IP Library Granted Patent US 7,638,076
Granted Patent B2
US 7,638,076 · App. 11/977,827 · Granted Dec 29, 2009

Method and system for pelletizing sulfur

Assignee: Martin Resource Management Corporation
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Quick Facts
Patent No.
US 7,638,076
App. No.
11/977,827
Granted
Dec 29, 2009
Kind
B2
Abstract

Relatively uniform spherical shaped solid pellets (prills) may be created by passing molten sulfur through a nested strainer to remove particles that would otherwise become trapped in the system, a drip tray with a heating channel attached on its underside, an injection conduit for delivery of a cooled zone of water to create solid prills, and thereafter moving the prills through a stationary curved screen to remove most of the excess water and a vibrating screen.

Claims (93)

1. A system for converting molten sulfur to sulfur prills, comprising:

a heated removable strainer for removing non-sulfur particles from the molten sulfur;

the removable strainer coupled to a drip tray wherein the removable strainer having at least two nested filters;

a first conduit attached to the drip tray for heating the drip tray;

the molten sulfur traversing to the drip tray forming sulfur droplets;

a tank storing a media, said media comprising a first media and a second media;

a second conduit for delivering the first media to a first area of the tank;

a third conduit for delivering the second media to a second area of the tank;

the sulfur droplets traversing a distance from the drip tray to the media in the tank; and

relatively spherical shaped sulfur prills formed by the interaction of the sulfur droplets with the media.

2. A system for converting molten sulfur to sulfur prills, comprising:

a heated removable strainer for removing non-sulfur particles from the molten sulfur wherein the removable strainer is heated by steam;

the removable strainer coupled to a drip tray;

a first conduit attached to the drip tray for heating the drip tray;

the molten sulfur traversing to the drip tray forming sulfur droplets;

a tank storing a media, said media comprising a first media and a second media;

a second conduit for delivering the first media to a first area of the tank;

a third conduit for delivering the second media to a second area of the tank;

the sulfur droplets traversing a distance from the drip tray to the media in the tank; and

relatively spherical shaped sulfur prills formed by the interaction of the sulfur droplets with the media.

3. The system of claim 2 , wherein the removable strainer having an overflow conduit.

4. The system of claim 2 wherein the first media is relatively cooler than the second media.

5. A system for converting molten sulfur to sulfur prills, comprising:

a heated removable strainer for removing non-sulfur particles from the molten sulfur;

the removable strainer coupled to a drip tray;

a first conduit attached to the drip tray for heating the drip tray;

the molten sulfur traversing to the drip tray forming sulfur droplets;

a tank storing a media, said media comprising a first media and a second media wherein the first media is relatively cooler than the second media;

a second conduit for delivering the first media to a first area of the tank;

a third conduit for delivering the second media to a second area of the tank;

the sulfur droplets traversing a distance from the drip tray to the media in the tank, and relatively spherical shaped sulfur prills formed by the interaction of the sulfur droplets with the media;

an output port having a cross sectional rectangular shape, the output port coupled to the tank, and the spherical sulfur prills exiting the tank from the output port;

a screen having a curved shape for removing the media from the spherical sulfur prills;

a vibrating screen for removing fines from the spherical sulfur prills;

a first sensor for detecting an amount of the media in the tank and a second sensor for detecting an amount of the spherical sulfur prills in the tank, said first sensor and said second sensor coupled to a computer processing unit wherein the computer processing unit coupled to the output port and said output port having an open position and a closed position and

a storage tank coupled to the output port and a hydro-cyclone coupled to the storage tank.

6. The system of claim 5 , wherein the storage tank having a top section and a bottom section and said bottom section having a conical shape.

7. A method for converting molten sulfur into sulfur prills, comprising the steps of:

heating a strainer and a drip tray;

injecting molten sulfur through the strainer and the drip tray;

forming sulfur droplets in the drip tray from the molten sulfur;

injecting a first media and a second media into a forming tank wherein the first media and second media are water and the first media is relatively cooler than the second media, wherein the first media creating a sulfur prill forming zone in the tank; and

dropping the sulfur droplets from the drip tray into the tank a distance certain from the forming zone of the forming tank.

8. The method of claim 7 , wherein the strainer having a plurality of nested filters.

9. The method of claim 7 , wherein the distance certain is approximately 2 inches.

10. A method for converting molten sulfur into sulfur prills, comprising the steps of:

heating a strainer and a drip tray;

injecting molten sulfur through the strainer and the drip tray;

forming sulfur droplets in the drip tray from the molten sulfur;

injecting a first media and a second media into a forming tank wherein the first media and second media are water and the first media is relatively cooler than the second media, wherein the first media having a temperature range of 55-60° F. and the second media having a temperature range of 95-105° F., wherein the first media creating a sulfur prill forming zone in the tank; and

dropping the sulfur droplets from the drip tray into the tank a distance certain from the forming zone of the forming tank.

11. A system for converting molten sulfur to sulfur prills, comprising:

filtering means for removing non-sulfur particles from the molten sulfur wherein the filtering means having at least two nested filters and said filtering means coupled to a sulfur forming droplet means;

heating means coupled to only one side of the sulfur forming droplet means; said molten sulfur traversing to the sulfur forming droplet means to form sulfur droplets;

a tank storing a media, said media comprising a first media and a second media;

a first conduit for introducing the first media to a first area of the tank;

a second conduit for introducing the second media to a second area of the tank;

the sulfur droplets traversing a distance from the sulfur forming droplet means to the media in the tank; and

relatively spherical shaped sulfur prills formed by interaction of the sulfur droplets with the media, wherein the filtering means having at least two nested filters.

12. The system of claim 11 , wherein the media, the first media and the second media are water.

13. The system of claim 12 further comprising a second heating means for heating the filter means.

14. The system of claim 13 , wherein the heating means and the second heating means comprising steam.

15. The system of claim 14 , wherein the first media is relatively cooler than the second media.

16. The system of claim 14 , wherein the first media having a temperature range of 55-60° F. and the second media having a temperature range of 95-105° F.

17. The system of claim 15 , wherein the first conduit having a plurality of orifices.

18. The system of claim 16 , wherein the spherical sulfur prills having a low moisture content.

19. The system of claim 18 , wherein the low moisture content is less than 2.2 percent.

20. The system of claim 15 further comprising an output means, the output means coupled to the tank, wherein the spherical sulfur prills exiting the tank from the output means.

21. The system of claim 20 , wherein the output means having a cross sectional rectangular shape.

22. The system of claim 20 further comprising first means for removing excess water from the relatively spherical sulfur prills and second means for removing fines from the relatively spherical sulfur prills.

23. The system of claim 22 , wherein the first means for removing the excess water from the relatively spherical sulfur prills having a curved shape.

24. A system for converting molten sulfur to sulfur prills, comprising:

means having at least two filters in series for removing non-sulfur particles from the molten sulfur;

said means coupled to a drip tray;

a first conduit attached to the drip tray for heating the drip tray;

the molten sulfur traversing to the drip tray forming sulfur droplets;

a second means for storing a media, said media comprising a first media and a second media;

a second conduit for delivering the first media to a first area of said second means;

a third conduit for delivering the second media to a second area of said second means;

the sulfur droplets traversing a distance from the drip tray to the media in said second means; and

relatively spherical shaped sulfur prills formed by the interaction of the sulfur droplets with the media.

25. The system of claim 24 wherein the first media is relatively cooler than the second media.

26. A method for converting molten sulfur into sulfur prills, comprising the steps of:

injecting molten sulfur through a strainer and a drip tray;

forming sulfur droplets in the drip tray from the molten sulfur;

creating a forming zone and a non-forming zone in a tank; and

dropping the sulfur droplets from the drip tray into the forming zone to create the sulphur prills, wherein the forming zone is relatively cooler than the non-forming zone of the tank.

27. The method of claim 26 wherein the forming zone having a temperature range of 55-60° F. and the non-forming zone having a temperature range of 95-105° F.

28. The method of claim 27 wherein the forming zone and non-forming zone comprising a liquid.

29. The method of claim 28 wherein the liquid is water.

30. The method of claim 26 further comprising the step of dropping the sulphur prills onto a screen.

31. The method of claim 30 wherein the screen is a curved screen.

32. The method of claim 26 further comprising the step of measuring the temperatures of the forming zone and non-forming zone and regulating the temperature of the forming zone by injecting a cooling media.

Assignments (10)
CHANGE OF NAME Recorded Jul 27, 2018
From: SANDVIK PROCESS SYSTEMS, LLC
To: IPCO US LLC
Reel/Frame 047270/0499 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2014
From: MARTIN PRODUCT SALES LLC
To: SANDVIK PROCESS SYSTEMS LLC
Reel/Frame 033282/0629 →
RELEASE OF SECURITY INTEREST Recorded Jun 13, 2014
From: REGIONS BANK, AS AGENT
To: MARTIN PRODUCT SALES LLC; MARTIN RESOURCE MANAGEMENT CORPORATION
Reel/Frame 033146/0990 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2013
From: BRIMROCK US LLC
To: MARTIN PRODUCT SALES LLC
Reel/Frame 031814/0103 →
NUNC PRO TUNC ASSIGNMENT Recorded Dec 17, 2013
From: BRIMROCK INTERNATIONAL INC.
To: BRIMROCK US LLC
Reel/Frame 031802/0847 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 9, 2011
From: BRIMROCK US LLC
To: BRIMROCK INTERNATIONAL INC.
Reel/Frame 026718/0191 →
SECURITY AGREEMENT Recorded Jan 6, 2011
From: MARTIN RESOURCE MANAGEMENT CORPORATION; MARTIN PRODUCT SALES LLC; MARTIN RESOURCE LLC; MARTIN UNDERGROUND STORAGE, INC.; CROSS OIL REFINING & MARKETING, INC.; BERRY PETROLEUM COMPANY; BRIMROCK US LLC; ALTEC ENVIRONMENTAL CONSULTING LLC; MARTIN TRANSPORT, INC.; MIDSTREAM FUEL SERVICE LLC
To: REGIONS BANK, AS AGENT
Reel/Frame 025596/0001 →
CHANGE OF NAME Recorded Feb 12, 2010
From: MARTIN INTEGRATED SULFUR SYSTEMS LLC
To: BRIMROCK US LLC
Reel/Frame 023931/0844 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 12, 2010
From: MARTIN RESOURCE MANAGEMENT CORPORATION
To: MARTIN INTEGRATED SULFUR SYSTEMS, LLC
Reel/Frame 023931/0685 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2007
From: KOTEN, JEAN-MARIE
To: MARTIN RESOURCE MANAGEMENT CORPORATION
Reel/Frame 020079/0155 →
Continuity (1)
Related Publication 20090108481A1 · Apr 30, 2009