IP Library › Granted Patent US 7,696,375
Granted Patent B2
US 7,696,375 · App. 11/995,864 · Granted Apr 13, 2010

Method for producing lactic acid ester

Assignee: Toyota Jidosha Kabushiki Kaisha
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Quick Facts
Patent No.
US 7,696,375
App. No.
11/995,864
Granted
Apr 13, 2010
Kind
B2
Abstract

This invention provides a method for producing a lactic acid ester that can minimize input energy at the time of production, that can reduce chemical costs, and that can minimize equipment costs. This method comprises steps of: performing an esterification reaction in a reaction solution containing ammonium lactate obtained via fermentation and alcohol with an ammonia concentration of 1.0% by weight or lower; and recovering the lactic acid ester synthesized in the above step.

Claims (5)

1. A method for producing a lactic acid ester comprising:

performing an esterification reaction in a reaction solution containing ammonium lactate obtained via fermentation and alcohol comprising adjusting the ammonia concentration in the reaction solution to an ammonia concentration of between 0.3% and 0.8% by weight; and

recovering the lactic acid ester synthesized in the esterification reaction wherein the esterification reaction is completed at a conversion rate that is 50% to 90% of the equilibrium conversion rate of the esterification reaction.

2. The method for producing a lactic acid ester according to claim 1 , wherein the ammonia contained in the reaction solution is discharged to the outside of the reaction system with butanol vapor.

3. The method for producing a lactic acid ester according to claim 1 , wherein at least some of the liquid remaining after the recovery of the lactic acid ester is reacted with additional reaction solution.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 16, 2012
From: TOYOTA JIDOSHA KABUSHIKI KAISHA
To: TEIJIN LIMITED
Reel/Frame 028560/0063 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 16, 2012
From: TEIJIN LIMITED
To: UNITIKA LTD.
Reel/Frame 028560/0078 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 16, 2008
From: KUROMIYA, SHIGERU; SAOTOME, OSAMU; YAMAGUCHI, IKUO; HABU, KAZUNORI
To: TOYOTA JIDOSHA KABUSHIKI KAISHA
Reel/Frame 020372/0039 →
Priority Claims (1)
JP 2005-217749 · Jul 27, 2005 · national
Continuity (1)
Related Publication 20090105501A1 · Apr 23, 2009