Capillary electrophoresis apparatus
View Patent ↗The invention provides a capillary electrophoresis apparatus which can improve the operability and measuring speed. According to the invention, a sensor for identifying the type of sample containers is fixed at the position away from a capillary anode electrode. The sensor is made to be closer to the sample containers by moving a moving stage so that the sample containers disposed on the moving stage can be identified by the sensor. A fixing apparatus for fixing at least a pair of sample containers is provided on the moving stage.
1. A capillary electrophoresis apparatus comprising:
a capillary in which a capillary head is provided at one end and a capillary anode electrode is formed at the other end; and
an autosampler having a moving stage which transports one or a plurality of containers including sample containers to the capillary anode electrode;
wherein the moving stage has a fixing apparatus for fixing at least a pair of sample containers which are arranged and disposed on the moving stage,
the fixing apparatus has first and second movable hooks as well as first, second, and third fixed hooks which are arranged in a row, the movable hooks have projected portions rotatable around a shaft, the first fixed hook has a projected portion which is projected on an inside, the second fixed hook has first and second projected portions which are projected on both sides, the third fixed hook has a projected portion which is projected on an inside,
when a first sample container having holes on side surfaces of both sides is disposed between the first fixed hook and the second fixed hook and a second sample container having holes on side surfaces of both sides is disposed between the second fixed hook and the third fixed hook,
wherein, the capillary electrophoresis apparatus is configured in such a manner that when the hole of the outside side surface of the first sample container is engaged with the projected portion of the first fixed hook, the hole of the inside side surface of the first sample container is engaged with the first projected portion of the second fixed hook, the hole of the inside side surface of the second sample container is engaged with the second projected portion of the second fixed hook, the hole of the outside side surface of the second sample container is engaged with the projected portion of the third fixed hook,
the projected portion of the first movable hook is pressed against the outside side surface of the first sample container, and the projected portion of the second movable hook is pressed against the outside side surface of the second sample container
wherein two concave portions are provided on each of the bottom surfaces of the first and second sample containers, convex portions corresponding to the concave portions are provided on the moving stage, when the first sample container is disposed to the first fixed hook and the second fixed hook and the second sample container is disposed to the second fixed hook and the third fixed hook, the corresponding convex portions on the moving stage are engaged with the two concave portions on each of bottom surfaces of the first and second sample containers,
a gap between the first concave portion on the bottom surface of each of the first and the second sample containers and the first convex portion on the moving stage is larger than a gap between the second concave portion on the bottom surface of each of the first and the second sample containers and the second convex portion on the moving stage and,
wherein when the projected portion of the first and second movable hooks are not pressed against the outside surfaces of the first and second sample containers, the first and second sample containers on the moving stage are pivotable around the second convex portions respectively on the moving stage which are engaged with their respective second concave portions on the bottom surfaces of the first and second sample containers, and the first and second sample containers are fixed on the moving stage by pressing the projected portions of the first and second movable hooks against their respective outside side surfaces of the first and second sample containers.
2. The capillary electrophoresis apparatus according to claim 1 , wherein the shaft is disposed in the vertical direction and the movable hook is rotatable along the horizontal plane.
3. The capillary electrophoresis apparatus according to claim 1 , wherein a spring which generates the torque allowing the movable hook to rotate around the shaft is provided, and by the torque, the movable hook is pressed in the direction where the projected portion of the movable hook is engaged with the hole of the outside side surface of the sample containers.