IP Library Granted Patent US 7,723,251
Granted Patent B2
US 7,723,251 · App. 12/287,347 · Granted May 25, 2010

Method of regeneration of SCR catalyst

Assignee: Evonik Energy Services LLC
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Quick Facts
Patent No.
US 7,723,251
App. No.
12/287,347
Granted
May 25, 2010
Kind
B2
Abstract

A method of regeneration of a SCR catalyst for use in a power plant facility burning fossil fuels, bio-based fuels, or a combination thereof, wherein poisons are removed from the catalyst. The method is suitable for use during neutralization using C 1 to C 8 carboxylic acids.

Claims (19)

1. A method of regenerating a SCR catalyst, the method comprising:

treating a used catalyst with a basic solution, and

treating the basic solution remaining in the used catalyst with an organic acid at a pH in a range of up to about 5.5 for a time period of up to about four hours to effect neutralization of the basic solution remaining in the used catalyst after the treatment of the used catalyst with the basic solution.

2. The method according to claim 1 , wherein the pH is in a range of from about 1 to about 5.5.

3. The method according to claim 1 , wherein the time period is in a range of from about thirty minutes to about four hours.

4. The method according to claim 1 , wherein the organic acid is a C 1 to C 8 carboxylic acid.

5. The method according to claim 4 , wherein the C 1 to C 8 carboxylic acid is selected from the group consisting of formic acid, acetic acid, and a combination thereof.

6. A method of regenerating a SCR catalyst, the method comprising:

treating a used catalyst with a basic solution, and

treating the basic solution remaining in the used catalyst with a C 1 to C 8 carboxylic acid to effect neutralization of the basic solution remaining in the used catalyst.

7. The method according to claim 6 , wherein the C 1 to C 8 carboxylic acid is selected from the group consisting of formic acid, acetic acid, and a combination thereof.

8. A method of regenerating a SCR catalyst, the method comprising:

treating a used catalyst with a basic solution, and

treating the basic solution remaining in the used catalyst with a C 1 to C 8 carboxylic acid to increase neutralization rate of the basic solution remaining in the used catalyst.

9. The method according to claim 8 , wherein the C 1 to C 8 carboxylic acid is selected from the group consisting of formic acid, acetic acid, and a combination thereof.

10. A method of regenerating a SCR catalyst, the method comprising:

treating a used catalyst with a basic solution, and

treating the basic solution remaining in the used catalyst with a C 1 to C 8 carboxylic acid to reduce mobilization of iron ions in the basic solution remaining in the used catalyst.

11. The method according to claim 10 , wherein the C 1 to C 8 carboxylic acid is selected from the group consisting of formic acid, acetic acid, and a combination thereof.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2012
From: STEAG ENERGY SERVICES LLC
To: STEAG ENERGY SERVICES GMBH
Reel/Frame 028140/0666 →
CHANGE OF NAME Recorded Jan 27, 2012
From: EVONIK ENERGY SERVICES LLC
To: STEAG ENERGY SERVICES LLC
Reel/Frame 027611/0821 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 8, 2008
From: HARTENSTEIN, HANS-ULRICH; HOFFMANN, THIES
To: EVONIK ENERGY SERVICES LLC
Reel/Frame 021706/0463 →
Continuity (2)
Provisional Application 6106898900 · Mar 11, 2008
Related Publication 20090233786A1 · Sep 17, 2009