IP Library Granted Patent US 7,651,712
Granted Patent B2
US 7,651,712 · App. 11/732,018 · Granted Jan 26, 2010

Process for drying high-lactose aqueous fluids

Assignee: Relco Unisystems Corporation
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Quick Facts
Patent No.
US 7,651,712
App. No.
11/732,018
Granted
Jan 26, 2010
Kind
B2
Abstract

A method for processing a high-lactose aqueous fluid (HLAF), such as permeate from ultrafiltration of whey fluid, is provided. The process includes introducing a highly concentrated high-lactose aqueous fluid into a cooling, concentrating, crystallizing apparatus in which the highly concentrated high-lactose aqueous fluid is exposed to mixing and to movement of a gaseous fluid at a temperature, moisture content and air speed effective to create a cooling, concentrating, crystallizing cascade to generate a partially crystallized high-lactose aqueous fluid and spraying the partially crystallized high-lactose aqueous fluid into an enclosed drying chamber containing hot air to form a high-solids crystalline product rich in crystalline alpha-lactose monohydrate crystals.

Claims (3)

1. A method of crystallizing lactose from a concentrated whey permeate, wherein whey permeate comprises at least about 78% total solids, including at least about 50% lactose and the temperature of the whey permeate is greater than about 50 degrees Celsius, the method comprising the steps of:

introducing the whey permeate into a cooling, concentrating, crystallizing apparatus in which the whey permeate is exposed both to mixing and to movement of a gaseous fluid at a temperature, moisture content and air speed effective to create a cooling, concentrating, crystallizing cascade in which evaporative cooling causes loss of moisture and an increase in solids which in turn facilitate lactose crystallization which in turn releases lactose's heat of crystallization which in turn increases fluid temperature which in turn facilitates more evaporative cooling, so that a whey permeate with an equilibrium of lactose in solution and lactose in crystallized form is generated; and

spraying the whey permeate into an enclosed drying chamber containing hot air to form a product rich in crystalline alpha-lactose monohydrate crystals.

Assignments (5)
NOTICE OF PATENT SECURITY INTEREST AGREEMENT (REPLACES DOCUMENT RECORDED AT REEL 065426 FRAME 0044) Recorded Dec 12, 2023
From: RELCO, LLC; KOVALUS SEPARATION SOLUTIONS, LLC
To: CERBERUS BUSINESS FINANCE AGENCY, LLC, AS AGENT
Reel/Frame 065966/0967 →
NOTICE OF PATENT SECURITY INTEREST AGREEMENT Recorded Nov 1, 2023
From: RELCO, LLC; KOVALUS SEPARATION SOLUTIONS, LLC
To: CERBERUS BUSINESS FINANCE AGENCY, LLC, AS AGENT
Reel/Frame 065426/0044 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2023
From: KELLER, A. KENT
To: KELLER TECHNOLOGIES, INC.
Reel/Frame 064687/0930 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2023
From: KELLER TECHNOLOGIES, INC.
To: RELCO UNISYSTEMS CORPORATION
Reel/Frame 064687/0934 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2020
From: RELCO UNISYSTEMS CORPORATION
To: RELCO LLC
Reel/Frame 053615/0391 →
Continuity (1)
Related Publication 20070184170A1 · Aug 9, 2007