECURITY AGREEMENT Recorded May 25, 2012
From: SWISHER INTERNATIONAL, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 028275/0661 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2006
From: BAILEY, WILLIAM A., DR.
To: UNIVERSITY OF KENTUCKY RESEARCH FOUNDATION
Reel/Frame 018626/0050 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2006
From: BRANDON, JOHN, MR.
To: SWISHER INTERNATIONAL, INC.
Reel/Frame 018626/0159 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2006
From: LOSTY, THOMAS, MR.
To: SWISHER INTERNATIONAL, INC.
Reel/Frame 018626/0285 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2006
From: THOMAS, TERRY, MR.
To: SWISHER INTERNATIONAL, INC.
Reel/Frame 018626/0590 →
Continuity (2)
Provisional Application 6075368300 · Dec 22, 2005
Related Publication 20070149408A1 · Jun 28, 2007