IP Library Granted Patent US 7,648,643
Granted Patent B1
US 7,648,643 · App. 11/765,868 · Granted Jan 19, 2010

Metal recovery process and method

Assignee: Phitex, L.L.L.P.
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Quick Facts
Patent No.
US 7,648,643
App. No.
11/765,868
Granted
Jan 19, 2010
Kind
B1
Abstract

A process and composition of matter for the recovery of metal from a metal-laden ore, soil or rock is provided. A liquid, non-toxic, low pH acidic composition is used as a chelating agent that extracts the metal into a pregnant liquid solution. The pregnant solution is treated by known conventional means, such as filtration, centrifuging, or electrolysis to remove the extracted metals. The low pH, acidic composition (LpHAC) does not have any known toxicity to man or the environment and performs as an ideal fluidized reaction metal extractant. As a metal extracting agent, it effectively and efficiently extracts gold and other metals from ore laden soil or rock with no environmental and negative health impact.

Claims (7)

1. A composition of matter for extracting metal ions from a metal containing ore, consisting essentially of:

a) a product prepared by the process of combining a high purity acid selected from at least one of phosphoric acid, fumaric acid or acetic acid with water selected from at least one of deionized water and filtered water and an ammonium compound selected from at least one of anhydrous ammonia and buffered ammonium nitrate used in a ratio of approximately 1 lb. to approximately 5 lbs. of ammonium compound per gallon of water, heating the mixture to approximately 140° F. to form mixture (I), placing mixture (I) in a pressurized vessel and heating the mixture to temperatures in a range between approximately 250 F. and approximately 400 F., then, cooling the mixture, and after the mixture is cooled, adding a stabilizing amount of the starting mixture (I) forming a low PH acid (LpHAC) product that is not an irritant; and

b) water selected from the group consisting of fresh water, sea water, brine, and a mixture thereof is combined with the product from a) to form an aqueous metal extracting solution that extracts metal ions from a metal-laden ore in soil and rock at a recovery rate between approximately 75% and 98% of total metal in the ore.

2. The composition of matter of claim 1 , wherein the mixing ratio of water to low pH acid (LpHAC) product is in a range between approximately 1% to 90% water to approximately 10 to 99% LpHAC product.

3. A composition of matter for extracting metal ions from a metal containing ore, consisting essentially of:

a product prepared by the process of combining a high purity acid selected from at least one of phosphoric acid, fumaric acid or acetic acid with water selected from at least one of deionized water and filtered water and an ammonium compound selected from at least one of anhydrous ammonia and buffered ammonium nitrate used in a ratio of approximately 1 lb. to approximately 5 lbs, of ammonium compound per gallon of water, heating the mixture to approximately 140° F. to form mixture (I), placing mixture (I) in a pressurized vessel and heating the mixture to temperatures in a range between approximately 250 F. and approximately 400 F., then, cooling the mixture, and after the mixture is cooled, adding a stabilizing amount of the starting mixture (I) forming a low PH acid (LpHAC) product that extracts metal ions from a metal-laden ore in soil and rock at a recovery rate between approximately 75% and 98% of total metal in the ore.

4. The composition of matter of claim 3 , wherein the composition is 100% of the liquid, low pH acid (LpHAC) product which extracts metal ions from a metal-laden ore in soil and rock at a recovery rate between approximately 75% and 98% of total metal in the ore.

Assignments (5)
MERGER Recorded Dec 30, 2013
From: CMS HOLDINGS, LLC
To: CMS INNOVATIVE TECHNOLOGIES, INC.
Reel/Frame 031857/0763 →
CHANGE OF NAME Recorded Dec 30, 2013
From: CONTACT MARKETING SOLUTIONS, LLC
To: CMS HOLDINGS, LLC
Reel/Frame 031876/0496 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2011
From: PHITEX MEIP, LLC
To: CONTACT MARKETING SOLUTIONS, LLC
Reel/Frame 026302/0387 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 14, 2008
From: PHITEX, LLLP
To: PHITEX MEIP, LLC
Reel/Frame 020358/0544 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2007
From: CREASEY, DAVID H
To: PHITEX, LLLP
Reel/Frame 019456/0721 →
Continuity (1)
Provisional Application 6081550000 · Jun 21, 2006