IP Library Granted Patent US 7,627,438
Granted Patent B1
US 7,627,438 · App. 11/796,205 · Granted Dec 1, 2009

Observer based

Assignee: Iowa State University Research Foundation, Inc.
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Quick Facts
Patent No.
US 7,627,438
App. No.
11/796,205
Granted
Dec 1, 2009
Kind
B1
Abstract

An observer based Q control method for a cantilever in an atomic force microscopy is provided that provides for a “dual” Q behavior such that a particular effective Q is achieved when a sample is present and another effective Q when a sample is absent. In the control method, the transfer function from dither input to photo-diode output is independent of the observer so that the cantilever effectively behaves like a spring-mass-damper system. The effective quality factor and stiffness of the cantilever can be changed by appropriately choosing the state feedback gain. The method provides sample-imaging using transient atomic force microscopy.

Claims (163)

1. A method to perform high-speed high resolution imaging of a sample from detecting transient cantilever movement in an atomic force microscope, the cantilever having a tip, the method comprising the steps of:

receiving an input dither signal and tip deflection data corresponding to the input dither signal;

generating an innovation signal based upon the input dither signal and tip deflection data, the innovation signal having a dynamic profile of unknown arrival time and unknown magnitude with additive white noise;

computing maximum likelihood estimates of the arrival time and magnitude using a likelihood ratio test;

deriving an image of the sample using the maximum likelihood estimates of the arrival time and magnitude; and

wherein the likelihood ratio test is in accordance with

r

(

M

)

=

e

_

T

e

_

T

V

where V is a covariance matrix, ē=[e 1 , e 2 , . . . , e M ] T , and e is an error in an estimate of the output of an observer.

2. The method of claim 1 wherein the step of generating the innovation signal comprises the step of generating the innovation signal according to

e

(

s

)

=

η

(

s

)

+

(

s

2

+

ω

0

Q

s

+

ω

0

2

)

υ

(

s

)

+

(

s

+

ω

0

Q

)

v

1

+

v

2

s

2

+

(

ω

0

Q

+

l

1

)

s

+

(

ω

0

2

+

l

2

+

ω

0

Q

l

1

)

where L=[l 1 l 2 ] T is an observer gain such that

(

ω

0

Q

+

l

1

)

>

0

and

(

ω

0

2

+

ω

0

Q

l

1

+

l

2

)

>

0

,

ω 0 is the resonant frequency, ν is measurement noise, η is thermal noise, Q is the quality factor and v=[v 1 , v 2 ] is a state-jump that occurs when the cantilever tip hits the sample surface.

3. The method of claim 1 further comprising the step of comparing a likelihood ratio from the likelihood ratio test to a threshold value to arrive at a decision whether the dynamic profile is present.

4. The method of claim 3 wherein the threshold value is chosen such that a false alarm rate is below a predefined level.

5. The method of claim 3 wherein the threshold value is chosen such that a detection probability is above a predefined level.

6. A method to perform transient imaging of a sample from detecting transient cantilever movement in an atomic force microscope using Q control, the cantilever having a tip, the method comprising the steps of:

receiving an input dither signal and tip deflection data corresponding to the input dither signal;

generating an estimated position and an estimate velocity of the tip;

generating an innovation signal based upon the input dither signal, the tip deflection data, the estimated position and the estimated velocity, the innovation signal having a dynamic profile of unknown arrival time and unknown magnitude with additive white noise;

computing maximum likelihood estimates of the arrival time and magnitude using a likelihood ratio test;

deriving an image of the sample using the maximum likelihood estimates of the arrival time and magnitude; and

further comprising the step of adding the estimated position and the estimate velocity in a feedback loop to add to the input dither signal, thereby actively damping a quality factor (“Q”) of the cantilever.

7. The method of claim 6 further comprising the step of comparing a likelihood ratio from the likelihood ratio test to a threshold value to arrive at a decision whether the dynamic profile is present.

8. The method of claim 7 wherein the threshold value is chosen such that a false alarm rate is below a predefined level.

9. The method of claim 7 wherein the threshold value is chosen such that a detection probability is above a predefined level.

10. A method to perform transient imaging of a sample from detecting transient cantilever movement in an atomic force microscope using Q control, the cantilever having a tip, the method comprising the steps of:

receiving an input dither signal and tip deflection data corresponding to the input dither signal;

generating an estimated position and an estimate velocity of the tip;

generating an innovation signal based upon the input dither signal, the tip deflection data, the estimated position and the estimated velocity, the innovation signal having a dynamic profile of unknown arrival time and unknown magnitude with additive white noise;

computing maximum likelihood estimates of the arrival time and magnitude using a likelihood ratio test;

deriving an image of the sample using the maximum likelihood estimates of the arrival time and magnitude; and

further comprising the step of adding the estimated position and the estimate velocity in a feedback loop to add to the input dither signal, thereby actively enhancing a quality factor (“Q”) of the cantilever.

11. A method to perform transient imaging of a sample from detecting transient cantilever movement in an atomic force microscope using Q control, the cantilever having a tip, the method comprising the steps of:

receiving an input dither signal and tip deflection data corresponding to the input signal;

generating an estimated position and an estimate velocity of the tip;

generating an innovation signal based upon the input dither signal, the tip deflection data, the estimated position and the estimated velocity, the innovation signal having a dynamic profile of unknown arrival time and unknown magnitude with additive white noise;

computing maximum likelihood estimates of the arrival time and magnitude using a likelihood ratio test;

deriving an image of the sample using the maximum likelihood estimates of the arrival time and magnitude;

wherein the step of generating an estimated position and an estimate velocity comprises the step of generating an estimated position and an estimate velocity using an observer; and

wherein dynamics of the observer are given in accordance with:

{circumflex over ({dot over (x)})}=A{circumflex over (x)}+Bu+L ( y−C{circumflex over (x)} ); {circumflex over (x)} (0)= {circumflex over (x)} 0

u= ( g+F{circumflex over (x)} )

{circumflex over (p)}=C{circumflex over (x)}

{circumflex over (ν)}=D{circumflex over (x)}

where {circumflex over ({dot over (x)})} is the estimate dynamic state of the cantilever, L is the observer gain, F is the state feedback gain, g is the input dither signal, {circumflex over (p)} is the estimate position, A, B, C, and D are state matrices realized from the frequency response from a dither-piezo input to a photo-diode output, u is the dither-piezo input, y is the photo-diode output, and {circumflex over (ν)} is the estimated velocity.

12. The method of claim 11 wherein a transfer function from dither input to photo-diode output is independent of the observer.

13. The method of claim 11 wherein the state feedback gain F does not affect the effective resonant frequency of the cantilever.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 15, 2017
From: IOWA STATE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 042014/0110 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 25, 2007
From: SALAPAKA, MURTI V.; SAHOO, DEEPAK RANJAN
To: IOWA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 019343/0606 →
Continuity (1)
Provisional Application 6074596800 · Apr 28, 2006