IP Library Granted Patent US 7,550,457
Granted Patent B2
US 7,550,457 · App. 11/981,422 · Granted Jun 23, 2009

Pharmaceutically effective compounds

Assignee: CytRx Corporation
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Quick Facts
Patent No.
US 7,550,457
App. No.
11/981,422
Granted
Jun 23, 2009
Kind
B2
Abstract

The subject invention relates to carboxamidine derivatives, to pharmaceutical compositions containing the carboxamidine derivatives of the invention, and the use thereof for the treatment of vascular diseases and in the preparation of pharmaceutical compositions for the treatment of vascular diseases.

Claims (46)

1. A method for treating a vascular disease or vascular disorder comprising administering to a patient in need thereof an effective amount of a compound of formula III as defined below:

wherein R 1 and R 2 are independently hydrogen, straight chained C 1-6 alkyl group optionally substituted with a phenyl group, branched C 1-6 alkyl group optionally substituted with a phenyl group, or

R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is optionally substituted with one or more hydroxy, oxo or benzyl groups;

A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl, nitro, or halogen, or is a 5-6 membered heteroaromatic ring containing at least one heteroatom is selected from the group consisting of nitrogen, oxygen and sulfur, wherein the nitrogen heteroatom is optionally an N-oxide structure;

n is 0, 1, or 2;

z is 0 or 1;

with the proviso that

if R 1 and R 2 independently represent a hydrogen atom, a straight chained C 1-6 alkyl group optionally substituted with a phenyl group, a branched C 1-6 alkyl group optionally substituted with a phenyl group, or together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, then A is a heteroaromatic ring containing oxygen or sulfur heteroatom or an N-containing heteroaromatic ring having an N-oxide structure on the nitrogen heteroatom and

if A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl or nitro groups or halogen, or is a 5-6 membered N-containing heteroaromatic ring, then R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is substituted with one or more hydroxy, oxo, or benzyl groups;

or a stereoisomer or salt thereof.

2. The method according to claim 1 , wherein the compound is 5,6-dihydro-5-[(1 -piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

3. The method according to claim 1 , wherein the compound is 5,6-dihydro-5-[(4-benzyl-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

4. The method according to claim 1 , wherein the compound is 5,6-dihydro-5-[(2-oxo-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

5. The method according to claim 1 , wherein the compound is (+)-5,6-dihydro-5-[(1-piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

6. The method according to claim 1 , wherein the compound is 5,6-dihydro-5-[(1-oxido-1-piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

7. The method according to claim 1 , wherein the compound is 5,6-dihydro-5-[(4-hydroxy-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

8. A method for inhibiting or reversing damage to one or more endothelial cells comprising administering to the one or more endothelial cells an effective amount of a compound of formula III as defined below:

wherein R 1 and R 2 are independently hydrogen, straight chained C 1-6 alkyl group optionally substituted with a phenyl group, branched C 1-6 alkyl group optionally substituted with a phenyl group, or

R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is optionally substituted with one or more hydroxy, oxo or benzyl groups;

A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl, nitro, or halogen, or is a 5-6 membered heteroaromatic ring containing at least one heteroatom is selected from the group consisting of nitrogen, oxygen and sulfur, wherein the nitrogen heteroatom is optionally an N-oxide structure;

n is 0, 1, or 2;

z is 0 or 1;

with the proviso that

if R 1 and R 2 independently represent a hydrogen atom, a straight chained C 1-6 alkyl group optionally substituted with a phenyl group, a branched C 1-6 alkyl group optionally substituted with a phenyl group, or together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, then A is a heteroaromatic ring containing oxygen or sulfur heteroatom or an N-containing heteroaromatic ring having an N-oxide structure on the nitrogen heteroatom and

if A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl or nitro groups or halogen, or is a 5-6 membered N-containing heteroaromatic ring, then R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is substituted with one or more hydroxy, oxo, or benzyl groups;

or a stereoisomer or salt thereof.

9. The method according to claim 8 , wherein the compound is 5,6-dihydro-5-[(1-piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

10. The method according to claim 8 , wherein the compound is 5,6-dihydro-5-[(4-benzyl-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

11. The method according to claim 8 , wherein the compound is 5,6-dihydro-5-[(2-oxo-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

12. The method according to claim 8 , wherein the compound is (+)-5,6-dihydro-5-[(1-piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

13. The method according to claim 8 , wherein the compound is 5,6-dihydro-5-[(1-oxido-1-piperidinyl)methyl]-3-(1-oxido-3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

14. The method according to claim 8 , wherein the compound is 5,6-dihydro-5-[(4-hydroxy-1-piperidinyl)methyl]-3-(3-pyridyl)-4H-1,2,4-oxadiazine, or a stereoisomer or salt thereof.

15. The method of claim 8 , wherein the compound is administered to one or more of the endothelial cells in culture.

16. The method of claim 8 , wherein the compound is administered to one or more endothelial cells of a patient.

17. A method for increasing vaso-relaxation of a vessel associated with endothelial cells comprising administering to the cells an effective amount of a compound of formula III as defined below:

wherein R 1 and R 2 are independently hydrogen, straight chained C 1-6 alkyl group optionally substituted with a phenyl group, branched C 1-6 alkyl group optionally substituted with a phenyl group, or

R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is optionally substituted with one or more hydroxy, oxo or benzyl groups;

A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl, nitro, or halogen, or is a 5-6 membered heteroaromatic ring containing at least one heteroatom is selected from the group consisting of nitrogen, oxygen and sulfur, wherein the nitrogen heteroatom is optionally an N-oxide structure;

n is 0, 1, or 2;

z is 0 or 1;

with the proviso that

if R 1 and R 2 independently represent a hydrogen atom, a straight chained C 1-6 alkyl group optionally substituted with a phenyl group, a branched C 1-6 alkyl group optionally substituted with a phenyl group, or together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, then A is a heteroaromatic ring containing oxygen or sulfur heteroatom or an N-containing heteroaromatic ring having an N-oxide structure on the nitrogen heteroatom and

if A is a phenyl group optionally substituted with one or more C 1-4 alkyl, C 1-4 haloalkyl or nitro groups or halogen, or is a 5-6 membered N-containing heteroaromatic ring, then R 1 and R 2 together with the nitrogen atom attached thereto form a 5-7 membered saturated heterocyclic ring optionally containing further nitrogen and/or oxygen heteroatom, wherein said heterocyclic ring is substituted with one or more hydroxy, oxo, or benzyl groups;

or a stereoisomer or salt thereof.

18. The method of claim 17 , wherein the compound is administered to one or more of the endothelial cells in culture.

19. The method of claim 17 , wherein the compound is administered to one or more endothelial cells of a patient.

Assignments (6)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 6, 2022
From: KEMPHARM, INC.
To: KEMPHARM DENMARK A/S
Reel/Frame 060592/0595 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 6, 2022
From: ORPHAZYME A/S
To: KEMPHARM, INC.
Reel/Frame 060592/0646 →
CHANGE OF NAME Recorded Apr 11, 2018
From: ORPHAZYME APS
To: ORPHAZYME A/S
Reel/Frame 045911/0992 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2012
From: CYTRX CORPORATION
To: ORPHAZYME APS
Reel/Frame 027901/0269 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 4, 2009
From: CSAKAI, ZITA JEGESNE; MARVANYOS, EDE; UROGDI, LASZLO; TOROK, MAGDOLNA BATHONE; DENES, LASZLO
To: BIOREX RESEARCH AND DEVELOPMENT CO.
Reel/Frame 023050/0725 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 4, 2009
From: BIOREX KUTATO ES FEJLESZTO RT. ("V.A."); BIOREX RESEARCH AND DEVELOPMENT CO.
To: CYTRX CORPORATION
Reel/Frame 023050/0893 →
Priority Claims (2)
HU 0200109 · Jan 11, 2002 · national
HU 0204362 · Dec 17, 2002 · national
Continuity (3)
Division 1088996600 · Jul 12, 2004
Continuation In Part PCTHU030000300 · Jan 10, 2003
Related Publication 20080058323A1 · Mar 6, 2008