IP Library Granted Patent US 7,521,394
Granted Patent B2
US 7,521,394 · App. 11/615,702 · Granted Apr 21, 2009

Nanoparticles containing titanium oxide

Assignee: The Board of Trustees of the University of Illinois
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Quick Facts
Patent No.
US 7,521,394
App. No.
11/615,702
Granted
Apr 21, 2009
Kind
B2
Abstract

A titanium oxide nanoparticle includes anatase titanium oxide, and may be a nanofiber having a minimum dimension less than 200 nanometers and having an aspect ratio greater than 20:1. A titanium oxide nanoparticle including anatase titanium oxide may include a dopant metal and/or a dopant nonmetal, and may be in a form other than a nanosphere. A method of making nanoparticles includes heating a reaction mixture in an autoclave, where the reaction mixture includes a titanium source and a polar organic solvent.

Claims (24)

1. A nanofiber, comprising:

anatase titanium oxide,

where the nanofiber has a longest dimension of at least 2 micrometers, and an aspect ratio greater than 20:1.

2. The nanofiber of claim 1 , having a longest dimension of at least 5 micrometers.

3. The nanofiber of claim 1 , further comprising at least one element selected from the group consisting of a dopant metal and a dopant nonmetal.

4. The nanofiber of claim 3 , comprising a dopant metal selected from the group consisting of calcium, cobalt, nickel, copper, gallium, strontium, yttrium, zirconium, palladium, silver, tin, lanthanum and platinum.

5. The nanofiber of claim 4 , comprising a dopant nonmetal selected from the group consisting of boron, carbon, nitrogen, sulfur and fluorine.

6. The nanofiber of claim 3 , comprising a dopant nonmetal selected from the group consisting of boron, carbon, nitrogen, sulfur and fluorine.

7. The nanofiber of claim 1 , where the nanofiber is a nanobelt having a thickness of at most 10 nanometers.

8. The nanofiber of claim 1 , where the nanofiber is a nanosheet having a width greater than 200 nanometers.

9. The nanofiber of claim 1 , where the nanofiber is a nanoprism.

10. The nanofiber of claim 1 , where the nanofiber is a nanowire having a longest dimension of at least 1,000 nanometers.

11. A nanoparticle, comprising:

anatase titanium oxide, and

at least one element selected from the group consisting of a dopant metal and a dopant nonmetal;

where the nanoparticle is not a nanosphere, and

the nanoparticle has a longest dimension of at least 2 micrometers.

12. The nanoparticle of claim 11 , comprising a dopant metal selected from the group consisting of calcium, cobalt, nickel, copper, gallium, strontium, yttrium, zirconium, palladium, silver, tin, lanthanum and platinum.

13. The nanoparticle of claim 12 , comprising a dopant nonmetal selected from the group consisting of boron, carbon, nitrogen, sulfur and fluorine.

14. The nanoparticle of claim 11 , comprising a dopant nonmetal selected from the group consisting of boron, carbon, nitrogen, sulfur and fluorine.

15. The nanoparticle of claim 11 , where the nanoparticle is in a form selected from the group consisting of a nanowire, a nanobelt, a nanosheet, and a nanoprism.

16. The nanoparticle of claim 15 , where the nanoparticle is a nanobelt having a thickness of at most 10 nanometers.

17. The nanoparticle of claim 15 , where the nanoparticle is a nanosheet having a width greater than 200 nanometers.

18. The nanoparticle of claim 15 , where the nanoparticle is a nanoprism.

Assignments (4)
CONFIRMATORY LICENSE Recorded May 23, 2011
From: UNIVERSITY OF ILLINOIS URBANA-CHAMPAIGN
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 026322/0600 →
CONFIRMATORY LICENSE Recorded Aug 11, 2009
From: UNIVERSITY OF ILLINOIS URBANA-CHAMPAIGN
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 023077/0255 →
CONFIRMATORY LICENSE Recorded Aug 10, 2009
From: UNIVERSITY OF ILLINOIS URBANA-CHAMPAIGN
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 023071/0276 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 13, 2007
From: XIE, RONG-CAI; SHANG, JIAN-KU; WU, PINGGUI
To: THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Reel/Frame 019687/0272 →
Continuity (2)
Provisional Application 6075468000 · Dec 29, 2005
Related Publication 20070202334A1 · Aug 30, 2007