IP Library Granted Patent US 8,163,715
Granted Patent B2
US 8,163,715 · App. 12/298,680 · Granted Apr 24, 2012

Inulin of very high chain length

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Quick Facts
Patent No.
US 8,163,715
App. No.
12/298,680
Granted
Apr 24, 2012
Kind
B2
Abstract

The invention relates to a long-chain inulin and its preparation from artichoke roots, to its use in foodstuffs and cosmetic preparations and to foodstuffs and cosmetic preparations which comprise the long-chain inulin.

Claims (53)

1. Inulin having a weight average degree of polymerization DP W of between 83 and 103, wherein said inulin is spray-dried.

2. The inulin of claim 1 , wherein said inulin has a weight average degree of polymerization DP W of between 85 and 95.

3. The inulin of claim 1 , wherein said inulin has a degree of branching of between 0.5 and 2.0 mol % of 2-1,6 linked fructose monomers based on all inulin monomers.

4. The inulin of claim 1 , wherein the quotient between the weight average degree of polymerization and the number average degree of polymerization (DPw/DPn) of said inulin is less than 1.25.

5. The inulin of claim 1 , wherein the quotient DPw/DPn of said inulin is less than 1.20.

6. The inulin of claim 1 , wherein the quotient DPw/DPn of said inulin is less than 1.15.

7. The inulin of claim 1 , wherein said inulin has a glucose content less than 2% by weight based on the total dry weight.

8. The inulin of claim 1 , wherein said inulin has a glucose content less than 1% by weight based on the total dry weight.

9. The inulin of claim 1 , wherein said inulin has a fructose content less than 2.5% by weight based on the total dry weight.

10. The inulin of claim 1 , wherein said inulin has a fructose content less than 1.5% by weight based on the total dry weight.

11. The inulin of claim 1 , wherein said inulin has a weight average degree of polymerization DP W of between 85 and 95.

12. The inulin of claim 1 , wherein said inulin is in the form of particles with an average diameter of 100-250 μm.

13. A process for obtaining inulin comprising

a) comminuting artichoke roots,

b) obtaining an extract by treating the comminuted roots with water,

c) removing coloring constituents from the extract,

d) precipitating inulin from the extract,

e) reprecipitating the inulin at least once,

f) dissolving and filtering the inulin obtained in step e), and

g) precipitating and separating the inulin obtained in step f),

wherein said inulin has a weight average degree of polymerization DP W of between 83 and 103.

14. The process as claimed in claim 13 , further comprising an additional filtration step.

15. The process as claimed in claim 13 wherein the coloring constituents are removed in step c) by

i) admixing magnesium ions (Mg 2+ ) to the plant extract,

ii) admixing at least one alkaline component to the plant extract,

iii) forming a precipitate, and

iv) removing the precipitate which has formed from the plant extract.

16. The process as claimed in claim 15 , further comprising admixing a magnesium salt in step i).

17. The process as claimed in claim 16 , wherein the magnesium salt is magnesium chloride, magnesium sulfate, magnesium nitrate, magnesium acetate, or magnesium propionate.

18. The process as claimed in claim 15 , wherein step i) is carried out at a temperature of 60-80° C.

19. The process as claimed in claim 15 , wherein the amount of alkaline component is chosen so that the OH − :Mg 2+ molar ratio set up is 2.2:1-1.8:1.

20. The process as claimed in claim 15 , wherein the alkaline component is an aqueous solution or suspension of an alkali metal hydroxide or alkaline earth metal hydroxide.

21. The process as claimed in claim 15 , wherein the alkaline component is a suspension of calcium hydroxide.

22. A foodstuff comprising inulin having an average degree of polymerization DP w of between 83 and 103.

23. The foodstuff as claimed in claim 22 , wherein said foodstuff is a dairy product, yoghurt, ice cream, milk-based soft ice, milk-based garnish, pudding, milkshake, egg custard, cheese, nutrition bar, energy bar, breakfast bar, confectionery, bakery product, cracker, cookie, biscuit, cereal chip, snack product, ice tea, soft ice made from fruit juice, diet drink, finished drink, sports drink, stamina drink, powdered drink mixture for dietary supplementation, infant and baby food, calcium-supplemented orange juice, bread, croissant, breakfast cereal, noodle, spread, sugar-free biscuit, sugar-free chocolate, calcium chew, meat product, mayonnaise, salad dressing, nut butter, deep-frozen meal, sauce, soup or ready-to-serve meal.

24. The foodstuff as claimed in claim 22 , wherein said foodstuff is an extrusion product.

25. A dietary supplement comprising inulin having an average degree of polymerization DP w of between 83 and 103.

26. A cosmetic preparation comprising inulin having an average degree of polymerization DP w of between 83 and 103.

27. A method for manufacture of a foodstuff comprising adding inulin having an average degree of polymerization DP w of between 83 and 103 to a foodstuff.

28. The method as claimed in claim 27 , wherein said inulin acts as an additive with prebiotic properties, a texturizing agent, a stability enhancing agent, a viscosity-building agent, and/or a dietary fiber in said foodstuff.

29. A method of making a foodstuff comprising inulin having an average degree of polymerization DP w of between 83 and 103 comprising adding inulin to a food stuff, wherein said inulin acts as a fat or oil substitute in said foodstuff.

30. A method for manufacture of a cosmetic preparation comprising adding inulin having an average degree of polymerization DP w of between 83 and 103 to a cosmetic preparation.

31. The method as claimed in claim 30 , wherein said inulin acts as a texturizing agent, a stability enhancing agent, and/or a viscosity-building agent in said cosmetic preparation.

32. An aqueous paste comprising the inulin having an average degree of polymerization DP w of between 83 and 103.

33. A method for the manufacture of a foodstuff or a cosmetic preparation comprising adding the aqueous paste as claimed in claim 32 , wherein the inulin in the aqueous paste acts as a structure imparting component, a fat substitute, an oil substitute, a texturizing agent, a stability enhancing agent, and/or a viscosity-building agent in said foodstuff or cosmetic preparation.

34. The process as claimed in claim 13 , further comprising spray drying said inulin.

35. The foodstuff as claimed in claim 22 , wherein said inulin is spray-dried.

36. The dietary supplement as claimed in claim 25 , wherein said inulin is spray-dried.

37. The cosmetic preparation as claimed in claim 26 , wherein said inulin is spray-dried.

38. The method as claimed in claim 27 , wherein said inulin is spray-dried.

39. The method as claimed in claim 29 , wherein said inulin is spray-dried.

40. The method as claimed in claim 30 , wherein said inulin is spray-dried.

41. The aqueous paste as claimed in claim 32 , wherein said inulin is spray-dried.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Jul 4, 2023
From: BAYER INTELLECTUAL PROPERTY GMBH
To: BAYER CROPSCIENCE AKTIENGESELLSCHAFT
Reel/Frame 064198/0823 →
CHANGE OF ADDRESS Recorded Jun 12, 2023
From: BAYER INTELLECTUAL PROPERTY GMBH
To: BAYER INTELLECTUAL PROPERTY GMBH
Reel/Frame 064021/0344 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 2, 2015
From: BAYER CROPSCIENCE AG
To: BAYER INTELLECTUAL PROPERTY GMBH
Reel/Frame 035355/0836 →