X-ray analysis apparatus
View Patent ↗When an X-ray focused by using an X-ray lens is irradiated to a sample, there is generated an X-ray halo component at the peripheral part of the focal point of the focused X-ray in the sample and, by this, precision of an analysis of a microscopic region becomes an issue. In order to control the shape of the X-rays from the X-ray lens, a collimator is installed between the X-ray lens and the sample, with an opening part having a tapering shape in which the opening at the side toward the sample is made smaller than that at the side toward the X-ray lens.
1. An X-ray analysis apparatus comprising:
an X-ray tubular bulb configured to generate an X-ray;
an X-ray lens having one end which receives the X-ray from the X-ray tubular bulb and another end which emits the focused X-ray onto a sample;
a collimator provided between said another end of the X-ray lens and the sample at non-zero distances away therefrom, the collimator having an opening formed therethrough which is shaped to have cross-sections substantially equal to or smaller than corresponding cross-sections of the focused X-ray passing through the opening; and
a detector configured to detect a fluorescent X-ray excited out from the sample by the focused X-ray allowed through the opening of the collimator.
2. An X-ray analysis apparatus according to claim 1 , wherein the opening of the collimator is shaped to have the cross-sections substantially equal to the corresponding cross-sections the focused X-rays passing through the opening.
3. An X-ray analysis apparatus according to claim 1 , wherein the opening of the collimator is shaped to have the cross-sections smaller than the corresponding cross-sections of the focused X-rays passing through the opening.
4. An X-ray analysis apparatus according to claim 3 , wherein the opening is shaped to have the cross-sections each smaller by a constant rate than a corresponding cross-section of the focused X-ray passing through the opening.
5. An X-ray analysis apparatus according to claim 4 , wherein the constant rate is about 20%.
6. An X-ray analysis apparatus according to claim 1 , wherein the collimator is positioned closer to the sample than to the X-ray lens.
7. An X-ray analysis apparatus according to claim 1 , wherein the detector has a function detecting the X-ray.
8. An X-ray analysis apparatus according to claim 1 , wherein the X-ray lens is made of a polycapillary.
9. An X-ray analysis apparatus according to claim 1 , wherein the opening is shaped to become generally narrower from an X-ray entrance thereof towards an X-ray exit thereof.
10. An X-ray analysis apparatus according to claim 1 , wherein the opening has a cross-section of a shape other than a circle.
11. An X-ray analysis apparatus according to claim 1 , wherein the opening has a peripheral wall which is concave in shape.
12. An X-ray analysis apparatus according to claim 1 , further comprising at least one other collimator having an opening of a shape different from that of the opening of the collimator.
13. An X-ray analysis apparatus according to claim 1 , wherein the collimator has a thickness of about 1 mm.
14. An X-ray analysis apparatus according to claim 1 , wherein the X-ray tubular bulb generates the X-ray at a maximum energy of 50 KV sufficiently strong to emit an innegligible amount of halo X-ray onto the sample without the collimator.
15. An X-ray analysis apparatus according to claim 1 , further comprising a case surrounding the X-ray lens configured to block halo X-ray from the X-ray lens.