IP Library Granted Patent US 7,534,490
Granted Patent B1
US 7,534,490 · App. 12/236,389 · Granted May 19, 2009

Composite nanoparticles, nanoparticles and methods for producing same

Assignee: Northern Nanotechnologies, Inc.
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Quick Facts
Patent No.
US 7,534,490
App. No.
12/236,389
Granted
May 19, 2009
Kind
B1
Abstract

In various aspects provided are methods for producing a nanoparticle within a cross-linked, collapsed polymeric material. In various embodiments, the methods comprise (a) providing a polymeric solution comprising a polymeric material; (b) collapsing at least a portion of the polymeric material about one or more precursor moieties; (c) cross-linking the polymeric material; (d) modifying at least a portion of said precursor moieties to form one or more nanoparticles and thereby forming a composite nanoparticle.

Claims (28)

1. A method for producing a composite nanoparticle, comprising the steps of:

a) providing a polymeric solution comprising a polymeric material and a solvent;

b) collapsing at least a portion of the polymeric material about one or more precursor moieties to form a composite precursor moiety having a mean diameter in the range between about 1 nm and about 100 nm;

c) cross-linking the polymeric material of said composite precursor moiety; and

d) modifying at least a portion of said precursor moieties of said composite precursor moiety to form one or more nanoparticles and thereby forming a composite nanoparticle.

2. The method of claim 1 , wherein said composite nanoparticle has a mean diameter in the range between about 1 nm and about 100 nm.

3. The method of claim 1 , wherein said collapsing step comprises adding a collapsing agent to the polymeric solution.

4. The method of claim 1 , wherein said precursor moiety is a collapsing agent.

5. The method of claim 4 , wherein the collapsing agent comprises at least one ionic species.

6. The method of claim 5 , wherein the said at least one ionic species that is a salt and comprises one or more inorganic salts, organic salts, or combination thereof.

7. The method of claim 1 , wherein said modifying step comprises exposing said composite precursor moiety to electromagnetic radiation to effect formation of the nanoparticle from said precursor moiety.

8. The method of claim 1 , wherein said modifying step comprises subjecting said composite precursor moiety to a chemical treatment.

9. The method of claim 8 , wherein said chemical treatment results in a reduction or oxidation of said precursor moiety.

10. The method of claim 8 , wherein said chemical treatment comprises addition of a counter ion to a precursor moiety of a composite precursor moiety, or precursor of said counter ion, to effect formation of the nanoparticle from said precursor moiety.

11. The method of claim 1 , wherein said solvent is an aqueous solution.

12. The method of claim 1 , wherein said one or more precursor moieties are one or more of a metal cation, complexed metal cation or complexed metal anion.

13. The method of claim 12 , wherein at least a portion of said precursor moieties comprise two or more different metals; and wherein the nanoparticle formed by the modifying step comprises an alloy of two or more of the two or more metals.

14. The method of claim 1 , wherein said polymeric material comprises linear or branched segments comprising polyions, the polyions comprising one or more anions, cations, or combinations thereof.

15. The method of claim 1 , wherein said polymeric material comprises one or more functional groups.

16. A method for producing a nanoparticle material, comprising the steps of:

a) providing a polymeric solution comprising a polymeric material and a solvent;

b) collapsing at least a portion of the polymeric material about one or more precursor moieties to form a composite precursor moiety;

c) cross-linking the polymeric material of said composite precursor moiety; and

d) modifying at least a portion of said precursor moieties of said composite precursor moiety to form one or more nanoparticles having a mean diameter in the range between about 1 nm and about 100 nm and thereby forming a composite nanoparticle; and

e) pyrolysing said composite nanoparticle to form a nanoparticle material.

17. The method of claim 16 , wherein the pyrolysis substantially removes the polymeric material from the composite nanoparticle.

18. The method of claim 16 , wherein the pyrolysis conditions are controlled such that the nanoparticle material formed comprises at least a partially carbon-coated nanoparticle.

19. An at least partially carbon-coated nanoparticle when made by a method as claimed in claim 18 .

Assignments (6)
SECURITY INTEREST Recorded Apr 18, 2022
From: VIVE CROP PROTECTION INC.
To: SILICON VALLEY BANK
Reel/Frame 059627/0547 →
RELEASE OF SECURITY INTEREST Recorded Mar 15, 2022
From: CANADIAN IMPERIAL BANK OF COMMERCE
To: VIVE CROP PROTECTION INC.
Reel/Frame 059271/0993 →
SECURITY INTEREST Recorded Oct 1, 2019
From: VIVE CROP PROTECTION INC
To: CANADIAN IMPERIAL BANK OF COMMERCE, AS LENDER
Reel/Frame 050582/0102 →
CHANGE OF NAME Recorded Mar 1, 2012
From: VIVE NANO INC.
To: VIVE CROP PROTECTION INC.
Reel/Frame 027793/0715 →
CHANGE OF NAME Recorded Apr 10, 2009
From: NORTHERN NANOTECHNOLOGIES, INC.
To: VIVE NANO, INC.
Reel/Frame 022534/0706 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2009
From: GOH, CYNTHIA M.; GOH, JANE B.; DINGLASAN, JOSE ARMANDO; LOO, RICHARD; VELENTANLIC, EMINA
To: NORTHERN NANOTECHNOLOGIES, INC.
Reel/Frame 022438/0093 →
Continuity (4)
Continuation 1174537700 · May 7, 2007
Continuation 1174950700 · May 16, 2007
Continuation PCTCA200600168600 · Oct 13, 2006
Provisional Application 6072618400 · Oct 14, 2005