IP Library Granted Patent US 8,431,406
Granted Patent B2
US 8,431,406 · App. 12/229,466 · Granted Apr 30, 2013

Terpyridine-substituted compounds and related selective detection methods

Inventors: Gregory N. Tew (Amherst, MA); Raja Shunmugam (Amherst, MA)
Assignee: University of Massachusetts
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Quick Facts
Patent No.
US 8,431,406
App. No.
12/229,466
Granted
Apr 30, 2013
Kind
B2
Abstract

Terpyridine-substituted compounds, compositions and/or related methods, as can be used to selectively detect a wide range of analytes.

Claims (12)

1. A method of detecting Hg 2+ ion, the method comprising:

contacting a compound comprising a terpyridine moiety with a sample to be tested for the presence of Hg 2+ under a condition such that, if Hg 2+ ions are present in the sample, at least some of Hg 2+ ions present will bind with the terpyridine moiety; and

detecting a colorimetric change of the sample resulting from the binding of Hg 2+ ions, if present, with the terpyridine moiety,

wherein the compound is a polymer and the terpyridine moiety is pendent to a monomeric component of the polymer, and wherein the colorimetric change is detectable in the presence of one or more ions selected from the group consisting of Ag + , Ba 2+ , Pb 2+ , Cd 2+ , Ca 2+ , Mg 2+ , and Zn 2+ and provides a limit of detection of 2 ppb Hg 2+ at 557 nm, wherein the polymer comprises a backbone selected from the group consisting of a poly(alkylene oxide) backbone, a poly(alkylene) backbone and a poly(methylmethacrylate) backbone.

2. The method of claim 1 , wherein the sample comprises at least one non-Hg ion.

3. The method of claim 2 , wherein the colorimetric change comprises a visible color change.

4. The method of claim 2 , wherein the polymer comprises the poly(alkylene oxide) backbone.

5. The method of claim 2 , wherein the polymer comprises the poly(alkylene) backbone.

6. The method of claim 2 , wherein the polymer comprises the poly(methylmethacrylate) backbone.

7. The method of claim 2 , wherein the polymer is in a medium selected from solid and liquid media.

8. The method of claim 7 , wherein the solid medium comprises a substrate coupled to the polymer compound, the substrate being selected from metallic, polymeric and cellulosic substrates.

9. The method of claim 8 , wherein the solid medium comprises a paper strip coated with the compound.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 21, 2010
From: UNIVERSITY OF MASSACHUSETTS
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 024422/0820 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 17, 2008
From: TEW, GREGORY N.; SHUNMUGAM, RAJA
To: UNIVERSITY OF MASSACHUSETTS
Reel/Frame 021842/0121 →
Continuity (2)
Provisional Application 60965768 · Aug 22, 2007
Related Publication 20110065195A1 · Mar 17, 2011