IP Library Granted Patent US 7,713,459
Granted Patent B2
US 7,713,459 · App. 11/812,854 · Granted May 11, 2010

Cellulose fiber for using as industrial materials

Assignee: HYOSUNG Corporation
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Quick Facts
Patent No.
US 7,713,459
App. No.
11/812,854
Granted
May 11, 2010
Kind
B2
Abstract

The present invention relates to cellulose fiber containing 500 to 2000 of filaments and having homogeneous physical properties and the multi-filaments according to the present invention is characterized in that the strength and the breaking elongation of the multi-filaments are 4 to 9 g/d and 4 to 15%, respectively. In particular, the present invention is characterized in that each mono-filament selected 100 strands from every three part divided from multi-filaments has properties as following: (a) 3 to 9 g/d in average strength, 7 to 15% in average breaking elongation and 0.035 to 0.055 in by birefringence, (b) the differences of the above three parts are below 1.0 g/d in average strength, 1.5% in breaking elongation and 0.7 denier in denier, (c) the CV (%) (coefficient of variation) of the above three parts are below 10%, and (d) the birefringence differences of the above three parts are below 0.004.

Claims (15)

1. A method of producing a cellulose fiber comprising the steps of:

(A) preparing a cellulose solution by swelling and homogenizing a cellulose powder having a diameter no more than 300 μm into an aqueous concentrated N-methyl morpholine N-oxide (NMMO) solution with 10 to 15 wt % of moisture;

(B) passing the cellulose solution through a distributing plate having 50 to 300 holes having a diameter of 50 to 200 mm;

(C) obtaining multi-filaments by spinning the cellulose solution with a spinning nozzle having 500 to 2000 orifices and subsequently precipitating the cellulose solution into a coagulating bath through an air gap; and

(D) water-washing, drying, treating with a finishing oil and winding the multi-filaments, which filaments so produced which have the following physical properties:

(1) 700 to 3000 in denier of the multi-filaments;

(2) 4 to 9 g/d and 4 to 15% in strength and breaking elongation of the multi-filaments, respectively;

(3) when the multi-filaments are divided into three parts and 100 mono-filaments selected from each part of the three parts have the following physical properties;

a) 3 to 9 g/d in strength, 7 to 15% in breaking elongation and 0.035 and 0.055 birefringence, respectively;

b) the differences of average strength, average breaking elongation and average denier are less than 1.0 g/d, 1.5% and 0.7 denier, respectively;

c) CV (coefficient of variation) of average strength, average breaking elongation and denier of the three parts less than 10%; and

d) the differences of average birefringence of the three parts are less than 0.004.

2. The method according to claim 1 , wherein air at 5 to 30° C. in temperature and 10 to 60% in humidity is blown into the air gap at an air speed of 3 to 12 m/sec.

3. The method according to claim 1 , wherein the temperature of the coagulating bath is 0 to 35° C.

4. The method according to claim 1 , wherein the drying is performed with a drying roller at 80 to 170° C.

Assignments (2)
CHANGE OF NAME Recorded Feb 27, 2025
From: HYOSUNG ADVANCED MATERIALS CORPORATION
To: HS HYOSUNG ADVANCED MATERIALS CORPORATION
Reel/Frame 070355/0207 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2018
From: HYOSUNG CORPORATION
To: HYOSUNG ADVANCED MATERIALS CORPORATION
Reel/Frame 048963/0092 →
Priority Claims (1)
KR 10-2004-0092051 · Nov 11, 2004 · national
Continuity (2)
Division 1104766700 · Feb 2, 2005
Related Publication 20070241477A1 · Oct 18, 2007