IP Library Granted Patent US 7,858,377
Granted Patent B2
US 7,858,377 · App. 12/097,047 · Granted Dec 28, 2010

Method for preparing a quality control mixture for glycine tablets

Assignee: Nekommercheskoe Uchrezhdenie “Nauchno-Issledovateljskiyj Institut Citokhimii I Molekulyarnoyj Farmakologii”
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Quick Facts
Patent No.
US 7,858,377
App. No.
12/097,047
Granted
Dec 28, 2010
Kind
B2
Abstract

A method is described for preparing a mixture for quality control of 0.1 g glycine tablets for sublingual application. The mixture for quality control includes a 100:1 ratio of water to porphyrized tablets, each tablet containing 0.101 g microcapsules of non-agglomerated crystals of amino-acetic acid covered with polymeric film of water-soluble methylcellulose, each tablet further comprising 0.001 g magnesium stearate. The process of dissolution takes 20 minutes and is carried out at a temperature of 37° C. in an apparatus using a paddle rotation speed of 150 revolutions per minute. After the mixture is dissolved, it is allowed to stand for 10 minutes, then a light transmission coefficient is measured at 700±2 nm for a 10 mm thick layer of the mixture. A transmission value within the range of 50% to 70% compared to purified water corresponds to the proper quality.

Claims (11)

1. A method of preparing a mixture for quality control of 0.1 g glycine tablets for sublingual application,

the tablets having stress-preventative, anti-stress, nootropic, and neuroprotective effects,

the tablets being suitable for single administration or for long-term treatment,

each tablet comprising microcapsulated glycine comprising non-agglomerated crystals of amino-acetic acid covered with a polymeric film of water-soluble methylcellulose,

each tablet further comprising magnesium stearate,

each tablet having a crush resistance of at least 10 N and no more than 30 N,

the method comprising:

providing said tablets that have been porphyrized;

obtaining the mixture by mixing 2.5 g of porphyrized tablets in 250 mL purified water for 20 minutes at a temperature of 37° C. in an apparatus using a paddle rotation speed of 150 revolutions per minute;

allowing the mixture to stand for 10 minutes; and

measuring a light transmission coefficient of 4 mL of the mixture for a 10 mm thick layer in a container relative to the light transmission coefficient for purified water using a light transmission spectrophotometer at a wavelength of 700±2 nm.

Assignments (2)
CHANGE OF NAME Recorded Dec 29, 2014
From: NEKOMMERCHESKOE UCHREZHDENIE "NAUCHNO-ISSLEDOVATELJSKIYJ INSTITUT CITOKHIMII I MOLEKULYARNOYJ FARMAKOLOGII"
To: CHASTNOE UCHREZHDENIE "NAUCHNO-ISSLEDOVATELJSKIYJ INSTITUT CITOKHIMII I MOLEKULYARNOYJ FARMAKOLOGII"
Reel/Frame 034708/0245 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 17, 2010
From: KOMISSAROVA, IRINA ALEKSEEVNA; SOLDATENKOVA, TATJYANA DMITRIEVNA; GUDKOVA, YULIYA VASILJEVNA; KONDRASHOVA, TATJYANA TIKHONOVNA; BURBENSKAYA, NATALJYA MIKHAYJLOVNA
To: NEKOMMERCHESKOE UCHREZHDENIE "NAUCHNO-ISSLEDOVATELJSKIYJ INSTITUT CITOKHIMII I MOLEKULYARNOYJ FARMAKOLOGII"
Reel/Frame 025382/0651 →
Priority Claims (1)
EA 200600147 · Dec 16, 2005 · regional
Continuity (1)
Related Publication 20090124018A1 · May 14, 2009